Laboratory Report Number(s) Lone Tree Road (Deep) 10/5/15, 10/19/15, 6/13/16. Address Sample Date(s) Analyses Requested

Similar documents
A Site Location Map and Site and Surrounding Properties Map are attached as Figure 1 and Figure 2, respectively.

BIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: CTRA Project: 6454 T Lab Order: A 6454 Aqueous 3/1/2013.

BIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: Cascade Thornapple River Assoc. Project: Water Analysis Lab Order:

ANALYTICAL REPORT. Job Number: Job Description: Transform Complete

The following report includes the data for the above referenced project for sample(s) received on 5/15/2017 at Air Toxics Ltd.

ANALYTICAL REPORT. Results relate only to the items tested and the sample(s) as received by the laboratory. Page 1 of 5

EPA TO-17 Volatile Organic Compounds

US EPA Method 8260 with the Tekmar Atomx XYZ P&T System and Agilent 7890B GC/5977A MS

ANALYTICAL RESULTS. Project: Mayflower, AR Pipeline Incident

Analysis of Volatile Organic Compounds Using USEPA Method 8260 and the 4760 Purge and Trap and the 4100 Autosampler

Copies: Dave Favero, RACER File

APPENDIX D Laboratory Analytical Reports

Building 280A and Building 450 Soil Sampling Results Richmond Field Station Site Berkeley Global Campus at Richmond Bay, Richmond, California

Validation of Environmental Water Methods on One System: Considerations for Sample Volume, Purge Parameters and Quality Control Parameters

US EPA Method with the Tekmar Lumin P&T Concentrator, AQUATek LVA and Agilent 7890B GC/5977A MS

Validation of USEPA Method Using a Stratum PTC, AQUATek 100 Autosampler, and Perkin-Elmer Clarus 600 GC/MS

Solid Phase Micro Extraction of Flavor Compounds in Beer

October 26, Dear Mr. White:

Using Hydrogen as An Alternative Carrier Gas for US EPA 8260

Optimal VOC Method Parameters for the StratUm PTC Purge & Trap Concentrator

Roger Bardsley, Applications Chemist; Teledyne Tekmar Page 1

Optimizing. Abstract: is standardd. procedures. altered to

Analysis of Volatile Organic Compounds in Soil Samples by EPA Method 8260 with The Stratum PTC and SOLATek 72 Multi-Matrix Autosampler

CALA Directory of Laboratories

Methanol Extraction of high level soil samples by USEPA Method 8260C

Validation of USEPA Method 8260C Using Teledyne Tekmar Atomx, and Perkin-Elmer Clarus 600 GC/MS


Table 1 Soil and Groundwater Sampling Summary Table

Target Compound Results Summary

317 Elm Street Milford, NH (603) Fax (603)

KSA Environmental Laboratory Inc.

A Comparison of Volatile Organic Compound Response When Using Nitrogen as a Purge Gas

Amec Foster Wheeler Environment & Infrastructure, Inc BIG SHANTY ROAD, NW, SUITE 100 KENNESAW, GEORGIA (770)

Associates. Project No.: October 25, 2017

SUMMARY REPORT OF AIR MONITORING FOR LEED CERTIFICATION PHASE 2 SWANSFIELD ELEMENTARY SCHOOL 5610 CEDAR LANE COLUMBIA, MD PREPARED FOR:

Validation of Volatile Organic Compound by USEPA. Method 8260C. Application Note. Abstract. Introduction. Experimental-Instrument Conditions

Non-Potable Water A2LA Certificate

National Pollutant Discharge Elimination System (NPDES); BADCT Limits for Volatile Organic Compounds

Analysis of Volatile Organic Compounds in Water and Soil by EPA Method 8260 with the Atomx Concentrator/Multimatrix Autosampler

2. September 2015 Sub-Concrete Slab Soil Investigation

Roger Bardsley, Applications Chemist; Teledyne Tekmar P a g e 1

Maximizing Sample Throughput In Purge And Trap Analysis

ANALYTICAL REPORT. Job Number: SDG Number: Job Description: Joint Base Cape Cod

OREGON Environmental Laboratory Accreditation Program ORELAP Fields of Accreditation ALS Environmental - Simi Valley

Exploring US EPA Method 524 Purge and Trap Variables: Water Vapor Reduction and Minimizing Cycle Time

2017 EPA Method Update Rule and EPA Method 624.1

A Single Calibration Method for Water AND Soil Samples Performing EPA Method 8260

CERTIFICATE OF ANALYSIS

Solid Phase Micro Extraction of Flavor Compounds in Beer

Date Issued: April 01, 2013 Expiration Date: June 30, 2013

Method 8270C PAH. FD- Field Duplicate Samples

Maximizing Production While Minimizing Costs

January 19, Dear Mr. Nightingale:

ANALYTICAL REPORT. Job Number: Job Description: Gasoline Uptake Study. For: IRST Commonwealth Dr. Louisville, KY 40299

Improved Volatiles Analysis Using Static Headspace, the Agilent 5977B GC/MSD, and a High-efficiency Source

Method 8260C by Purge and Trap Gas Chromatography Mass Spectrometry using the Clarus SQ 8

Optimizing Standard Preparation

If you have any questions or concerns, please do not hesitate to contact our office at

Performance of a Next Generation Vial Autosampler for the Analysis of VOCs in Water Matrices

Helium conservation in volatile organic compound analysis using U.S. EPA Method 8260C

Detection of Environmental Contaminants Caused by the Oil Spill in the Gulf of Mexico by GC and Hplc

ANALYTICAL REPORT. Attn: Dan Spector

Appendix 2 Data Distributions for Contaminants in Water and Sediment Samples in Response to the Deepwater Horizon Oil Spill, 2010

/J~ GOLDER. Golder Associates Inc. golder.com. Project No April 25, 2018

STONY HOLLOW LANDFILL, INC S. Gettysburg Ave. Dayton, OH (937) (937) Fax

Certificate of Accreditation

Validation of USEPA Method Using a Stratum PTC and the New AQUATek 100 Autosampler

Ed George and Anaïs Viven Varian, Inc.

Certificate of Accreditation

INNOVATIVE PRODUCTS, SUPERIOR SUPPORT. Presenter: Anne Jurek, Senior Applications Chemist, EST Analytical

Application News AD Quantitative Determination of Volatile Organic Compounds in Drinking Water by EPA Method with Headspace Trap GC-MS

McCAMPBELL ANALYTICAL INC Willow Pass Road Pittsburg CA

Analysis. Introduction: necessary. presented. Discussion: As part of be carried. consistent and reliable data. (MoRT) to.

1. Introduction. 2. Sampling Activities

AUTONOMOUS, REAL TIME DETECTION OF 58 VOCS IN THE PANAMA CANAL

U.S. EPA VOLATILE ORGANICS METHOD USING PURGE AND TRAP GC/MS

Barbara Johnson, PE Associate

Texas Commission on Environmental Quality INTEROFFICE MEMORANDUM

SUBSURFACE (PHASE II) INVESTIGATION REPORT

F 2: Phase 2 Soil Vapor Investigation for Potential Off Site Vapor Intrusion

Certificate of Accreditation

TETRA TECH, INC. December 8, Lynn Nakashima Berkeley Regional Office 700 Heinz Avenue, Suite 200C Berkeley, California 94710

System and JUREK ANNE. Introduction: in an in purge and. trap sampling. Discussion: As part of. consistent and reliable data. (MoRT) to.

