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Available online at www.sciencedirect.com ScienceDirect Energy Procedia 59 (2014 ) 366 373 European Geosciences Union General Assembly 2014, EGU 2014 Laboratory measurements of fluid transport properties on tight gas sandstones and applications Daniel Albrecht *, Viktor Reitenbach Institute for Petroleum Engineering, Clausthal University of Technology, Agricolastr. 10, 38678 Clausthal-Zellefeld, Germany Abstract Deep gas reservoirs are of great interest for the E&P industry. Large areas of such reservoirs have permeabilities below 1 md. The reservoir rocks in these areas show a strong stress sensitivity of the fluid transport properties and a considerable productivity decline due to changing stress conditions during the production process. For correct modeling and simulation of Tight Gas reservoirs it is important to know the behavior of the fluid transport properties under the changing stress condition the reservoir experiences. In several measurement series the effects of changing overburden and pore pressure on Rotliegend sandstone samples from north German Tight Gas reservoirs have been quantified and used to set up correlation functions. With the correlation functions from the own measurements and additional data and correlations from literature a Rock Data Catalog has been developed as tool to help reservoir engineers with modeling and simulation of such reservoirs. The Rock Data Catalog consists of the Rock Database and the Correlation Module. The Rock Database contains general and petrophysical rock data. The Correlation Module uses this data to generate secondary data of e.g. in-situ capillary and hydraulic rock properties with appropriate correlation functions. Viability of the economic gas production from Tight Gas Reservoirs strongly depends on reservoir quality. Therefore identification of high quality reservoir parts or so called Sweet Spots for placing production wells and planning hydraulic fracturing stimulation, is one of key issues of the tight gas reservoir characterization and evaluation. The data and correlation functions collected in the Rock Data Catalog could also be used to identify Sweet Spots in Tight Gas reservoirs. Several rock parameters and properties, which affect the fluid flow in a reservoir (like lithology, clay content, water saturation, permeability, pore size distribution) can be identified and used to set up a Sweet Spot Index as a measure for the reservoir quality. 2014 2014The The Authors. Authors. Published Published by Elsevier by Elsevier Ltd. Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/3.0/). Peer-review under responsibility of the Austrian Academy of Sciences. Peer-review under responsibility of the Austrian Academy of Sciences Keywords: Tight gas; Rock Data Catalog; Sweet spots * Corresponding author. E-mail address: daniel.albrecht@tu-clausthal.de 1876-6102 2014 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/3.0/). Peer-review under responsibility of the Austrian Academy of Sciences doi:10.1016/j.egypro.2014.10.390

Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 367 1. Introduction Tight gas reservoirs represent an important part of the world gas resources and are therefore of high interest for the petroleum industry. Such reservoirs are characterized by low permeabilities. Fluid flow properties show a great variability and are affected by several properties like mineral content, residual water saturation, stress conditions. Petrophysical measurements in laboratory normally do not take these factors into account. Therefore, modeling and simulation of Tight Gas reservoirs based on petrophysical data measured on rock samples under standard laboratory pressure and temperature conditions is often inaccurate. For better results the relevant petrophysical parameters measured in laboratory have to be converted to reservoir conditions. This can be done by using suitable correlation functions which fit the reservoir rock type. The rock type can be defined by lithology and mineral content of the rock. A specialized Rock Data Base, which contains petrophysical rock data and other information, e.g. about the rock type, from tight gas reservoirs and correlation functions can be a useful tool to support modeling and simulation of such reservoirs. A Rock Data Base for tight gas could also be used to identify sweet spots. 2. Factors affecting fluid transport properties of Tight Gas rocks The fluid flow properties of Tight Gas rocks are affected by several factors, i.e. mineral content (especially clay contents), saturation state and stress conditions. Authigenic cement minerals are known to have a negative effect on the fluid flow properties. Illites with fibrous habits have the most detrimental effect on reservoir permeability, often causing tight reservoirs [2]. The lithology and mineral content can be used for the rock typing, which is necessary to choose appropriate correlation functions for the modeling and/or simulation. Fig. 1 shows the permeabilities and immobile water saturations for different rock types. The factors mineral content, immobile water saturation and permeability are i.a. also important to identify so called Sweet Spots in a tight reservoir. Fig. 1. Rotliegend sandstone rock types [1]. 3. Correlation functions for Tight Gas rocks In an experimental study several measurements have been performed on samples from North-German Rotliegend tight gas rock samples. In these measurements the influence of stress, pore pressure and loading patterns on permeability has been quantified. Additional measurements have been performed to get capillary pressure data, threshold pressures and other parameters, which are important for reservoir modeling and simulation. From the

