Test Report No. : CE/2007/C7382B Date : 2008/06/18 Page : 1 of 5 The following sample(s) was/were submitted and identified by/on behalf of the client as : Sample Description : Style/Item No. : Manufacturer : Sample Receiving Date : Testing Period : HEAT SHRINKABLE POLYOLEFIN (HALOGEN FREE) TUBING PRINTING INK (WHITE) RP* ZHEJIANG NEW EAST PRINTING INK GROUP CO., LTD. 2007/12/27 AND 2008/6/10 2007/12/27 TO 2008/01/04 AND 2008/06/10 TO 2008/06/17 ==================================================================================== Test Requested : In accordance with the RoHS Directive 2002/95/EC, and its amendment directives. Test Method : (1) (2) (3) (4) (5) 8. Determination of Cadmium by ICP-AES. 8. Determination of Lead by ICP-AES. 7. Determination of Mercury by ICP-AES. With reference to IEC 62321/2nd CDV (111/95/CDV) - Annex C. Determination of Hexavalent Chromium for non-metallic samples by UV/Vis Spectrometry. With reference to IEC 62321/2nd CDV (111/95/CDV) - Annex A. Determination of PBB and PBDE by GC/MS. Test Result(s) : Please refer to next page(s). * This report is added testing and combined with CE/2007/C7382 *
Test Report No. : CE/2007/C7382B Date : 2008/06/18 Page : 2 of 5 Test results by chemical method (Unit: mg/kg) Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) by alkaline extraction Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Test Item (s): Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs (Mono to Nona) Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether Sum of PBDEs (Mono to Deca) TEST PART DESCRIPTION: NO.1 : WHITE INK Note: 1. mg/kg = ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. "-" = Not Regulated Method (Refer to) (1) (2) (3) (4) (5) Result No.1 MDL
Test Report No. : CE/2007/C7382B Date : 2008/06/18 Page : 3 of 5 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr 6+ test method excluded) 2) Name of the person who made measurement: Climbgreat Yang 3) Name of the person in charge of measurement: Troy Chang Cutting / Preparation Sample Measurement Pb Cd Acid digestion by suitable acid depended on different sample material (as below table) Hg Microwave digestion with HNO 3 /HCl/HF Cr 6+ Add appropriate amount of digestion reagent Filtration Heat to appropriate temperature to extract Solution ICP-AES Residue 1) Alkali Fusion 2) HCl to dissolve Cool, filter digestate through filter Add diphenyl-carbazide for color development Sample Material Digestion Acid Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2 O 2 Glass HNO 3 /HF Gold, platinum, palladium, ceramic Aqua regia measure the absorbance at 540 nm by UV-VIS Silver HNO 3 Plastic Others H 2 SO 4, H 2 O 2, HNO 3, HCl Any acid to total digestion
Test Report No. : CE/2007/C7382B Date : 2008/06/18 Page : 4 of 5 PBB/PBDE analytical FLOW CHART 1) Name of the person who made measurement: Roman Wong 2) Name of the person in charge of measurement: Shinjyh Chen First testing process Optional screen process Confirmation process Sample Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report
Test Report No. : CE/2007/C7382B Date : 2008/06/18 Page : 5 of 5 ** End of Report **