Analysis of Low Level Volatile Organic Compounds in Air Anne Jurek

Detection of Volatile Organic Compounds in polluted air by an Agilent mini Thermal Desorber and an Agilent 5975T LTM GC/MS

A Single Calibration for Waters and Soil Samples Performing EPA Method Anne Jurek Applications Chemist

GOLDER. Golder Associates Inc. Al-1!1f;s. golder.com. June 22, Project No

-~~ Barbara Johnson, PE Associate

Solid Phase Microextraction of Cyanogen Chloride and Other Volatile Organic Compounds in Drinking Water with Fast Analysis by GC-TOFMS

R.E.A.C.T. Roxbury Environmental Action CoaliTion P.O. Box 244 Ledgewood, N.J Website:

Optimizing of Volatile Organic Compound Determination by Static Headspace Sampling

Methods and Analytes Requiring Laboratory Certification Attachment 3

ANALYTICAL REPORT. Job Number: SDG Number: Kingston Job Description: Ulster County Resource Recovery Agency

Certificate of Accreditation

AIR QUALITY SURVEY OF SYNTHETIC TURF FIELDS CONTAINING CRUMB RUBBER INFILL

Reduced VOC Sample Analysis Times Using a New Dual Purge-and-Trap System

Optimal Conditions for USEPA Method 8260B Analysis using the EST Analytical Sampling system and the Shimadzu GCMS-QP2010s

ANALYTICAL RESULTS. Project: Mayflower, AR Pipeline Incident

METHOD 5021 VOLATILE ORGANIC COMPOUNDS IN SOILS AND OTHER SOLID MATRICES USING EQUILIBRIUM HEADSPACE ANALYSIS

LABORATORY DATA REVIEW CHECKLIST

Transcription:

July 14, 216 Mr. Shaun Lehman MDEQ-OOGM Lansing District Office Constitution Hall 2 South 525 West Allegan Street Lansing, MI 48913 Re: Residential Well Sampling Hartland 36 Gas Plant SE/NE/NW Section 36, T3N-R6E Hartland Township, Livingston County, Michigan Dear Mr. Lehman: Per the request of Merit Energy Company (MEC), Environmental Consulting & Technology, Inc. (ECT) performed residential water supply well sampling in October 215, June 216, and July 216 in Hartland Township, Michigan. A total of fifteen water supply wells were sampled by personnel from ECT. The samples were submitted for the analyses noted in the below table to an independent/third party accredited laboratory. Laboratory analytical results were reported as not detected at the Reporting Limit for all analyses requested for all samples collected. Laboratory analytical reports are attached. Figure 1, attached, depicts the approximate locations of all sampled residential water supply wells. The following table indicates the addresses, dates, laboratory analyses requested, and laboratory report number for sampled wells: 3399 Veterans Drive Traverse City, MI 49684 (231) 946-82 FAX (231) 946-828 Address Sample Date(s) Analyses Requested Laboratory Report Number(s) 1339 Lone Tree Road (Deep) 1/5/15, 1/19/15, 6/13/16 Sulfolane 1, ethylene glycol 2, SVOCs 3, VOCs 4 151283, 1511248, 166871 1339 Lone Tree Road (Shallow) 1/3/15, 6/13/16 Sulfolane, ethylene 1511956, 16687 glycol, SVOCs, VOCs 9 Erin Lane 6/7/16 Sulfolane, DIPA 5, VOCs 166476 9 Erin Lane (Pole Bldg) 6/14/16 Sulfolane, DIPA, VOCs 16693 139 Cherry Blossom Lane 6/13/16 Sulfolane, DIPA, VOCs 166887 1385 Cherry Blossom Lane 6/6/16 Sulfolane, DIPA, VOCs 166479 13593 Sheila Lane 6/6/16 Sulfolane, DIPA, VOCs 166481 46 Jeni Lane 6/13/16 Sulfolane, DIPA, VOCs 166873 513 Jeni Lane 6 6/14/16 Sulfolane, DIPA, VOCs 16692 477 Jeni Lane 6/13/16 Sulfolane, DIPA, VOCs 166884 495 Jeni Lane 6/6/16 Sulfolane, DIPA, VOCS 166478 869 Pleasant Valley Road 6/13/16 Sulfolane, DIPA, VOCs 166886 13223 Lone Tree Road 6/7/16 Sulfolane, DIPA, VOCs 16648 13247 Lone Tree Road 6/7/16 Sulfolane, DIPA, VOCs 166484 13955 Cherry Blossom Lane 7/7/16 Sulfolane, DIPA, VOCs 16739 1 Sulfolane analyzed by method SW846 827D 2 Ethylene glycol analyzed by method SW815M 3 SVOCs: Semi-Volatile Organic Compounds analyzed by method SW846 827D 4 VOCs: Volatile Organic Compounds analyzed by method SW826B 5 DIPA: Diisopropanolamine analyzed by method SW846 827D 6 Due to a transcription error, 513 Jeni Lane is recorded in laboratory report 16692 as 731 Jeni Lane A copy of this letter has been sent to the Livingston County Department of Public Health and copies of each laboratory report have been sent to respective property owners. An Equal Opportunity/Affirmative Action Employer www.ectinc.com

Residential Well Sampling Hartland 36 Gas Plant July 14, 216 Page 2 Closing ECT sincerely appreciates the opportunity to provide our consulting services on this important project. Should you have questions or require additional information, please do not hesitate to contact me at your convenience at 231.946.82 or jlewandowski@ectinc.com. Sincerely, ENVIRONMENTAL CONSULTING & TECHNOLOGY, INC. Jeremy S. Lewandowski Senior Engineer Dirk S. Mammen Principal Scientist CC: Matt Bolang Livingston County Department of Public Health Sean Craven Merit Energy Company Attachments: Figure 1 Sampled Residential Well Locations Laboratory Analytical Reports

8-Oct-215 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: Hartland Gas Plant Work Order: 151283 Dear Sean, ALS Environmental received 24 samples on 6-Oct-215 8:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 31. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 8-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 151283 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 151283-1 F-2 (18') Soil 1/2/215 15:5 1/6/215 8:3 151283-2 F-3 (18') Soil 1/2/215 15:4 1/6/215 8:3 151283-3 SS-18 (.5') Soil 1/2/215 17:5 1/6/215 8:3 151283-4 SW-1 (8') Soil 1/5/215 15:3 1/6/215 8:3 151283-5 SW-2 (8') Soil 1/5/215 15:35 1/6/215 8:3 151283-6 SW-3 (7') Soil 1/5/215 15:4 1/6/215 8:3 151283-7 SW-4 (1') Soil 1/5/215 15:45 1/6/215 8:3 151283-8 F-1 (11') Soil 1/5/215 15:5 1/6/215 8:3 151283-9 SS-9 (4') Soil 1/5/215 15:55 1/6/215 8:3 151283-1 SS-9 (8') Soil 1/5/215 16: 1/6/215 8:3 151283-11 SS-1 (2') Soil 1/5/215 16:5 1/6/215 8:3 151283-12 SS-1 (1') Soil 1/5/215 16:1 1/6/215 8:3 151283-13 SS-11 (2') Soil 1/5/215 16:12 1/6/215 8:3 151283-14 SS-11 (4') Soil 1/5/215 16:14 1/6/215 8:3 151283-15 SS-12 (4') Soil 1/5/215 16:16 1/6/215 8:3 151283-16 SS-12 (6') Soil 1/5/215 16:18 1/6/215 8:3 151283-17 SS-13 (4') Soil 1/5/215 16:2 1/6/215 8:3 151283-18 SS-14 (2') Soil 1/5/215 16:22 1/6/215 8:3 151283-19 SS-14 (4') Soil 1/5/215 16:24 1/6/215 8:3 151283-2 SS-15 (6') Soil 1/5/215 16:26 1/6/215 8:3 151283-21 SS-15 (1') Soil 1/5/215 16:28 1/6/215 8:3 151283-22 SS-16 (2') Soil 1/5/215 16:3 1/6/215 8:3 151283-23 SS-17 (2') Soil 1/5/215 16:32 1/6/215 8:3 151283-24 W-13339 Water 1/5/215 14:25 1/6/215 8:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 8-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 151283 Sample ID: W-13339 Lab ID: 151283-24 Collection Date: 1/5/215 2:25 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 1/6/15 Analyst: RM Sulfolane 1 µg/l 1 1/6/215 6:6 PM Surr: 2,4,6-Tribromophenol 78.2 38-115 %REC 1 1/6/215 6:6 PM Surr: 2-Fluorobiphenyl 7.5 32-1 %REC 1 1/6/215 6:6 PM Surr: 2-Fluorophenol 35.6 22-59 %REC 1 1/6/215 6:6 PM Surr: 4-Terphenyl-d14 8.2 23-112 %REC 1 1/6/215 6:6 PM Surr: Nitrobenzene-d5 72. 31-93 %REC 1 1/6/215 6:6 PM Surr: Phenol-d6 22. 13-36 %REC 1 1/6/215 6:6 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 18 of 18

