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MATRIX Reference Code Analyte Code Description ASTM C471M- 14 2014 ASTM D5504-12 2012 3964 Orthorhombic Cyclooctasulfur 4842 1-Propanethiol 6113 2,5-Dimethylthiophene 4544 2-Ethylthiophene 4843 2-Propanethiol 5783 3-Methylthiophene 4450 Carbon disulfide 7215 Carbonyl sulfide 6078 Diethyl Disulfide 6081 Diethyl Sulfide 4729 Dimethyl disulfide 6116 Dimethyl Sulfide 7506 Ethanethiol 3840 Hydrogen sulfide 3725 i-butanethiol 7507 Methanethiol 7509 Methyl ethyl sulfide 9508 n-butanethiol 9556 t-butanethiol 9574 Tetrahydrothiophene 9578 Thiophene 30002256 Gypsum and Gypsum Products 30032270 Sulfur Compounds in Natural Gas and Gaseous Fuels by GC and Chemiluminescence EPA 325B 2013 10277437 Sorbent Tubes Coupled with Thermal Desorption and GC/MS EPA TO-10A (GC/ECD) OREGON Environmental Laboratory Program 9318 1,3-Butadiene 4375 Benzene 4765 Ethylbenzene 5240 m+p-xylene 5250 o-xylene 5140 Toluene 7355 4,4'-DDD 7360 4,4'-DDE 7365 4,4'-DDT 7025 Aldrin 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 10247504 Pesticides and PCBs with LV PUF by GC/ECD 1 of 7

7240 alpha-chlordane EPA TO-10A (GC/ECD) OREGON Environmental Laboratory Program 8880 Aroclor-1016 (PCB-1016) 8910 Aroclor-1260 (PCB-1260) 7115 beta-bhc (beta- Hexachlorocyclohexane) 7105 delta-bhc 7470 Dieldrin 7510 Endosulfan I 7515 Endosulfan II 7520 Endosulfan sulfate 7540 Endrin 7530 Endrin aldehyde 7535 Endrin ketone 7120 gamma-bhc (Lindane, gamma- HexachlorocyclohexanE) 7245 gamma-chlordane 7685 Heptachlor 7690 Heptachlor epoxide 7810 Methoxychlor EPA TO-13A 10248405 Polycyclic Aromatic Hydrocarbons in Ambient by GC/MS 5500 Acenaphthene 5505 Acenaphthylene 5555 Anthracene 5575 Benzo(a)anthracene 5580 Benzo(a)pyrene 5590 Benzo(g,h,i)perylene 5600 Benzo(k)fluoranthene 5585 Benzo[b]fluoranthene 5855 Chrysene 5895 Dibenz(a,h) anthracene 6265 Fluoranthene 6270 Fluorene 6315 Indeno(1,2,3-cd) pyrene 5005 Naphthalene 6615 Phenanthrene 6665 Pyrene EPA TO-15 10248803 VOCs collected in Canisters by GC/MS 5160 1,1,1-Trichloroethane 5110 1,1,2,2-Tetrachloroethane 5195 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 5165 1,1,2-Trichloroethane 4630 1,1-Dichloroethane 2 of 7

OREGON Environmental Laboratory Program EPA TO-15 4640 1,1-Dichloroethylene 5182 1,2,3-Trimethylbenzene 5155 1,2,4-Trichlorobenzene 5210 1,2,4-Trimethylbenzene 4570 1,2-Dibromo-3-chloropropane (DBCP) 4585 1,2-Dibromoethane (EDB, Ethylene dibromide) 4695 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon-114) 4610 1,2-Dichlorobenzene 4635 1,2-Dichloroethane (Ethylene dichloride) 4655 1,2-Dichloropropane 5215 1,3,5-Trimethylbenzene 9318 1,3-Butadiene 4615 1,3-Dichlorobenzene 4620 1,4-Dichlorobenzene 4735 1,4-Dioxane (1,4- Diethyleneoxide) 4836 1-Propene (Propylene) 5220 2,2,4-Trimethylpentane 4410 2-Butanone (Methyl ethyl ketone, MEK) 4538 2-Ethyltoluene 4860 2-Hexanone (MBK) 4531 3-Ethyltoluene (1-Methyl-3- ethylbenzene) 4542 4-Ethyltoluene 4910 4-Isopropyltoluene (p-cymene) 4995 4-Methyl-2-pentanone (MIBK) 4315 Acetone 4320 Acetonitrile 4325 Acrolein (Propenal) 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 4357 alpha-methylstyrene 6698 alpha-pinene 4375 Benzene 5635 Benzyl chloride 4385 Bromobenzene 4395 Bromodichloromethane 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane 4485 Chloroethane (Ethyl chloride) 3 of 7

