Charging of the test masses past, present and future. R. Weiss LIGO Systems Mee=ng September 23, 2014

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Charging of the test masses past, present and future R. Weiss LIGO Systems Mee=ng September 23, 2014

Past to present Find rela=on between electrosta=c force on test mass and voltage applied to gold traces to be variable and not the expected value. F = α(v bias V control ) 2 + β(v bias V control ) Test for β devised using op=cal levers to measure pitch and yaw excita=on ini=ally noisy and confusing measurements further confusion from mislabeled and bad wiring indica=ons of charge from longitudinal measurements using the full interferometer with care pitch and yaw became reliable now show fluctua=ng charge density

Past to present 2 Full interferometer tests ini=al opera=on of electrosta=c drive exhibited excess displacement noise traced to D/A glitches and noise in driver low pass bias filter reduced noise significantly, low pass control filter reduced noise a liqle elimina=ng the electrosta=c drive en=rely (by using magnets on the penul=mate mass) reduced noise a liqle also but disappoin=ngly liqle remaining noise in the 40 to 100 Hz band exhibits 1/f 3 spectrum and varies linearly with bias voltage for bias greater than 200V but remains constant for smaller bias voltages consistent with fluctua=ng charge density on the mirror (LIGO T960137) interac=ng with surroundings Need to eliminate charge on the mirror

Past to present 3 External injec=on ionizer applied at LHO ETMY (LIGO- T1100332,LIGO- G1100364,LIGO- T1400535) Reduced charge from 0.4 to 0.01 depending on quadrant. Need to beqer understand opera=ng condi=ons injec=on =mes, flow rates and pressures to op=mize performance. Injec=on used 1 hour, recovery to prior pressure required 12 hours (could be faster) Charge recovered to pre injec=on values in about 36 hours, 3 hours aber ion pump was open to chamber. Ionizer requires more development: improved flow measurement, beqer equality of + and - ions (described later)

Ionizer at LHO

# Figure!5#The#discharge#gauge#measured#chamber#pressure#before#and#after#the#two# injections.#in#the#trace#before#the#first#injection#the#chamber#is#maintained#by#its#ion# pump.#the#ion#pump#is#closed#off#from#the#system#before#the#first#injection#and# turned#on#again#at#the#downward#step#after#the#second#injection.#the#pump#out#is# with#a#turbo#pump.## # # Chamber pressure N 2 vs =me # Figure!4#Pirani#gauge#on#the#test#mass#chamber#showing#pressure#profile#during#the# injection#and#subsequent#rough#pumping#for#both#test1#and#test#2.#

Past to present 4 Ionizer test at MIT showed LIGO test mass charge as small (had to induce charging). What is different? No use of First Contact: leaves glass nega=vely charged neutraliza=on methods were inadequate leaving charge densi=es 10-11 to 10-12 coulombs/cm 2 Now improved by ~1/100 No green light Possibility of 2 quantum photoemission with SiO 2 work func=on of 4 volts. Unlikely, though requires only a quantum efficiency of 10-13. Current test not adequate to reject hypothesis. No ion pumps (the most significant difference) Experience at MIT, Princeton, JILA, Glasgow in other precision experiments indicates emission of UV and sob X- ray (5eV to 7KeV) photons by ion pumps Op=cal lever tests on advanced LIGO test masses show correla=on of increase and fluctua=ons in charge with ion pumps on while more constant charge on surfaces with ion pumps off. Charge on test mass mostly posi=ve (direct electron photo emission) and occasionally nega=ve (photo emission by neighboring materials with lower work func=on and larger quantum efficiency yielding electrons that migrate to test mass)

Gamma Vacuum ion pump test Collector Feedthrough Silver (Ag) Collector Collector Shield Deflector Voltage Feedthrough Ion Pump High Voltage Feedthrough Deflector

Ground Potential Collector Results 20S CV Ion Pump Collector Current vs. Pressure Collector Bias = 0V 10 1 Current, na Deflection Voltage = 1000V 0.1 Deflection Voltage = 0V 0.01 1.00E-08 1.00E-07 1.00E-06 1.00E-05 Presure (torr)

+90V Collector Bias Results 20S CV Ion Pump Collector Current vs. Pressure Collector Bias = +90V 100 Note: Collector Current is Negative Negative Current, na 10 1 Deflection Voltage = 1000V Deflection Voltage = 0V 0.1 1.00E-08 1.00E-07 1.00E-06 1.00E-05 Pressure (torr)

EXIMO Pump Test Results 20S Normal vs. 25S EXIMO Ion Pump Collector Current vs. Pressure Collector Bias = +90V 10.00000 7 KV Pump Voltage Negative Current, na 1.00000 0.10000 0.01000 0.00100 0.00010 Normal Pump EXIMO Pump 0.00001 1.00E-10 1.00E-09 1.00E-08 1.00E-07 1.00E-06 1.00E-05 Pressure, Torr

End sta=on layout ion pump

Es=mate of ion emission at LHO ETMY

Charging model

Displacement from the surface charge

Noise from charge fluctua=ons

Steps to reduce the charging Gamma vacuum to see it they can make 1/1000 reduc=on shield for ion pumps. If so would replace them at all pumps in LIGO near the ITM and ETM Replace ion pump on manifold with NEG pump and place more ion pumps on beam tube. Improve and mul=ply the number of ionizers