ALS Group USA, Corp Client: Merit Energy Work Order: 151283 Project: Hartland Gas Plant Date: 8-Oct-15 Batch ID: 7718 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-7718-7718 Units: µg/l Client ID: Run ID: SVMS8_1516A SeqNo: 3495142 Analysis Date: 1/6/215 4:7 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1 Surr: 2,4,6-Tribromophenol 39.49 5 79 38-115 Surr: 2-Fluorobiphenyl 35.54 5 71.1 32-1 Surr: 2-Fluorophenol 18.97 5 37.9 22-59 Surr: 4-Terphenyl-d14 43.6 5 86.1 23-112 Surr: Nitrobenzene-d5 34.66 5 69.3 31-93 Surr: Phenol-d6 11.92 5 23.8 13-36 LCS Sample ID: SLCSW2-7718-7718 Units: µg/l Client ID: Run ID: SVMS8_1516A SeqNo: 3495143 Analysis Date: 1/6/215 4:47 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1.45 1 2 52.2 Surr: 2,4,6-Tribromophenol 38.13 5 76.3 38-115 Surr: 2-Fluorobiphenyl 34.88 5 69.8 32-1 Surr: 2-Fluorophenol 18.82 5 37.6 22-59 Surr: 4-Terphenyl-d14 41.58 5 83.2 23-112 Surr: Nitrobenzene-d5 34.45 5 68.9 31-93 Surr: Phenol-d6 12.37 5 24.7 13-36 The following samples were analyzed in this batch: 151283-24A QC Page: 1 of 5

Client: Merit Energy Work Order: 151283 Project: Hartland Gas Plant Batch ID: 7728 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKS1-7728-7728 Units: µg/kg Client ID: Run ID: SVMS8_1516A SeqNo: 3495145 Analysis Date: 1/6/215 6:26 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 17 Surr: 2,4,6-Tribromophenol 1357 1667 81.4 34-14 Surr: 2-Fluorobiphenyl 1249 1667 75 12-1 Surr: 2-Fluorophenol 124 1667 72.2 33-117 Surr: 4-Terphenyl-d14 1554 1667 93.3 25-137 Surr: Nitrobenzene-d5 1247 1667 74.8 37-17 Surr: Phenol-d6 1167 1667 7 4-16 LCS Sample ID: SLCSS1-7728-7728 Units: µg/kg Client ID: Run ID: SVMS8_1516A SeqNo: 3495146 Analysis Date: 1/6/215 6:45 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 474.3 17 666.7 71.1 Surr: 2,4,6-Tribromophenol 133 1667 79.8 34-14 Surr: 2-Fluorobiphenyl 1254 1667 75.2 12-1 Surr: 2-Fluorophenol 1252 1667 75.1 33-117 Surr: 4-Terphenyl-d14 16 1667 96 25-137 Surr: Nitrobenzene-d5 1263 1667 75.8 37-17 Surr: Phenol-d6 122 1667 73.2 4-16 MS Sample ID: 151283-3A MS Units: µg/kg Client ID: SS-18 (.5') Run ID: SVMS8_1516A SeqNo: 3495147 Analysis Date: 1/6/215 7:5 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 41.5 16 656.1 61.2 Surr: 2,4,6-Tribromophenol 1181 164 72 34-14 Surr: 2-Fluorobiphenyl 139 164 63.4 12-1 Surr: 2-Fluorophenol 18 164 61.5 33-117 Surr: 4-Terphenyl-d14 1249 164 76.1 25-137 Surr: Nitrobenzene-d5 125 164 62.5 37-17 Surr: Phenol-d6 979.8 164 59.7 4-16 QC Page: 2 of 5

Client: Merit Energy Work Order: 151283 Project: Hartland Gas Plant Batch ID: 7728 Instrument ID: SVMS8 Method: SW846 827D MSD Sample ID: 151283-3A MSD Units: µg/kg Client ID: SS-18 (.5') Run ID: SVMS8_1516A SeqNo: 3495148 Analysis Date: 1/6/215 7:25 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 422.7 17 664.1 63.6 41.5 5.14 Surr: 2,4,6-Tribromophenol 123 166 74.1 34-14 1181 4.6 4 Surr: 2-Fluorobiphenyl 1129 166 68 12-1 139 8.28 4 Surr: 2-Fluorophenol 114 166 66.5 33-117 18 9.6 4 Surr: 4-Terphenyl-d14 1383 166 83.3 25-137 1249 1.2 4 Surr: Nitrobenzene-d5 1111 166 66.9 37-17 125 8.4 4 Surr: Phenol-d6 185 166 65.3 4-16 979.8 1.2 4 The following samples were analyzed in this batch: 151283-1A 151283-2A 151283-3A 151283-4A 151283-5A 151283-6A 151283-7A 151283-8A 151283-9A 151283-11A 151283-13A 151283-15A 151283-17A 151283-18A 151283-2A 151283-22A 151283-23A QC Page: 3 of 5

Client: Merit Energy Work Order: 151283 Project: Hartland Gas Plant Batch ID: R173214 Instrument ID: MOIST Method: E16.3M MBLK Sample ID: WBLKS-R173214 Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: Run ID: MOIST_1516C SeqNo: 3494733 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Moisture.5 Limit Qual LCS Sample ID: LCS-R173214 Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: Run ID: MOIST_1516C SeqNo: 349473 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture 99.99.5 1 1 99.5-1.5 DUP Sample ID: 151283-6A DUP Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: SW-3 (7') Run ID: MOIST_1516C SeqNo: 3494711 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture 17.3.5 17.46 2.49 2 DUP Sample ID: 15132-1B DUP Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: Run ID: MOIST_1516C SeqNo: 3494724 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture 13.89.5 14.1.86 2 The following samples were analyzed in this batch: 151283-1A 151283-2A 151283-3A 151283-4A 151283-5A 151283-6A 151283-7A 151283-8A 151283-9A 151283-11A 151283-13A 151283-15A 151283-17A 151283-18A 151283-2A QC Page: 4 of 5

Client: Merit Energy Work Order: 151283 Project: Hartland Gas Plant Batch ID: R173341 Instrument ID: MOIST Method: E16.3M MBLK Sample ID: WBLKS-R173341 Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: 3497864 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Moisture.5 Limit Qual LCS Sample ID: LCS-R173341 Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: 3497863 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture 1.5 1 1 99.5-1.5 DUP Sample ID: 1591436-3B DUP Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: 3497844 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture 19.85.5 2.58 3.61 2 DUP Sample ID: 151261-4A DUP Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: 3497858 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture 6.47.5 6.89 6.29 2 The following samples were analyzed in this batch: 151283-22A 151283-23A QC Page: 5 of 5

ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant WorkOrder: 151283 Date: 8-Oct-15 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported % of sample µg/kg-dry µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Percent of Sample Micrograms per Kilogram Dry Weight Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 6-Oct-15 8:3 Work Order: 151283 Received by: NML Checklist completed by Diane Shaw Gary Byar 6-Oct-15 Reviewed by: esignature Date esignature 6-Oct-15 Date Matrices: Carrier name: Soil, water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2./2. c SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 1/6/215 8:54:55 AM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

3-Oct-215 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: Hartland Gas Plant Work Order: 1511248 Dear Sean, ALS Environmental received 1 sample on 2-Oct-215 1: AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 22. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511248 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 1511248-1 W-1339 Deep Water 1/19/215 9:3 1/2/215 1: Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511248 Sample ID: W-1339 Deep Lab ID: 1511248-1 Collection Date: 1/19/215 9:3 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed ORGANIC COMPOUS BY GC-FID SW815M Analyst: KYM Ethylene glycol 5. mg/l 1 1/21/215 12:41 PM SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 1/23/15 Analyst: RS 2-Methylnaphthalene 5. µg/l 1 1/23/215 9:12 PM Acenaphthene 5. µg/l 1 1/23/215 9:12 PM Acenaphthylene 5. µg/l 1 1/23/215 9:12 PM Anthracene 5. µg/l 1 1/23/215 9:12 PM Benzo(a)anthracene 5. µg/l 1 1/23/215 9:12 PM Benzo(a)pyrene 5. µg/l 1 1/23/215 9:12 PM Benzo(b)fluoranthene 5. µg/l 1 1/23/215 9:12 PM Benzo(g,h,i)perylene 5. µg/l 1 1/23/215 9:12 PM Benzo(k)fluoranthene 5. µg/l 1 1/23/215 9:12 PM Chrysene 5. µg/l 1 1/23/215 9:12 PM Dibenzo(a,h)anthracene 5. µg/l 1 1/23/215 9:12 PM Fluoranthene 5. µg/l 1 1/23/215 9:12 PM Fluorene 5. µg/l 1 1/23/215 9:12 PM Indeno(1,2,3-cd)pyrene 5. µg/l 1 1/23/215 9:12 PM Naphthalene 5. µg/l 1 1/23/215 9:12 PM Phenanthrene 5. µg/l 1 1/23/215 9:12 PM Pyrene 5. µg/l 1 1/23/215 9:12 PM Surr: 2,4,6-Tribromophenol 75. 38-115 %REC 1 1/23/215 9:12 PM Surr: 2-Fluorobiphenyl 62.5 32-1 %REC 1 1/23/215 9:12 PM Surr: 2-Fluorophenol 34.7 22-59 %REC 1 1/23/215 9:12 PM Surr: 4-Terphenyl-d14 9.5 23-112 %REC 1 1/23/215 9:12 PM Surr: Nitrobenzene-d5 58.9 31-93 %REC 1 1/23/215 9:12 PM Surr: Phenol-d6 22.2 13-36 %REC 1 1/23/215 9:12 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,1-Trichloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,2-Trichloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 1/29/215 7:1 PM 1,1-Dichloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1-Dichloroethene 1. µg/l 1 1/29/215 7:1 PM 1,2,3-Trichloropropane 1. µg/l 1 1/29/215 7:1 PM 1,2,4-Trichlorobenzene 1. µg/l 1 1/29/215 7:1 PM 1,2,4-Trimethylbenzene 1. µg/l 1 1/29/215 7:1 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 1/29/215 7:1 PM 1,2-Dibromoethane 1. µg/l 1 1/29/215 7:1 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 3

ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511248 Sample ID: W-1339 Deep Lab ID: 1511248-1 Collection Date: 1/19/215 9:3 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 2-Methylnaphthalene 4-Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1 µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 3

ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511248 Sample ID: W-1339 Deep Lab ID: 1511248-1 Collection Date: 1/19/215 9:3 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 99.8 95.6 98.5 97.4 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 3 of 3

ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511248 Date: 3-Oct-15 Case Narrative Batch R174943A The MS/MSD data for volatiles is not related tot his project's samples. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Date: 3-Oct-15 Batch ID: R174314 Instrument ID: GC11 Method: SW815M MBLK Sample ID: MB-R174314-R174314 Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: 3521228 Analysis Date: 1/21/215 11:1 A Prep Date: 1/21/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Ethylene glycol 5. Limit Qual LCS Sample ID: LCS-R174314-R174314 Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: 3521229 Analysis Date: 1/21/215 1:7 A Prep Date: 1/21/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol 534.2 5. 5 17 5-15 MS Sample ID: 151115-1A MS Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: 3521237 Analysis Date: 1/21/215 1:16 A Prep Date: 1/21/215 DF: 2 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol 935.3 1 1 93.5 5-15 MSD Sample ID: 151115-1A MSD Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: 3521238 Analysis Date: 1/21/215 1:25 A Prep Date: 1/21/215 DF: 2 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol 949.6 1 1 95 5-15 935.3 1.51 3 The following samples were analyzed in this batch: 1511248-1A QC Page: 1 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: 77892 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-77892-77892 Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: 352942 Analysis Date: 1/23/215 3:37 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 5. Acenaphthene 5. Acenaphthylene 5. Anthracene 5. Benzo(a)anthracene 5. Benzo(a)pyrene 5. Benzo(b)fluoranthene 5. Benzo(g,h,i)perylene 5. Benzo(k)fluoranthene 5. Chrysene 5. Dibenzo(a,h)anthracene 5. Fluoranthene 5. Fluorene 5. Indeno(1,2,3-cd)pyrene 5. Naphthalene 5. Phenanthrene 5. Pyrene 5. Surr: 2,4,6-Tribromophenol 36.48 5 73 38-115 Surr: 2-Fluorobiphenyl 34.53 5 69.1 32-1 Surr: 2-Fluorophenol 18.53 5 37.1 22-59 Surr: 4-Terphenyl-d14 42.61 5 85.2 23-112 Surr: Nitrobenzene-d5 33.2 5 66.4 31-93 Surr: Phenol-d6 9.69 5 19.4 13-36 QC Page: 2 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: 77892 Instrument ID: SVMS8 Method: SW846 827D LCS Sample ID: SLCSW1-77892-77892 Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: 352945 Analysis Date: 1/23/215 3:57 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 13.48 5. 2 67.4 45-15 Acenaphthene 13.35 5. 2 66.8 45-11 Acenaphthylene 14.37 5. 2 71.8 5-15 Anthracene 15.46 5. 2 77.3 55-11 Benzo(a)anthracene 16.65 5. 2 83.2 55-11 Benzo(a)pyrene 17.5 5. 2 85.2 55-11 Benzo(b)fluoranthene 16.55 5. 2 82.8 45-12 Benzo(g,h,i)perylene 18.28 5. 2 91.4 4-125 Benzo(k)fluoranthene 16.56 5. 2 82.8 45-125 Chrysene 16.75 5. 2 83.8 55-11 Dibenzo(a,h)anthracene 18.31 5. 2 91.6 4-125 Fluoranthene 16.23 5. 2 81.2 55-115 Fluorene 15.84 5. 2 79.2 5-11 Indeno(1,2,3-cd)pyrene 18.66 5. 2 93.3 45-125 Naphthalene 12.23 5. 2 61.2 4-1 Phenanthrene 15.44 5. 2 77.2 5-115 Pyrene 17.17 5. 2 85.8 5-13 Surr: 2,4,6-Tribromophenol 41.17 5 82.3 38-115 Surr: 2-Fluorobiphenyl 34.84 5 69.7 32-1 Surr: 2-Fluorophenol 2.35 5 4.7 22-59 Surr: 4-Terphenyl-d14 41.6 5 83.2 23-112 Surr: Nitrobenzene-d5 35.6 5 7.1 31-93 Surr: Phenol-d6 11.82 5 23.6 13-36 QC Page: 3 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: 77892 Instrument ID: SVMS8 Method: SW846 827D MS Sample ID: 1511326-6B MS Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: 352947 Analysis Date: 1/23/215 5:36 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 15.44 5. 2 77.2 45-15 Acenaphthene 14.71 5. 2 73.6 45-11 Acenaphthylene 15.2 5. 2 76 5-15 Anthracene 16.3 5. 2 81.5 55-11 Benzo(a)anthracene 17.32 5. 2 86.6 55-11 Benzo(a)pyrene 17.76 5. 2 88.8 55-11 Benzo(b)fluoranthene 17.21 5. 2 86 45-12 Benzo(g,h,i)perylene 19 5. 2 95 4-125 Benzo(k)fluoranthene 17.2 5. 2 85.1 45-125 Chrysene 17.9 5. 2 85.4 55-11 Dibenzo(a,h)anthracene 18.88 5. 2 94.4 4-125 Fluoranthene 16.84 5. 2 84.2 55-115 Fluorene 16.5 5. 2 82.5 5-11 Indeno(1,2,3-cd)pyrene 19.5 5. 2 95.2 45-125 Naphthalene 13.98 5. 2 69.9 4-1 Phenanthrene 15.93 5. 2 79.6 5-115 Pyrene 17.29 5. 2 86.4 5-13 Surr: 2,4,6-Tribromophenol 41.32 5 82.6 38-115 Surr: 2-Fluorobiphenyl 35.32 5 7.6 32-1 Surr: 2-Fluorophenol 17.26 5 34.5 22-59 Surr: 4-Terphenyl-d14 35.7 5 7.1 23-112 Surr: Nitrobenzene-d5 36.92 5 73.8 31-93 Surr: Phenol-d6 9.64 5 19.3 13-36 QC Page: 4 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: 77892 Instrument ID: SVMS8 Method: SW846 827D DUP Sample ID: 1511326-8B DUP Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: 352941 Analysis Date: 1/23/215 6:15 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 5. - 3 Acenaphthene 5. - 3 Acenaphthylene 5. - 3 Anthracene 5. - 3 Benzo(a)anthracene 5. - 3 Benzo(a)pyrene 5. - 3 Benzo(b)fluoranthene 5. - 3 Benzo(g,h,i)perylene 5. - 3 Benzo(k)fluoranthene 5. - 3 Chrysene 5. - 3 Dibenzo(a,h)anthracene 5. - 3 Fluoranthene 5. - 3 Fluorene 5. - 3 Indeno(1,2,3-cd)pyrene 5. - 3 Naphthalene 5. - 3 Phenanthrene 5. - 3 Pyrene 5. - 3 Surr: 2,4,6-Tribromophenol 33.1 5 66.2 38-115 3.48 8.24 4 Surr: 2-Fluorobiphenyl 24.48 5 49 32-1 24.86 1.54 4 Surr: 2-Fluorophenol 14.5 5 29 22-59 13.86 4.51 4 Surr: 4-Terphenyl-d14 36.75 5 73.5 23-112 34.29 6.93 4 Surr: Nitrobenzene-d5 24.66 5 49.3 31-93 24.77.445 4 Surr: Phenol-d6 7.58 5 15.2 13-36 7.38 2.67 4 The following samples were analyzed in this batch: 1511248-1B QC Page: 5 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B MBLK Sample ID: VBLKW1-15129-R174943A Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: 3539439 Prep Date: Analysis Date: 1/29/215 12:12 P DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 6 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 19.66 2 98.3 75-12 Surr: 4-Bromofluorobenzene 19.2 2 96 8-11 Surr: Dibromofluoromethane 19.51 2 97.6 85-115 Surr: Toluene-d8 19.41 2 97 85-11 QC Page: 7 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B LCS Sample ID: VLCSW1-15129-R174943A Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: 3539423 Prep Date: Analysis Date: 1/29/215 1:56 A DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.59 1. 2 13 8-13 1,1,1-Trichloroethane 2.41 1. 2 12 75-13 1,1,2,2-Tetrachloroethane 19.89 1. 2 99.4 75-13 1,1,2-Trichloroethane 2.98 1. 2 15 75-125 1,1-Dichloroethane 2.77 1. 2 14 75-133 1,1-Dichloroethene 22.9 1. 2 11 7-145 1,2,3-Trichloropropane 2.57 1. 2 13 75-125 1,2,4-Trichlorobenzene 24.99 1. 2 125 7-135 1,2,4-Trimethylbenzene 22.33 1. 2 112 75-13 1,2-Dibromo-3-chloropropane 17.38 1. 