Page1of8 Thefolowingsample(s)was/weresubmittedandidentifiedby/onbehalfoftheapplicantas Sam plesubm ittedb y Sam pledescription Style/Item N o. Sam plereceivingdate TestingPeriod M OL D COM POUN D K L G200 2015/01/15 2015/01/15 T O 2015/01/21 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = TestRequested (1) As specifiedbyclient,withreferencetoroh S Directive2011/65/EU AnnexIItodeterm inecadm ium,l ead, M ercury,cr(v I),PB B s,pb DEs contents in thesubm ittedsam ple. (2) As specifiedbyclient,withreferencetog/tb T/N /EU/256ofW TO/TB T totestdb P,B B P,DEH P,DIB P. (3) Pleaserefertonextpages fortheotheritem (s). TestR esu lt(s) Pleaserefertonextpage(s).
Page2of8 TestR esu lt(s) PART N AM E N o.1 B L ACK GRAIN Cadm ium (Cd) L ead(pb) M ercury(h g) TestItem(s) H exavalentchrom ium Cr(V I) H exabrom ocyclododecane (H B CDD)andallm ajor dias tereois om ers identified (α- H B CDD, β- H B CDD, γ- H B CDD) (CAS N o.25637-99-4and3194-55-6(134237-51-7,134237-50-6, 134237-52-8)) DIB P (Di-isobutylphthalate)(CAS N o.84-69-5) DB P (Dibutylphthalate)(CAS N o. 84-74-2) B B P (B utylb enzylphthalate)(cas N o.85-68-7) DEH P (Di-(2-ethylhexyl) phthalate)(cas N o.117-81-7) DN OP (Di-n-octylphthalate)(CAS N o.117-84-0) DIN P (Di-isononylphthalate)(CAS N o.28553-12-0;68515-48-0) DIDP (Di-isodecylphthalate)(CAS N o.26761-40-0;68515-49-1) Unit M ethod m g/kg W ithreferencetoiec 62321-52013 andperform edbyicp-aes. m g/kg W ithreferencetoiec 62321-52013 andperform edbyicp-aes. m g/kg W ithreferencetoiec 62321-42013 andperform edbyicp-aes. m g/kg W ithreferencetoiec 623212008and perform edbyuv -V IS. m g/kg W ithreferencetoiec 623212008 m ethod.analysis was perform edby GC/M S. Result M DL N o.1 2 n.d. 2 n.d. 2 n.d. 2 n.d. 5 n.d. m g/kg W ithreferencetoiec 62321-8 (111/321/CD).Analysis was perform ed 50 n.d. m g/kg bygc/m S. 50 n.d.
Page3of8 TestItem(s) Unit M ethod M DL Result N o.1 Sum ofpbbs m g/kg - n.d. M onobrom obiphenyl D ibrom obiphenyl T ribrom obiphenyl T etrabrom obiphenyl P entabrom obiphenyl H exabrom obiphenyl H eptabrom obiphenyl Octabrom obiphenyl N onabrom obiphenyl D ecabrom obiphenyl Sum ofpbdes M onobrom odiphenylether D ibrom odiphenylether T ribrom odiphenylether T etrabrom odiphenylether P entabrom odiphenylether H exabrom odiphenylether H eptabrom odiphenylether Octabrom odiphenylether N onabrom odiphenylether D ecabrom odiphenylether m g/kg W ithreferencetoiec 623212008and 5 n.d. m g/kg perform edbygc/m S. - n.d. N ote 1. m g/kg= ppm ;0.1wt% = 1000ppm 2. n.d.= N ot D etected 3. M DL = M ethoddetection L im it 4. "-"= N otregulated
Page4of8 #FLO W 1) T hesesamples weredissolvedtotalybypre-conditioningm ethodaccordingtobelow flow chart. (Cr 6+ testmethodexclu ded) 2) N ameoftheperson whomademeasurem entclim bgreatyang 3) N ameoftheperson in chargeofm easurem enttroychang C u tting/preparation SampleM easurement Pb Cd Aciddigestion bysu itableacid dependedon diferentsample m aterial(as below table) H g M icrowavedigestion with H N O 3 /H Cl/H F Cr 6+ (N ote**) Addappropriateamount ofdiges tion reagent Filtration Solution ICP-AES Sam plem aterial Residu e 1) AlkaliFusion 2) H Cltodissolve D iges tion Acid H eat to appropriate tem peraturetoextract C ool,filterdiges tate throu gh filter Add diphenyl-carbazide forcolordev elopm ent Steel,copper,alum inum,solder Aquaregia,H N O 3,H Cl,H F,H 2 O 2 Glass H N O 3 /H F Gold,platinum,paladium,ceramic Aquaregia Silver H N O 3 Plastic Others H 2 SO 4,H 2 O 2,H N O 3,H Cl A dded appropriatereagent to total diges tion measuretheabsorbance at540nm byuv -V IS N ote**(foriec 62321) (1)Fornon-m eta licm aterial,add alkaline diges tion reagent and heat to 90~95. (2)Form eta licm aterial,add pu re w aterand heat to boiling.
Page5of8 PBB/PBDEanalyticalFLO W CH A RT N am eoftheperson whom adem easurementrom an W ong N am eoftheperson in chargeofmeasurem entt roychang Firsttestingprocess Optionals creen proces s Confirmation process Sam ple Sam plepretreatm ent Screen analys is Sam pleextraction/ Soxhletm ethod C oncentrate/d ilu te Extractedsolution Filter Analysis bygc/m S IssueReport
Page6of8 A nalyticalflow chartofp hthalate content N ameoftheperson whomademeasurementandyshu N ameoftheperson in chargeofm easurementtroychang Testm ethodiec 62321-8 Sam plepretreatm ent/s eparation Sam pledissolved/extractedbyth F DiluteExtractedsolution Analysis was perform edbygc/m S Data
Page7of8 #PIC H BCDD analyticalflow chart N am eoftheperson whomademeasurementroman W ong N am eoftheperson in chargeofm easurem enttroychang Samplepretreatm ent Sam ple extraction /U ltras onicm ethod Concentrate/DiluteExtractedsolution Filter Analysis was performedbygc/m S Data
Page8of8 *Thetestedsample/partismarkedbyanarrow ifit'sshownonthephoto.* **EndofReport **