368 Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 results of these measurements correlation functions have been derived, which describe the change of permeability in a tight gas reservoir arising from the production induced increase of effective stress and which enable to calculate in-situ permeabilities from laboratory measured data (see Fig. 2). The curve marked by blue dots was measured on a plug, which had been reconsolidated by applying isostatic pressure of 500 bar on the sample before starting the permeability measurements. In this way micro-fissures caused by the core extraction, plug drilling and a long storage time were closed. The curve marked by orange dots was in contrast measured on a plug which was not reconsolidated. In this case micro-fissures close during the measurement when higher stresses are applied on the plug, resulting in a much stronger stress dependency of the measured permeability. The blue framed function in this figure was derived from permeability measurements on reconsolidated plugs and represents the permeability decline in a reservoir at increasing effective stress. k is hereby the permeability at an effective stress eff and k a the permeability measured at laboratory (ambient) conditions. The orange framed function was derived from permeability measurements on not-reconsolidated plugs and can be used to calculate permeabilities at reservoir stress conditions from permeabilities measured at ambient conditions. Fig. 2. Correlation functions for permeability [3]. Fig. 3to Fig. 6 show correlation functions for porosity-permeablity, permeability-irreducible water saturation (S wi ), permeability-threshold pressure and Leverett functions for Rotliegend sandstone rock types plugs.

Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 369 Fig. 3.Poro-Perm correlation for Rotliegend sandstone rock type [3]. Fig. 4. Swi-Perm correlation for Rotliegend sandstone rock types [4].

370 Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 Fig. 5. Threshold pressure and Leverett function for Rotliegend sandstone rock types [4]. 4. The Rock Data Catalog Fig. 6. Leverett function for Rotliegend sandstone rock types [4]. The Rock Data Catalog (RDC) was developed as tool to support modeling and simulation of Tight Gas reservoirs. The Rock Data Catalog contains three parts: Rock Database Query Builder Correlation Module

Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 371 The Rock Database contains petrophysical data from own measurements and open sources (i.e. porosity data, permeability data, capillary pressure functions), log data and meta data (i.e. general data about the fields and wells within a field). The objects (Field, Borehole, Core, Plug) are hierarchically structured, successive objects are unambiguously assigned to a superior object. The data is assigned to a certain object. The Query Builder is a tool to search for and select data from the Rock Database. The selected data can then be transferred to the Correlation Module for further processing. The Correlation Module enables to use correlation functions to generate from the original data secondary data sets. For example laboratory measured permeability data from the Rock Database can be used to calculate in-situ permeabilities for a reservoir under given stress conditions. The secondary data sets can further on be used for reservoir modeling or simulation in other software programs like Eclipse or Petrel. Fig. 7shows a sample screenshot of the Rock Data Catalog and Fig. 8 the options available in the Correlation Module. Fig. 7. Screenshot of the Rock Data Catalog.