2 86.9 6-13 1,2-Dibromoethane 26.87 1. 2 134 8-15 1,2-Dichlorobenzene 21.88 1. 2 19 7-13 1,2-Dichloroethane 21.31 1. 2 17 78-125 1,2-Dichloropropane 2.94 1. 2 15 75-125 1,3,5-Trimethylbenzene 22.43 1. 2 112 75-13 1,3-Dichlorobenzene 23.59 1. 2 118 75-13 1,4-Dichlorobenzene 22.8 1. 2 114 75-13 2-Butanone 16.97 5. 2 84.8 55-15 2-Hexanone 17.29 5. 2 86.4 6-135 4-Methyl-2-pentanone 2.9 1. 2 14 77-178 Acetone 17.6 1 2 85.3 6-16 Acrylonitrile 21.8 1. 2 19 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 21.66 1. 2 18 75-13 Bromodichloromethane 19.62 1. 2 98.1 75-125 Bromoform 17.6 1. 2 88 6-125 Bromomethane 23.4 1. 2 117 3-185 Carbon disulfide 24.18 1. 2 121 6-165 Carbon tetrachloride 19.98 1. 2 99.9 65-14 Chlorobenzene 21.73 1. 2 19 8-12 Chloroethane 25.44 1. 2 127 5-14 Chloroform 2.6 1. 2 1 8-13 Chloromethane 2.22 1. 2 11 5-13 cis-1,2-dichloroethene 2.85 1. 2 14 75-134 cis-1,3-dichloropropene 19.67 1. 2 98.4 7-13 Dibromochloromethane 19.71 1. 2 98.6 6-115 Dibromomethane 21.75 1. 2 19 85-125 Dichlorodifluoromethane 18.86 1. 2 94.3 2-12 Ethylbenzene 21.16 1. 2 16 85-125 Hexachloroethane 19.7 1. 2 95.4 5-124 Isopropylbenzene 22.54 1. 2 113 8-127 m,p-xylene 43.28 2. 4 18 75-13 QC Page: 8 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Methyl iodide 3.61 1. 2 153 6-16 Methyl tert-butyl ether 21.27 1. 2 16 8-13 Methylene chloride 22.49 5. 2 112 75-14 Naphthalene 19.98 5. 2 99.9 55-16 n-propylbenzene 21.75 1. 2 19 78-12 o-xylene 2.5 1. 2 12 8-125 Styrene 2.37 1. 2 12 85-125 Tetrachloroethene 23.82 1. 2 119 77-138 Toluene 21.38 1. 2 17 85-125 trans-1,2-dichloroethene 2.57 1. 2 13 8-14 trans-1,3-dichloropropene 18.64 1. 2 93.2 81-123 trans-1,4-dichloro-2-butene 15.7 2. 2 78.5 46-118 Trichloroethene 2.93 1. 2 15 84-13 Trichlorofluoromethane 23.25 1. 2 116 6-14 Vinyl chloride 2.83 1. 2 14 5-136 Xylenes, Total 63.78 3. 6 16 8-126 Surr: 1,2-Dichloroethane-d4 19.54 2 97.7 75-12 Surr: 4-Bromofluorobenzene 19.23 2 96.2 8-11 Surr: Dibromofluoromethane 19.52 2 97.6 85-115 Surr: Toluene-d8 2 2 1 85-11 QC Page: 9 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B MS Sample ID: 151125-24A MS Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: 353948 Prep Date: Analysis Date: 1/29/215 8:39 P DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 186.1 1 2 93 8-13 1,1,1-Trichloroethane 195.3 1 2 97.6 75-13 1,1,2,2-Tetrachloroethane 186.3 1 2 93.2 75-13 1,1,2-Trichloroethane 193.4 1 2 96.7 75-125 1,1-Dichloroethane 196.3 1 2 98.2 75-133 1,1-Dichloroethene 214.3 1 2 17 7-145 1,2,3-Trichloropropane 22.4 1 2 11 75-125 1,2,4-Trichlorobenzene 18 1 2 9 7-135 1,2,4-Trimethylbenzene 23.4 1 2 12 75-13 1,2-Dibromo-3-chloropropane 154.9 1 2 77.4 6-13 1,2-Dibromoethane 242.8 1 2 121 8-15 1,2-Dichlorobenzene 188.2 1 2 94.1 7-13 1,2-Dichloroethane 21.3 1 2 11 78-125 1,2-Dichloropropane 21.7 1 2 11 75-125 1,3,5-Trimethylbenzene 19.5 1 2 95.2 75-13 1,3-Dichlorobenzene 21.2 1 2 11 75-13 1,4-Dichlorobenzene 198.1 1 2 99 75-13 2-Butanone 173.1 5 2 86.6 55-15 2-Hexanone 174.8 5 2 87.4 6-135 4-Methyl-2-pentanone 23.1 1 2 12 77-178 Acetone 171.5 1 2 85.8 6-16 Acrylonitrile 198.6 1 2 99.3 6-14 Benzene 2.6 1 2 1 85-125 Bromochloromethane 195.7 1 2 97.8 75-13 Bromodichloromethane 178.9 1 2 89.4 75-125 Bromoform 144.9 1 2 72.4 6-125 Bromomethane 187.1 1 2 93.6 3-185 Carbon disulfide 28.8 1 2 14 6-165 Carbon tetrachloride 192.5 1 2 96.2 65-14 Chlorobenzene 197.8 1 2 98.9 8-12 Chloroethane 246.4 1 2 123 5-14 Chloroform 187.5 1 2 93.8 8-13 Chloromethane 194.9 1 2 97.4 5-13 cis-1,2-dichloroethene 295.7 1 2 98.8 98.4 75-134 cis-1,3-dichloropropene 176.5 1 2 88.2 7-13 Dibromochloromethane 165.8 1 2 82.9 6-115 Dibromomethane 26.5 1 2 13 85-125 Dichlorodifluoromethane 159.2 1 2 79.6 2-12 Ethylbenzene 187.6 1 2 93.8 85-125 Hexachloroethane 15.7 1 2 75.4 5-124 Isopropylbenzene 199 1 2 99.5 8-127 m,p-xylene 383.7 2 4 3.2 95.1 75-13 QC Page: 1 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Methyl iodide 27.6 1 2 135 6-16 Methyl tert-butyl ether 199.4 1 2 99.7 8-13 Methylene chloride 218.5 5 2 19 75-14 Naphthalene 17.8 5 2 85.4 55-16 n-propylbenzene 188.8 1 2 94.4 78-12 o-xylene 185.4 1 2 92.7 8-125 Styrene 183.3 1 2 91.6 85-125 Tetrachloroethene 213.6 1 2 17 77-138 Toluene 196.7 1 2 2.7 97 85-125 trans-1,2-dichloroethene 195.3 1 2 97.6 8-14 trans-1,3-dichloropropene 157.1 1 2 78.6 81-123 trans-1,4-dichloro-2-butene 131.1 2 2 65.6 46-118 Trichloroethene 196.9 1 2 98.4 84-13 Trichlorofluoromethane 217.1 1 2 19 6-14 Vinyl chloride 349.1 1 2 158.8 95.2 5-136 Xylenes, Total 569.1 3 6 94.8 8-126 Surr: 1,2-Dichloroethane-d4 195.7 2 97.8 75-12 Surr: 4-Bromofluorobenzene 191.3 2 95.6 8-11 Surr: Dibromofluoromethane 198.9 2 99.4 85-115 Surr: Toluene-d8 195.8 2 97.9 85-11 S QC Page: 11 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B MSD Sample ID: 151125-24A MSD Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: 3539483 Prep Date: Analysis Date: 1/29/215 9:3 P DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 181.5 1 2 9.8 8-13 186.1 2.5 3 1,1,1-Trichloroethane 185.8 1 2 92.9 75-13 195.3 4.99 3 1,1,2,2-Tetrachloroethane 191.9 1 2 96 75-13 186.3 2.96 3 1,1,2-Trichloroethane 185.1 1 2 92.6 75-125 193.4 4.39 3 1,1-Dichloroethane 197.9 1 2 99 75-133 196.3.812 3 1,1-Dichloroethene 24.7 1 2 12 7-145 214.3 4.58 3 1,2,3-Trichloropropane 21.3 1 2 11 75-125 22.4.545 3 1,2,4-Trichlorobenzene 19 1 2 95 7-135 18 5.41 3 1,2,4-Trimethylbenzene 187.8 1 2 93.9 75-13 23.4 7.98 3 1,2-Dibromo-3-chloropropane 15 1 2 75 6-13 154.9 3.21 3 1,2-Dibromoethane 249.4 1 2 125 8-15 242.8 2.68 3 1,2-Dichlorobenzene 184.5 1 2 92.2 7-13 188.2 1.99 3 1,2-Dichloroethane 197.9 1 2 99 78-125 21.3 1.7 3 1,2-Dichloropropane 193.2 1 2 96.6 75-125 21.7 4.3 3 1,3,5-Trimethylbenzene 186.5 1 2 93.2 75-13 19.5 2.12 3 1,3-Dichlorobenzene 197.1 1 2 98.6 75-13 21.2 2.6 3 1,4-Dichlorobenzene 196.7 1 2 98.4 75-13 198.1.79 3 2-Butanone 179.1 5 2 89.6 55-15 173.1 3.41 3 2-Hexanone 171.6 5 2 85.8 6-135 174.8 1.85 3 4-Methyl-2-pentanone 26.1 1 2 13 77-178 23.1 1.47 3 Acetone 16.3 1 2 8.2 6-16 171.5 6.75 3 Acrylonitrile 26.8 1 2 13 6-14 198.6 4.5 3 Benzene 194.9 1 2 97.4 85-125 2.6 2.88 3 Bromochloromethane 22.4 1 2 11 75-13 195.7 3.37 3 Bromodichloromethane 176.1 1 2 88 75-125 178.9 1.58 3 Bromoform 15.5 1 2 75.2 6-125 144.9 3.79 3 Bromomethane 189 1 2 94.5 3-185 187.1 1.1 3 Carbon disulfide 26.5 1 2 13 6-165 28.8 1.11 3 Carbon tetrachloride 179 1 2 89.5 65-14 192.5 7.27 3 Chlorobenzene 198.8 1 2 99.4 8-12 197.8.54 3 Chloroethane 232.5 1 2 116 5-14 246.4 5.8 3 Chloroform 186.7 1 2 93.4 8-13 187.5.428 3 Chloromethane 188.1 1 2 94 5-13 194.9 3.55 3 cis-1,2-dichloroethene 292.8 1 2 98.8 97 75-134 295.7.986 3 cis-1,3-dichloropropene 175.5 1 2 87.8 7-13 176.5.568 3 Dibromochloromethane 165.1 1 2 82.6 6-115 165.8.423 3 Dibromomethane 23.1 1 2 12 85-125 26.5 1.66 3 Dichlorodifluoromethane 13.9 1 2 65.4 2-12 159.2 19.5 3 Ethylbenzene 187.5 1 2 93.8 85-125 187.6.533 3 Hexachloroethane 141.7 1 2 7.8 5-124 15.7 6.16 3 Isopropylbenzene 196.2 1 2 98.1 8-127 199 1.42 3 m,p-xylene 375.5 2 4 3.2 93.1 75-13 383.7 2.16 3 QC Page: 12 of 13