Proposed pumping strategy

Proper=es of SAES D3500 NEG CapaciTorr D 3500 HIGHLIGHTS General Features High pumping speed for all active gases High sorption capacity and increased lifetime Costant pumping speed in HV, UHV and XHV Reversible pumping of hydrogen and its isotopes Possibility of operation at room temperature after activation, without power Operation in the presence of high magnetic fields Oil free and vibration free in ultra high vacuum Low weight The CapaciTorr D 3500 pump is the highest performing pump of the CapaciTorr series. With the use of a special highly porous sintered Zr V Fe getter material, St 172, the pump is able to reach 3600 l/s pumping speed for hydrogen in UHV conditions. The St 172 getter cartridge is mounted on a heater structure using a single heater element, and it comes on CF150 or CF200 flanges. The flanges (AISI 316 LN) are conveniently supplied with a custom made bakeable electrical connector which combines power and thermocouple pins, for best integration and minimum footprint. St 172 material offers superior gas diffusivity characteristics and allows operation at room or intermediate temperatures (200 C) to increase the sorption capacity in presence of high gas loads. The pump sorption speed is at its maximum when the pump is mounted directly in the vacuum system without a body. The pumping speed curves related to different mounting positions are shown in the attached graph. Applications Improving ultimate vacuum in combination with ion, diffusion, cryogenetic or turbomolecular pumps Surface analysis systems Particle accelerators, synchrotron radiation sources and related equipment Process pumps for vacuum devices and deposition chambers Portable vacuum instrumentation Pumping, storing and releasing hydrogen isotopes Impurities removal in rare gas filled devices group making innovation happen, together Ordering Information Dimensions in mm Product Product description Code Base flange with Connector and Heater CapaciTorr Base Flange CF150 4H0480 Base flange with Connector and Heater CapaciTorr Base Flange CF200 4H0482 Pump body CF150/CF200 Special body CF150/CF200 4H0233 Pump body CF200/CF250 Special body CF200/CF250 4H0234 St 172 Getter Cartridge CapaciTorr D3500 4H0481

Proper=es of SAES D3500 NEG 10000 CapaciTorr D3500 sorption test (according to ASTM F798 97) CapaciTorr D 3500 Pumping Speed (l/s) 1000 100 10 120 Sorption Temperature: 25 C Activation:60' @ 92,4V(365 W) Sorption pressure: 3E 6 Torr 1 0,001 0,01 0,1 1 10 100 Sorbed Quantity (Torr l ) nude configuration Heating parameters N 2 CO H 2 H 2 O O 2 with body 250mm (CF200/CF250) 6 The SAES Group manufacturing companies are ISO9001 certified, the Asian and Italian companies are also ISO14001 certified. Full information about our certifications for each company of the Group is available on our website at: www.saesgroup.com 100 5 D.VS.114.0.13 Voltage (V) 80 60 40 4 3 2 Current (A) 20 1 0 0 100 200 300 400 500 600 Temperature ( C) Voltage (V) Current (A) 0 Typical Pump Characteristics CapaciTorr D 3500 Alloy Type St 172 Alloy Composition ZrVFe Getter Mass (g) 395 Getter Surface (cm 2 ) 2964 H 2 3600 Pumping Speed (l/s) H 2 O 2700 CO 1800 N 2 1000 Sorption Capacity (Torr l) H 2 3950 CO at 25 C 12 CO total 3100 Note: Pumping speed data refer to the initial values for the pump without in nude configuration. CO capacity based on a minimum sorption speed of 100 l/s in nude configuration. Power supply and cables Product Product description Code NEG Power Supply NEG pump controller V1.1 3B0351 NEG Power Supply RS 485 NEG pump controller V1.1 800P 3B0366 Input Cable Cable Mains Input V1.1 2Mt 3B0336 Output Cable 3Mt lenght Cable supply output V1.1 5 3Mt 3B0337 Output Cable 5Mt lenght Cable supply output V1.1 5 5Mt 3B0361 SAES Group. Printed in Italy. All rights reserved. SAES and CapaciTorr are registered trademarks of SAES Group. SAES Group reserves the right to change or modify product specifications at any timewithout notice. group SAES Group www.saesgroup.com neg_technology@saes group.com

Steps to improve and mul=ply ionizers Reliably generate equal + and ions different poten=als on the needles AC and DC, beqer instrumenta=on for flow add oxygen or use argon test in present setup Sample industry to determine if they can make 8 ionizer before the New Year Kimball Physics (New Hampshire) Electrosta=cs Inc (Pennsylvania) Possibility to use LIGO engineering to make the 8 ionizers

Steps we need to take Establish the charging on the ITM Measure the noise with the test masses discharged Probably best to do this at LLO, need to move ionizer to LLO Need to put gate valves on all the test mass chambers to receive the ionizer Fix the wiring and connectors Fix the D/A and reduce noise in ESD amplifiers by making a low voltage version for running

Current state of ESD in vacuum wiring!! LLO!ETMX! LLO!ETMY! LLO!ITMX! LLO!ITMY! LHO!ETMX! LHO!ETMY! LHO!ITMX! LHO!ITMY! bias! shorted!shield! ok! connected! not!connected! ok! shorted!shield! connected! connected! LL! probably!ok! probably!ok! connected! not!connected! probably!ul! probably!ul! connected! connected! UL! probably!ok! probably!ok! connected! not!connected! probably!ll! probably!ll! connected! connected! LR! probably!ok! probably!ok! connected! not!connected! probably!ur! probably!ok! connected! connected! UR! shorted!shield! probably!ok! probably!ok! connected! not!connected! probably!lr! probably!ok! connected! connected! 2!¾!!gate!valve! yes! no! no! no! yes! yes! yes! yes!!

To think about for the future Stop gambling Develop a conduc=ng coa=ng high resis=vity (10s- 100sGohms/square) low op=cal loss at 1 micron Low mechanical loss Most likely ionic coa=ngs Stanford may have tested an applicable electronic coa=ng Develop an annular ring recoil mass Reduces force from charging Reduces squeeze film thermal noise