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Phone/ (86)88-4800 / (86)88-471 http://www.emsl.com to1lab@emsl.com Customer ID: EMSL0A K12312.D 28 cc 0 0/01/2017 K12327.D 21 cc 600 Target Compound Results Summary Propylene 11-07-1 42.08 ND.0 ND 8.6 Freon 12(Dichlorodifluoromethane) 7-71-8 120.9 ND 2. ND 12 Freon 114(1,2-Dichlorotetrafluoroethan 76-14-2 170.9 ND 2. ND 17 Chloromethane 74-87-3 0.49 ND 2. ND.2 n-butane 106-97-8 8.12 24 2. 6.9 Vinyl chloride 7-01-4 62.0 ND 2. ND 6.4 1,3-Butadiene 106-99-0 4.09 ND 2. ND. Bromomethane 74-83-9 94.94 ND 2. ND 10 Chloroethane 7-00-3 64.2 ND 2. ND 6.6 Ethanol 64-17- 46.07 400 2 D 760 47 Reported Dilution #1 Bromoethene(Vinyl bromide) 93-60-2 106.9 ND 2. ND 11 Freon 11(Trichlorofluoromethane) 7-69-4 137.4 ND 2. ND 14 Isopropyl alcohol(2-propanol) 67-63-0 60.10 49 2. 120 6.1 Freon 113(1,1,2-Trichlorotrifluoroethan 76-13-1 187.4 ND 2. ND 19 Acetone 67-64-1 8.08 21000 300 D 49000 710 Reported Dilution #2 1,1-Dichloroethene 7-3-4 96.94 ND 2. ND 10 Acetonitrile 7-0-8 41.00 ND 2. ND 4.2 Tertiary butyl alcohol(tba) 7-6-0 74.12 ND 2. ND 7.6 Bromoethane(Ethyl bromide) 74-96-4 108.0 ND 2. ND 11 3-Chloropropene(Allyl chloride) 107-0-1 76.3 ND 2. ND 7.8 Carbon disulfide 7-1-0 76.14 ND 2. ND 7.8 Methylene chloride 7-09-2 84.94 ND 2. ND 8.7 Acrylonitrile 107-13-1 3.00 ND 2. ND.4 Methyl-tert-butyl ether(mtbe) 1634-04-4 88.1 ND 2. ND 9.0 trans-1,2-dichloroethene 16-60- 96.94 ND 2. ND 10 n-hexane 110-4-3 86.17 27 2. 94 8.8 1,1-Dichloroethane 7-34-3 98.96 ND 2. ND 10 Vinyl acetate 108-0-4 86.00 ND 2. ND 8.8 2-Butanone(MEK) 78-93-3 72.10 4.4 2. 13 7.4 cis-1,2-dichloroethene 16-9-2 96.94 ND 2. ND 10 Ethyl acetate 141-78-6 88.10 3 2. 130 9.0 Chloroform 67-66-3 119.4 ND 2. ND 12 Tetrahydrofuran 109-99-9 72.11 ND 2. ND 7.4 1,1,1-Trichloroethane 71--6 133.4 ND 2. ND 14 Cyclohexane 110-82-7 84.16 ND 2. ND 8.6 2,2,4-Trimethylpentane(Isooctane) 40-84-1 114.2 ND 2. ND 12 Carbon tetrachloride 6-23- 13.8 ND 2. ND 16 n-heptane 142-82- 100.2 7.4 2. 30 10 1,2-Dichloroethane 107-06-2 98.96 ND 2. ND 10 Benzene 71-43-2 78.11 ND 2. ND 8.0 Trichloroethene 79-01-6 131.4 29 2. 10 13 1,2-Dichloropropane 78-87- 113.0 ND 2. ND 12 Methyl Methacrylate 80-62-6 100.12 11 2. 4 10 Bromodichloromethane 7-27-4 163.8 ND 2. ND 17 1,4-Dioxane 123-91-1 88.12 ND 2. ND 9.0 4-Methyl-2-pentanone(MIBK) 108-10-1 100.2 ND 2. ND 10 TO1_Master_Reports_Feb_2018_V1011 V101 Page 1 of 11