Client: Merit Energy Work Order: 1511248 Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Methyl iodide 269.3 1 2 135 6-16 27.6.482 3 Methyl tert-butyl ether 21.5 1 2 11 8-13 199.4 1.5 3 Methylene chloride 216.5 5 2 18 75-14 218.5.92 3 Naphthalene 169.9 5 2 85 55-16 17.8.528 3 n-propylbenzene 183.3 1 2 91.6 78-12 188.8 2.96 3 o-xylene 181.8 1 2 9.9 8-125 185.4 1.96 3 Styrene 18.8 1 2 9.4 85-125 183.3 1.37 3 Tetrachloroethene 26.2 1 2 13 77-138 213.6 3.53 3 Toluene 194.6 1 2 2.7 96 85-125 196.7 1.7 3 trans-1,2-dichloroethene 191.1 1 2 95.6 8-14 195.3 2.17 3 trans-1,3-dichloropropene 158.4 1 2 79.2 81-123 157.1.824 3 trans-1,4-dichloro-2-butene 129.2 2 2 64.6 46-118 131.1 1.46 3 Trichloroethene 194 1 2 97 84-13 196.9 1.48 3 Trichlorofluoromethane 199.5 1 2 99.8 6-14 217.1 8.45 3 Vinyl chloride 329.9 1 2 158.8 85.6 5-136 349.1 5.66 3 Xylenes, Total 557.3 3 6 92.9 8-126 569.1 2.1 3 Surr: 1,2-Dichloroethane-d4 196.5 2 98.2 75-12 195.7.48 3 Surr: 4-Bromofluorobenzene 197 2 98.5 8-11 191.3 2.94 3 Surr: Dibromofluoromethane 196.9 2 98.4 85-115 198.9 1.1 3 Surr: Toluene-d8 194.5 2 97.2 85-11 195.8.666 3 S The following samples were analyzed in this batch: 1511248-1A QC Page: 13 of 13

ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant WorkOrder: 1511248 Date: 3-Oct-15 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l mg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter Milligrams per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 2-Oct-15 1: Work Order: 1511248 Received by: DS Checklist completed by Diane Shaw Gary Byar 21-Oct-15 Reviewed by: esignature Date esignature 21-Oct-15 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 c SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 1/21/215 8:11:49 AM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