372 Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 Fig. 8. Flow chart of the correlation options [3]. The RDC contains different correlation functions with validity for different types of rock and poro-perm ranges. To get good results the validity of a correlation function for the rock type of the considered reservoir has to be checked. This can be done using the Quality Check option of the Correlation Module. 4. Sweet Spot Identification Sweet Spots are areas of better petrophysical properties (e.g. permeability) and therefore enhanced productivity and deliverability [5].Naides [6] suggested a method to determine Sweet Spots from well log data. This method could be adapted and integrated in the Rock Data Catalog to use petrophysical data measured on plugs for Sweet Spot identification. Key parameters are i.a. lithology, diagenesis and clay content, porosity, absolute permeability k, end-point effective gas permeability k rgswi, connate water saturation S wi, displacement threshold pressure p d and pore size distribution. From these parameters a footprint can be generated for each well or depth interval of a well (see Fig. 9). Fig. 9. Footprint of a wellsection [7].

Daniel Albrecht and Viktor Reitenbach / Energy Procedia 59 ( 2014 ) 366 373 373 With this information a Sweet Spot Index (SSI) can be calculated for each well or depth interval of a well (see equation 1) according to the concept of Naides [6]. Here p 1, p 2, etc. are the parameters (like porosity, permeability, etc.). w 1, w 2, etc. are weighting factors for each parameter, which represent the influence of the parameter on the well performance. SSI p w p w p w w w w... 1 1 2 2 3 3... 1 2 3 (1) The Sweet Spot Index can help making decisions on improvements in well completions or to find preferable spots for stimulation treatments i.e. fracturing. 5. Conclusion Petrophysical differences of sandstones from deep burial tight gas reservoirs are related to lithofacies types. The permeabilities of such reservoirs is extremely stress dependent. Deviatoric stress conditions and loading patterns are crucial for the results of stress dependent permeability analysis. From laboratory measurements correlation functions of fluid transport properties could be derived, which provide an important base for lithotype related reservoir characterization and simulation studies. Properties measured under laboratory conditions have to be converted to insitu conditions using proper correlation functions to get appropriate results in modeling and simulation. Hereby a specialized Rock Data Catalog can be a useful tool to support the reservoir engineering analyses. An interactive computerized Rock Data Catalog developed at the Institute of Petroleum Engineering is based on the rock type- and stress-related correlation of the fluid transport properties of tight gas sandstones. It can be adopted for a wide range of applications as for example evaluation of relevant fluid transport properties for numerical reservoir modeling and simulation up to identification of sweet spots in tight gas reservoirs. References [1] Reitenbach V, Pusch G, Mizine A. Investigation on Water/CO 2 Mobilities in Lower Rhyolite and the Adjacent Bishop Tuff of the Long Valley Caldera by Means of Hydraulic and Low Frequency Nuclear Magnetic Resonance (NMR) Measurements. Final Research Report DFG PU 59/11-4, Clausthal-Zellerfeld; Mai 2004: 43 S. [2] Gaupp R, Okkerman JA. Diagenesis and Reservoir Quality of Rotliegend Sandstones in the Northern Netherlands A Review.SEPM No. 98; 2011. p. 193-226 [3] Reitenbach V, Albrecht D. Erarbeitung eines Rock Data Katalogs für Gasformationen Development of a Rock Data Catalog for Gas Formations. DGMK Research Report 593-9/4-3, DGMK, Hamburg; 2010. [4] Reitenbach V, Möller M. Erarbeitung eines computergestützten Rock Data Katalogs für Gasformationen - Development of a Computer Aided Rock Data Catalog of Gas Formations. DGMK Research Report 593-9/4, DGMK, Hamburg; 2006. [5] Urban LM. Determination of Indicators for Sweet Spots in Tight Gas Reservoirs from Core Data. Bc.-Thesis, Clausthal; 2012. [6] Naides C. Petrophysical Analysis Method to Identify Sweet Spots in Tight Reservoirs: Case Study from Punta Rosada Formation in Neuquen Basin, Argentina. SPE 121313; 2010. [7] Ganzer et.al. Sweet Spot Definition and Parametrization in Tight Gas Reservoirs Using Engineering Core Analysis. itf Project Review Meeting, Aberdeen; 3-4 February 2011.