Phone/ (86)88-4800 / (86)88-471 http://www.emsl.com to1lab@emsl.com Customer ID: EMSL0A K12312.D 28 cc 0 0/01/2017 K12327.D 21 cc 600 Target Compound Results Summary cis-1,3-dichloropropene 10061-01- 111.0 ND 2. ND 11 Toluene 108-88-3 92.14 2 2. 100 9.4 trans-1,3-dichloropropene 10061-02-6 111.0 ND 2. ND 11 1,1,2-Trichloroethane 79-00- 133.4 ND 2. ND 14 2-Hexanone(MBK) 91-78-6 100.1 ND 2. ND 10 Tetrachloroethene 127-18-4 16.8 ND 2. ND 17 Dibromochloromethane 124-48-1 208.3 ND 2. ND 21 1,2-Dibromoethane 106-93-4 187.8 ND 2. ND 19 Chlorobenzene 108-90-7 112.6 68 2. 310 12 Ethylbenzene 100-41-4 106.2 110 2. 460 11 Xylene (p,m) 1330-20-7 106.2 440 0 D 1900 220 Reported Dilution #1 Xylene (Ortho) 9-47-6 106.2 170 2. 70 11 Styrene 100-42- 104.1 ND 2. ND 11 Isopropylbenzene (cumene) 98-82-8 120.19 23 2. 120 12 Bromoform 7-2-2 22.8 ND 2. ND 26 1,1,2,2-Tetrachloroethane 79-34- 167.9 ND 2. ND 17 4-Ethyltoluene 622-96-8 120.2 460 2 D 2200 120 Reported Dilution #1 1,3,-Trimethylbenzene 108-67-8 120.2 170 2. 820 12 2-Chlorotoluene 9-49-8 126.6 ND 2. ND 13 1,2,4-Trimethylbenzene 9-63-6 120.2 00 2 D 200 120 Reported Dilution #1 1,3-Dichlorobenzene 41-73-1 147.0 ND 2. ND 1 1,4-Dichlorobenzene 106-46-7 147.0 ND 2. ND 1 Benzyl chloride 100-44-7 126.0 ND 2. ND 13 1,2-Dichlorobenzene 9-0-1 147.0 ND 2. ND 1 1,2,4-Trichlorobenzene 120-82-1 181. ND 2. ND 19 Hexachloro-1,3-butadiene 87-68-3 260.8 ND 2. ND 27 Naphthalene 91-20-3 128.17 9.0 2. 47 13 Total Target Compound Concentrations: 24000 ppbv 60000 ug/m3 Surrogate Result Spike Recovery 4-Bromofluorobenzene 11 10 110% ND = Non Detect E= Estimated concentration exceeding upper calibration range. D= Result reported from diluted analysis. Method Reference r USEPA: Compendium Method TO-1, Determination of Volatile Organic Compounds (VOCs) in Air " Collected in Specially-Prepared Canisters and Analyzed by Gas Chromatography/Mass Spectrometry (GC/MS), January 1999, (EPA/62/R-96/010b). TO1_Master_Reports_Feb_2018_V1011 V101 Page 2 of 11

Phone/ (86)88-4800 / (86)88-471 http://www.emsl.com to1lab@emsl.com Customer ID: EMSL0A K12312.D 28 cc 0 0/01/2017 K12327.D 21 cc 600 Tentatively Identified Compound Results Summary Result Result Retention Tentatively Identified Compounds CAS# MW(1) ppbv Q ug/m3 Time Comments Cyclohexanone 000108-94-1 98 87 JN 30 26.11 Benzene, propyl- 000103-6-1 120 110 JN 30 26.66 Unknown Substituted Benzene 92 160 JN 80 27.39 D-Limonene 00989-27- 136 100 JN 70 28.01 Benzene, 1,2,3-trimethyl- 00026-73-8 120 140 JN 690 28.46 Unknown Substituted Benzene 92 10 JN 0 28.69 Unknown Substituted Benzene 92 190 JN 730 28.81 Indane 000496-11-7 118 2 JN 20 29.0 Unknown Substituted Benzene 92 68 JN 260 29.17 Unknown Substituted Benzene 92 89 JN 340 29.31 Unknown Substituted Benzene 92 77 JN 290 29.39 Unknown Substituted Benzene 92 120 JN 40 29.3 Unknown Substituted Benzene 92 42 JN 160 30.1 Unknown Substituted Benzene 92 3 JN 200 30.20 Unknown Substituted Benzene 92 110 JN 410 30.33 Unknown Substituted Benzene 92 40 JN 10 31.38 Total TIC Concentrations: 1600 ppbv 600 ug/m3 (1) = If unknown, MW is assigned as equivalent Toluene (92) for ug/m3 conversion purposes. J= Estimated value based on a 1:1 response to internal standard. N= Presumptive evidence of compound based on library match. Method Reference USEPA: Compendium Method TO-1, Determination of Volatile Organic Compounds (VOCs) in Air " Collected in Specially-Prepared Canisters and Analyzed by Gas Chromatography/Mass Spectrometry (GC/MS), January 1999, (EPA/62/R-96/010b). TO1_Master_Reports_Feb_2018_V1011 V101 Page 3 of 11