OREGON Environmental Laboratory Program EPA TO-15 4505 Chloroform 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4555 Cyclohexane 4560 Cyclohexanone 4625 Dichlorodifluoromethane (Freon-12) 9375 Di-isopropylether (DIPE) 6208 d-limonene 4750 Ethanol 4755 Ethyl acetate 4765 Ethylbenzene 4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane) 4835 Hexachlorobutadiene 4890 Isopropyl acetate 4895 Isopropyl alcohol (2-Propanol, Isopropanol) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 4990 Methyl methacrylate 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5005 Naphthalene 4425 n-butyl alcohol (1-Butanol, n-butanol) 4415 n-butyl-acetate 4435 n-butylbenzene 5875 n-decane 6235 n-dodecane 4825 n-heptane 4855 n-hexane 5026 n-nonane 5027 n-octane 5090 n-propylbenzene 6747 n-undecane 5250 o-xylene 4440 sec-butylbenzene 5100 Styrene 4370 T-amylmethylether (TAME) 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5120 Tetrahydrofuran (THF) 4 of 7

OREGON Environmental Laboratory Program EPA TO-15 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5225 Vinyl acetate 5235 Vinyl chloride 5260 Xylene (total) EPA TO-17 10312206 Determination of Volatile Organic Compounds in Ambient Using Active Sampling Onto Sorbent Tubes 5160 1,1,1-Trichloroethane 5110 1,1,2,2-Tetrachloroethane 5195 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 5165 1,1,2-Trichloroethane 4630 1,1-Dichloroethane 4640 1,1-Dichloroethylene 5155 1,2,4-Trichlorobenzene 5210 1,2,4-Trimethylbenzene 4570 1,2-Dibromo-3-chloropropane (DBCP) 4585 1,2-Dibromoethane (EDB, Ethylene dibromide) 4695 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon-114) 4610 1,2-Dichlorobenzene 4635 1,2-Dichloroethane (Ethylene dichloride) 4655 1,2-Dichloropropane 5215 1,3,5-Trimethylbenzene 9318 1,3-Butadiene 4615 1,3-Dichlorobenzene 4620 1,4-Dichlorobenzene 4735 1,4-Dioxane (1,4- Diethyleneoxide) 5220 2,2,4-Trimethylpentane 4410 2-Butanone (Methyl ethyl ketone, MEK) 4860 2-Hexanone (MBK) 4995 4-Methyl-2-pentanone (MIBK) 4315 Acetone 4320 Acetonitrile 4375 Benzene 4395 Bromodichloromethane 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 5 of 7

OREGON Environmental Laboratory Program EPA TO-17 4475 Chlorobenzene 4575 Chlorodibromomethane 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4555 Cyclohexane 4625 Dichlorodifluoromethane (Freon-12) 4750 Ethanol 4765 Ethylbenzene 4835 Hexachlorobutadiene 4895 Isopropyl alcohol (2-Propanol, Isopropanol) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4960 Methyl chloride (Chloromethane) 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5005 Naphthalene 4825 n-heptane 4855 n-hexane 5027 n-octane 5250 o-xylene 5100 Styrene 5115 Tetrachloroethylene (Perchloroethylene) 5120 Tetrahydrofuran (THF) 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5235 Vinyl chloride 5260 Xylene (total) EPA TO-4A 10249204 Pesticides and PCBs by HV PUF GC 7355 4,4'-DDD 7360 4,4'-DDE 7365 4,4'-DDT 7025 Aldrin 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 7240 alpha-chlordane 8880 Aroclor-1016 (PCB-1016) 8910 Aroclor-1260 (PCB-1260) 6 of 7

EPA TO-4A 7115 beta-bhc (beta- Hexachlorocyclohexane) 7105 delta-bhc 7470 Dieldrin 7510 Endosulfan I 7515 Endosulfan II 7520 Endosulfan sulfate 7540 Endrin 7530 Endrin aldehyde 7535 Endrin ketone 7120 gamma-bhc (Lindane, gamma- HexachlorocyclohexanE) 7245 gamma-chlordane 7685 Heptachlor 7690 Heptachlor epoxide 7810 Methoxychlor MADEP APH 90017188 -Phase Petroleum Hydrocarbons 9318 1,3-Butadiene 3792 APH Aliphatics C5-C8 3793 APH Aliphatics C9-C12 3794 APH Aromatics C9-C10 4375 Benzene 4765 Ethylbenzene 5240 m+p-xylene 5000 Methyl tert-butyl ether (MTBE) 5005 Naphthalene 5250 o-xylene Non- Potable Water EPA RSK-175 (GC-FID) EPA RSK-175 (GC-TCD) 5140 Toluene 4747 Ethane 4752 Ethene 4926 Methane 3755 Carbon dioxide 10212905 Methane, Ethane, and Ethene in water by Headspace GC/FID 10212858 Fixed Gases in water by Headspace GC/TCD 7 of 7