Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 1 o 10 REDRING SOLDER (M) SDN. BHD. LOT 17486, JALAN DUA, TAMAN SELAYANG BARU 68100 BATU CAVES, SELANGOR DARUL EHSAN, MALAYSIA The ollowing merchandise was (were) submitted and identiied by the client as: Sample Description : Pure Tin Sample Receiving Date : 04/07/2014 Testing Period : 04/07/2014 to 11/07/2014 Test Requested : Selected test(s) as requested by client Test Method : Please reer to next page(s). Test Results : Please reer to next page(s). Analysts : Loh Mei Theng, Tay Siam Pine & Teh Pui Sean
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 2 o 10 Test results: Test Part Description : Sample Description : Pure Tin RoHS Directive 2011/65/EU Annex II Test Item(s): Unit Test Method Results MDL Limit Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium (CrVI) by Spot test / boiling water extraction (optional) # Sum o PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl With reerence to IEC 62321-5:2013 (Determination o Cd by ICP-OES) With reerence to IEC 62321-5:2013 (Determination o Pb by ICP-OES) With reerence to IEC 62321-4:2013 (Determination o Hg by ICP-OES) --- Negative N.D. 2 100 33 2 1000 N.D. 2 1000 0.02 per 50cm 2 sample in 50mL solution N.D. - 1000 -
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 3 o 10 Sum o PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether N.D. - 1000 Note : (a) = ppm;0.1wt% = 1000ppm (b) N.D..= Not Detected (c) MDL = Method Detection Limit (d) # = a. Positive means the presence o CrVI on the tested areas b. Negative means the absence o CrVI on the tested areas For corrosion protection coatings on metals: Inormation on storage conditions and production date o the tested sample is unavailable and thus results or Cr(VI) represent status o the sample at the time o testing represent status o the sample at the time o testing. (e) - = not regulated
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 4 o 10 Test results by chemical method: Test Item (s): Unit Method Result MDL Antimony (Sb) With reerence to EPA Method 3051A, and perormed by ICP-OES N.D. 2 Halogen --- --- --- --- Halogen-Fluorine (F) With reerence to BS EN 14582. Analysis was perormed by IC method or Fluorine content. N.D. 50 Halogen-Chlorine (Cl) With reerence to BS EN 14582. Analysis was perormed by IC method or Chlorine content. N.D. 50 Halogen-Bromine (Br) With reerence to BS EN 14582. Analysis was perormed by IC method or Bromine content. N.D. 50 Halogen-Iodine (I) With reerence to BS EN 14582. Analysis was perormed by IC method or Iodine content. N.D. 50 Test Part Description: Sample Description : Pure Tin Note : (a) = ppm (b) N.D. = Not Detected (c) MDL = Method Detection Limit (d) --- = Not Conducted
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 5 o 10 Test result: Test Part Description : Sample Description : Pure Tin Optional: RoHS Directive 2011/65/EU, priority substances Test Item(s): Unit Test Method Results MDL Limit Hexabromocyclododecane (HBCDD) Based on IEC 62321:2008 (Determination o HBCDD by GC-MS) N.D. 10 - Bis (2-ethylhexyl) phthalate (DEHP) Based on EN 14372:2004 (Determination o DEHP by GC-MS) N.D. 30 - Butyl benzyl phthalate (BBP) Based on EN 14372:2004 (Determination o BBP by GC-MS) N.D. 30 - Dibutyl phthalate (DBP) Based on EN 14372:2004 (Determination o DBP by GC-MS) N.D. 30 - Note: (a) Reerence Inormation: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Hexabromocyclododecane (HBCDD), Bis (2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP) and Dibutyl phthalate (DBP) are considered as a priority or risk evaluation and substance restriction. (b) - = not regulated
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 6 o 10 Test Part Description : Sample Description : Pure Tin REDRING SOLDER (M) SDN. BHD. CTSSA/13164/14 SGS authenticate the photo on original report only
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 7 o 10 1. DETERMINATION OF CADMIUM CONTENT BY IEC 62321-5 2013 Sample Receiving and Registration Weight sample (0.2-0.5g) into digestion vessel Acid digestion (Microwave) Totally Dissolved Filtration Analyses by ICP 3. DETERMINATION OF MERCURY CONTENT BY IEC 62321-4 2013 Sample Receiving and Registration Weight sample (0.1-0.5g) into digestion vessel Acid digestion (Microwave) Totally Dissolved Filtration Analyses by ICP 2. DETERMINATION OF LEAD CONTENT BY IEC 62321-5 2013 Sample Receiving and Registration Weight sample (0.2-0.5g) into digestion vessel Acid digestion (Microwave) Totally Dissolved Filtration Analyses by ICP 4. DETERMINATION OF HEXAVALENT CHROMIUM BY IEC 62321 2008 Sample Receiving and Registration Sample Preparation Spot-test (Qualitative) Boiling-water-extraction Analyses by UV- Spectrophotometer Test Report 5. DETERMINATION OF PBB/PBDE WITH GC-MS BY IEC 62321 2008 Weight sample (0.5-4.0g) into extraction thimble Soxhlet Extraction with Toluene Filter through 0.45 um membrane ilter Analyses by GC-MS (with appropriate dilution)
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 8 o 10 6. MICROWAVE ASSISTED ACID DIGESTION OF ORGANICALLY BASED METRICES (US EPA 3051A) Weight sample (0.2-0.5g) into digestion vessel Acid digestion (HNO 3) Microwave Totally Dissolved Filtration Analyses by ICP 7. DETERMINATION OF HALOGEN CONTENT Sample pretreatment Weighting and putting sample in cell Combustion / Absorption Dilution to ixed volume Analyses by IC
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 9 o 10 DETERMINATION OF HBCDD CONTENT BY IEC 62321 2008 Weight sample (0.5-4.0g) into extraction thimble Soxhlet Extraction with Toluene Filter through 0.45 um membrane ilter Analyses by GC-MS (with appropriate dilution)
Test Report No. CTSSA/13164/14 Date: 11/07/2014 Page: 10 o 10 Analytical low chart o Phthalates Content Sample pre-treatment/separation Sample extraction by soxhlet method Concentrate/Dilute Extracted solution Analysis was perormed by GC/MS Data **** End o Report ****