Phone/ (86)88-4800 / (86)88-471 http://www.emsl.com to1lab@emsl.com Customer ID: EMSL0A K12312.D 28 cc 0 0/01/2017 K12327.D 21 cc 600 Total Volatile Organic Compounds (TVOC) Summary n-butane 106-97-8 8.12 24 2. 6.9 Ethanol 64-17- 46.07 400 2 D 760 47 Reported Dilution #1 Isopropyl alcohol(2-propanol) 67-63-0 60.10 49 2. 120 6.1 Acetone 67-64-1 8.08 21000 300 D 49000 710 Reported Dilution #2 n-hexane 110-4-3 86.17 27 2. 94 8.8 2-Butanone(MEK) 78-93-3 72.10 4.4 2. 13 7.4 Ethyl acetate 141-78-6 88.10 3 2. 130 9.0 n-heptane 142-82- 100.20 7.4 2. 30 10 Trichloroethene 79-01-6 131.40 29 2. 10 13 Methyl Methacrylate 80-62-6 100.1 11 2. 4 10 Toluene 108-88-3 92.14 2 2. 100 9.4 Chlorobenzene 108-90-7 112.60 68 2. 310 12 Ethylbenzene 100-41-4 106.20 110 2. 460 11 Xylene (p,m) 1330-20-7 106.20 440 0 D 1900 220 Reported Dilution #1 Xylene (Ortho) 9-47-6 106.20 170 2. 70 11 Isopropylbenzene (cumene) 98-82-8 120.19 23 2. 120 12 4-Ethyltoluene 622-96-8 120.2 460 2 D 2200 120 Reported Dilution #1 1,3,-Trimethylbenzene 108-67-8 120.2 170 2. 820 12 1,2,4-Trimethylbenzene 9-63-6 120.20 00 2 D 200 120 Reported Dilution #1 Naphthalene 91-20-3 128.17 9.0 2. 47 13 Total Target Compound Concentrations: 24000 ppbv 60000 ug/m3 E= Estimated concentration exceeding upper calibration range. D= Result reported from diluted analysis. Result Result Retention Tentatively Identified Compounds CAS# MW(1) ppbv Q ug/m3 Time Comments Cyclohexanone 000108-94-1 98 87 JN 30 26.11 Benzene, propyl- 000103-6-1 120 110 JN 30 26.66 Unknown Substituted Benzene 92 160 JN 80 27.39 D-Limonene 00989-27- 136 100 JN 70 28.01 Benzene, 1,2,3-trimethyl- 00026-73-8 120 140 JN 690 28.46 Unknown Substituted Benzene 92 10 JN 0 28.69 Unknown Substituted Benzene 92 190 JN 730 28.81 Indane 000496-11-7 118 2 JN 20 29.0 Unknown Substituted Benzene 92 68 JN 260 29.17 Unknown Substituted Benzene 92 89 JN 340 29.31 Unknown Substituted Benzene 92 77 JN 290 29.39 Unknown Substituted Benzene 92 120 JN 40 29.3 Unknown Substituted Benzene 92 42 JN 160 30.1 Unknown Substituted Benzene 92 3 JN 200 30.2 Unknown Substituted Benzene 92 110 JN 410 30.33 TO1_Master_Reports_Feb_2018_V1011 V101 Page 4 of 11

Phone/ (86)88-4800 / (86)88-471 http://www.emsl.com to1lab@emsl.com Customer ID: EMSL0A K12312.D 28 cc 0 0/01/2017 K12327.D 21 cc 600 Total Volatile Organic Compounds (TVOC) Summary Unknown Substituted Benzene 92 40 JN 10 31.38 Total TIC Concentrations: 1600 ppbv 600 ug/m3 (1) = If unknown, MW is assigned as equivalent Toluene (92) for ug/m3 conversion purposes. J= Estimated value based on a 1:1 response to internal standard. N= Presumptive evidence of compound based on library match. Total Volatile Organic Compounds (TVOCs): 26000 ppbv 67000 ug/m3 TO1_Master_Reports_Feb_2018_V1011 V101 Page of 11

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