11-Nov-215 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: Hartland Gas Plant Work Order: 1511956 Dear Sean, ALS Environmental received 5 samples on 31-Oct-215 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 27. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511956 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 1511956-1 TMW-6 (65-7') Water 1/3/215 12:15 1/31/215 9:3 1511956-2 TMW-6 (55-6') Water 1/3/215 12:25 1/31/215 9:3 1511956-3 TMW-6 (45-5') Water 1/3/215 12:35 1/31/215 9:3 1511956-4 TMW-6 (35-4') Water 1/3/215 12:45 1/31/215 9:3 1511956-5 W-1339 Shallow Water 1/3/215 15:2 1/31/215 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511956 Sample ID: W-1339 Shallow Lab ID: 1511956-5 Collection Date: 1/3/215 3:2 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed ORGANIC COMPOUS BY GC-FID SW815M Analyst: KYM Ethylene glycol 5. mg/l 1 11/9/215 9:34 AM SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 11/3/15 Analyst: RM 2-Methylnaphthalene 5. µg/l 1 11/4/215 9:19 PM Acenaphthene 5. µg/l 1 11/4/215 9:19 PM Acenaphthylene 5. µg/l 1 11/4/215 9:19 PM Anthracene 5. µg/l 1 11/4/215 9:19 PM Benzo(a)anthracene 5. µg/l 1 11/4/215 9:19 PM Benzo(a)pyrene 5. µg/l 1 11/4/215 9:19 PM Benzo(b)fluoranthene 5. µg/l 1 11/4/215 9:19 PM Benzo(g,h,i)perylene 5. µg/l 1 11/4/215 9:19 PM Benzo(k)fluoranthene 5. µg/l 1 11/4/215 9:19 PM Chrysene 5. µg/l 1 11/4/215 9:19 PM Dibenzo(a,h)anthracene 5. µg/l 1 11/4/215 9:19 PM Fluoranthene 5. µg/l 1 11/4/215 9:19 PM Fluorene 5. µg/l 1 11/4/215 9:19 PM Indeno(1,2,3-cd)pyrene 5. µg/l 1 11/4/215 9:19 PM Naphthalene 5. µg/l 1 11/4/215 9:19 PM Phenanthrene 5. µg/l 1 11/4/215 9:19 PM Pyrene 5. µg/l 1 11/4/215 9:19 PM Sulfolane 1 µg/l 1 11/4/215 9:19 PM Surr: 2,4,6-Tribromophenol 64. 38-115 %REC 1 11/4/215 9:19 PM Surr: 2-Fluorobiphenyl 62.4 32-1 %REC 1 11/4/215 9:19 PM Surr: 2-Fluorophenol 31.5 22-59 %REC 1 11/4/215 9:19 PM Surr: 4-Terphenyl-d14 66.4 23-112 %REC 1 11/4/215 9:19 PM Surr: Nitrobenzene-d5 53.3 31-93 %REC 1 11/4/215 9:19 PM Surr: Phenol-d6 17.8 13-36 %REC 1 11/4/215 9:19 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,1-Trichloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,2-Trichloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 11/1/215 7:27 AM 1,1-Dichloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1-Dichloroethene 1. µg/l 1 11/1/215 7:27 AM 1,2,3-Trichloropropane 1. µg/l 1 11/1/215 7:27 AM 1,2,4-Trichlorobenzene 1. µg/l 1 11/1/215 7:27 AM 1,2,4-Trimethylbenzene 1. µg/l 1 11/1/215 7:27 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 11/1/215 7:27 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 5 of 7

ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511956 Sample ID: W-1339 Shallow Lab ID: 1511956-5 Collection Date: 1/3/215 3:2 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 2-Methylnaphthalene 4-Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1 µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 6 of 7

ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511956 Sample ID: W-1339 Shallow Lab ID: 1511956-5 Collection Date: 1/3/215 3:2 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 99.8 96.9 98.5 11 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 7 of 7

ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant Work Order: 1511956 Date: 11-Nov-15 Case Narrative Batch R175749A The MS/MSD data for volatiles is not related to this project's samples. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Date: 11-Nov-15 Batch ID: R175681 Instrument ID: GC11 Method: SW815M MBLK Sample ID: MB-R175681-R175681 Units: mg/l Client ID: Run ID: GC11_15119A SeqNo: 355486 Analysis Date: 11/9/215 9:16 AM Prep Date: 11/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Ethylene glycol 5. Limit Qual LCS Sample ID: LCS-R175681-R175681 Units: mg/l Client ID: Run ID: GC11_15119A SeqNo: 3554861 Analysis Date: 11/9/215 8:22 AM Prep Date: 11/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol 514.5 5. 5 13 5-15 The following samples were analyzed in this batch: 1511956-5B QC Page: 1 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: 78333 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-78333-78333 Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 355299 Analysis Date: 11/4/215 1:44 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 5. Acenaphthene 5. Acenaphthylene 5. Anthracene 5. Benzo(a)anthracene 5. Benzo(a)pyrene 5. Benzo(b)fluoranthene 5. Benzo(g,h,i)perylene 5. Benzo(k)fluoranthene 5. Chrysene 5. Dibenzo(a,h)anthracene 5. Fluoranthene 5. Fluorene 5. Indeno(1,2,3-cd)pyrene 5. Naphthalene 5. Phenanthrene 5. Pyrene 5. Sulfolane 1 Surr: 2,4,6-Tribromophenol 38.34 5 76.7 38-115 Surr: 2-Fluorobiphenyl 33.61 5 67.2 32-1 Surr: 2-Fluorophenol 21.44 5 42.9 22-59 Surr: 4-Terphenyl-d14 45.15 5 9.3 23-112 Surr: Nitrobenzene-d5 3.44 5 6.9 31-93 Surr: Phenol-d6 12.72 5 25.4 13-36 QC Page: 2 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: 78333 Instrument ID: SVMS8 Method: SW846 827D LCS Sample ID: SLCSW1-78333-78333 Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 3553 Analysis Date: 11/4/215 2:4 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 12.22 5. 2 61.1 45-15 Acenaphthene 13.99 5. 2 7 45-11 Acenaphthylene 14.65 5. 2 73.2 5-15 Anthracene 16.24 5. 2 81.2 55-11 Benzo(a)anthracene 16.3 5. 2 8.2 55-11 Benzo(a)pyrene 16.24 5. 2 81.2 55-11 Benzo(b)fluoranthene 16.53 5. 2 82.6 45-12 Benzo(g,h,i)perylene 17.52 5. 2 87.6 4-125 Benzo(k)fluoranthene 16.44 5. 2 82.2 45-125 Chrysene 15.87 5. 2 79.4 55-11 Dibenzo(a,h)anthracene 17.73 5. 2 88.6 4-125 Fluoranthene 16.43 5. 2 82.2 55-115 Fluorene 14.88 5. 2 74.4 5-11 Indeno(1,2,3-cd)pyrene 17.65 5. 2 88.2 45-125 Naphthalene 11.55 5. 2 57.8 4-1 Phenanthrene 15 5. 2 75 5-115 Pyrene 16.55 5. 2 82.8 5-13 Surr: 2,4,6-Tribromophenol 42.57 5 85.1 38-115 Surr: 2-Fluorobiphenyl 35.36 5 7.7 32-1 Surr: 2-Fluorophenol 21.41 5 42.8 22-59 Surr: 4-Terphenyl-d14 4.43 5 8.9 23-112 Surr: Nitrobenzene-d5 3.85 5 61.7 31-93 Surr: Phenol-d6 13.4 5 26.8 13-36 LCS Sample ID: SLCSW2-78349-78333 Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 35536 Analysis Date: 11/4/215 3:5 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 6.92 1 2 34.6 Surr: 2,4,6-Tribromophenol 38.23 5 76.5 38-115 Surr: 2-Fluorobiphenyl 38.52 5 77 32-1 Surr: 2-Fluorophenol 19.65 5 39.3 22-59 Surr: 4-Terphenyl-d14 46.97 5 93.9 23-112 Surr: Nitrobenzene-d5 32.12 5 64.2 31-93 Surr: Phenol-d6 11.99 5 24 13-36 J QC Page: 3 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: 78333 Instrument ID: SVMS8 Method: SW846 827D LCSD Sample ID: SLCSDW2-78349-78333 Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 35537 Analysis Date: 11/4/215 3:26 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 7.49 1 2 37.4 6.92 Surr: 2,4,6-Tribromophenol 4.79 5 81.6 38-115 38.23 6.48 Surr: 2-Fluorobiphenyl 38.91 5 77.8 32-1 38.52 1.1 Surr: 2-Fluorophenol 2.12 5 4.2 22-59 19.65 2.36 Surr: 4-Terphenyl-d14 49.44 5 98.9 23-112 46.97 5.12 Surr: Nitrobenzene-d5 33.6 5 66.1 31-93 32.12 2.88 Surr: Phenol-d6 12.9 5 24.2 13-36 11.99.831 J MS Sample ID: 151191-2B MS Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 35531 Analysis Date: 11/4/215 6:59 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 388.4 1 4 118.6 67.4 45-15 Acenaphthene 412 1 4 131 7.2 45-11 Acenaphthylene 288.6 1 4 72.2 5-15 Anthracene 334 1 4 1 81 55-11 Benzo(a)anthracene 328.2 1 4 82 55-11 Benzo(a)pyrene 339.8 1 4 85 55-11 Benzo(b)fluoranthene 325.6 1 4 81.4 45-12 Benzo(g,h,i)perylene 35.6 1 4 76.4 4-125 Benzo(k)fluoranthene 324 1 4 81 45-125 Chrysene 311.2 1 4 77.8 55-11 Dibenzo(a,h)anthracene 324.6 1 4 81.2 4-125 Fluoranthene 336.4 1 4 7.4 82.2 55-115 Fluorene 347 1 4 56.8 72.6 5-11 Indeno(1,2,3-cd)pyrene 326 1 4 81.5 45-125 Naphthalene 94.2 1 4 653.4 71.7 4-1 Phenanthrene 399 1 4 88.2 77.7 5-115 Pyrene 283.2 1 4 4.6 69.6 5-13 Surr: 2,4,6-Tribromophenol 832.4 1 83.2 38-115 Surr: 2-Fluorobiphenyl 7.4 1 7 32-1 Surr: 2-Fluorophenol 434.4 1 43.4 22-59 Surr: 4-Terphenyl-d14 676.2 1 67.6 23-112 Surr: Nitrobenzene-d5 643.6 1 64.4 31-93 Surr: Phenol-d6 276.2 1 27.6 13-36 QC Page: 4 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: 78333 Instrument ID: SVMS8 Method: SW846 827D MSD Sample ID: 151191-2B MSD Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 35532 Analysis Date: 11/4/215 7:19 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 377.4 1 4 118.6 64.7 45-15 388.4 2.87 3 Acenaphthene 421.8 1 4 131 72.7 45-11 412 2.35 3 Acenaphthylene 291 1 4 72.8 5-15 288.6.828 3 Anthracene 336.4 1 4 1 81.6 55-11 334.716 3 Benzo(a)anthracene 332.4 1 4 83.1 55-11 328.2 1.27 3 Benzo(a)pyrene 337.4 1 4 84.4 55-11 339.8.79 3 Benzo(b)fluoranthene 33.2 1 4 82.6 45-12 325.6 1.4 3 Benzo(g,h,i)perylene 297.8 1 4 74.4 4-125 35.6 2.59 3 Benzo(k)fluoranthene 317 1 4 79.2 45-125 324 2.18 3 Chrysene 321.2 1 4 8.3 55-11 311.2 3.16 3 Dibenzo(a,h)anthracene 318.2 1 4 79.6 4-125 324.6 1.99 3 Fluoranthene 334.4 1 4 7.4 81.8 55-115 336.4.596 3 Fluorene 351 1 4 56.8 73.6 5-11 347 1.15 3 Indeno(1,2,3-cd)pyrene 316.8 1 4 79.2 45-125 326 2.86 3 Naphthalene 935 1 4 653.4 7.4 4-1 94.2.555 3 Phenanthrene 411.4 1 4 88.2 8.8 5-115 399 3.6 3 Pyrene 284.4 1 4 4.6 7 5-13 283.2.423 3 Surr: 2,4,6-Tribromophenol 856.6 1 85.7 38-115 832.4 2.87 4 Surr: 2-Fluorobiphenyl 698.2 1 69.8 32-1 7.4.315 4 Surr: 2-Fluorophenol 443.6 1 44.4 22-59 434.4 2.1 4 Surr: 4-Terphenyl-d14 67.8 1 67.1 23-112 676.2.82 4 Surr: Nitrobenzene-d5 633 1 63.3 31-93 643.6 1.66 4 Surr: Phenol-d6 277 1 27.7 13-36 276.2.289 4 The following samples were analyzed in this batch: 1511956-1A 1511956-4A 1511956-2A 1511956-5A 1511956-3A QC Page: 5 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B MBLK Sample ID: VBLKW2-15119-R175749A Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: 355683 Prep Date: Analysis Date: 11/9/215 11:42 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 6 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 2.6 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 19.44 2 97.2 75-12 Surr: 4-Bromofluorobenzene 19.26 2 96.3 8-11 Surr: Dibromofluoromethane 18.77 2 93.8 85-115 Surr: Toluene-d8 21.15 2 16 85-11 J QC Page: 7 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B LCS Sample ID: VLCSW2-15119-R175749A Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: 3556829 Prep Date: Analysis Date: 11/9/215 1:5 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 21.5 1. 2 15 8-13 1,1,1-Trichloroethane 19.77 1. 2 98.8 75-13 1,1,2,2-Tetrachloroethane 17.66 1. 2 88.3 75-13 1,1,2-Trichloroethane 19.77 1. 2 98.8 75-125 1,1-Dichloroethane 17.33 1. 2 86.6 75-133 1,1-Dichloroethene 18.63 1. 2 93.2 7-145 1,2,3-Trichloropropane 17.67 1. 2 88.4 75-125 1,2,4-Trichlorobenzene 2.57 1. 2 13 7-135 1,2,4-Trimethylbenzene 19.96 1. 2 99.8 75-13 1,2-Dibromo-3-chloropropane 18.1 1. 2 9.5 6-13 1,2-Dibromoethane 2.62 1. 2 13 8-15 1,2-Dichlorobenzene 2.7 1. 2 1 7-13 1,2-Dichloroethane 2.5 1. 2 1 78-125 1,2-Dichloropropane 18.22 1. 2 91.1 75-125 1,3,5-Trimethylbenzene 2.63 1. 2 13 75-13 1,3-Dichlorobenzene 2.8 1. 2 1 75-13 1,4-Dichlorobenzene 19.44 1. 2 97.2 75-13 2-Butanone 14.19 5. 2 71 55-15 2-Hexanone 18.56 5. 2 92.8 6-135 4-Methyl-2-pentanone 21.44 1. 2 17 77-178 Acetone 15.13 1 2 75.6 6-16 Acrylonitrile 16.1 1. 2 8 6-14 Benzene 19.92 1. 2 99.6 85-125 Bromochloromethane 2.83 1. 2 14 75-13 Bromodichloromethane 19.53 1. 2 97.6 75-125 Bromoform 17.85 1. 2 89.2 6-125 Bromomethane 2.96 1. 2 15 3-185 Carbon disulfide 21.6 1. 2 15 6-165 Carbon tetrachloride 2.12 1. 2 11 65-14 Chlorobenzene 19.83 1. 2 99.2 8-12 Chloroethane 16.44 1. 2 82.2 5-14 Chloroform 16.1 1. 2 8 8-13 Chloromethane 17.87 1. 2 89.4 5-13 cis-1,2-dichloroethene 18.89 1. 2 94.4 75-134 cis-1,3-dichloropropene 2.78 1. 2 14 7-13 Dibromochloromethane 21.7 1. 2 15 6-115 Dibromomethane 17.51 1. 2 87.6 85-125 Dichlorodifluoromethane 16.11 1. 2 8.6 2-12 Ethylbenzene 22.21 1. 2 111 85-125 Hexachloroethane 18.47 1. 2 92.4 5-124 Isopropylbenzene 2.27 1. 2 11 8-127 m,p-xylene 45.45 2. 4 114 75-13 QC Page: 8 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Methyl iodide 19.16 1. 2 95.8 6-16 Methyl tert-butyl ether 17.49 1. 2 87.4 8-13 Methylene chloride 19.6 5. 2 95.3 75-14 Naphthalene 17.6 5. 2 88 55-16 n-propylbenzene 2.48 1. 2 12 78-12 o-xylene 2.77 1. 2 14 8-125 Styrene 19.52 1. 2 97.6 85-125 Tetrachloroethene 23.63 1. 2 118 77-138 Toluene 21.1 1. 2 15 85-125 trans-1,2-dichloroethene 18.45 1. 2 92.2 8-14 trans-1,3-dichloropropene 22.13 1. 2 111 81-123 trans-1,4-dichloro-2-butene 2.39 2. 2 12 46-118 Trichloroethene 19.91 1. 2 99.6 84-13 Trichlorofluoromethane 17.33 1. 2 86.6 6-14 Vinyl chloride 17.73 1. 2 88.6 5-136 Xylenes, Total 66.22 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 19.9 2 99.5 75-12 Surr: 4-Bromofluorobenzene 21.6 2 18 8-11 Surr: Dibromofluoromethane 19.98 2 99.9 85-115 Surr: Toluene-d8 2.77 2 14 85-11 QC Page: 9 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B MS Sample ID: 1511838-4A MS Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: 3556842 Prep Date: Analysis Date: 11/1/215 8:44 A DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 29.5 1 2 15 8-13 1,1,1-Trichloroethane 216.5 1 2 18 75-13 1,1,2,2-Tetrachloroethane 173.7 1 2 86.8 75-13 1,1,2-Trichloroethane 2.2 1 2 1 75-125 1,1-Dichloroethane 185.3 1 2 92.6 75-133 1,1-Dichloroethene 194.9 1 2 97.4 7-145 1,2,3-Trichloropropane 18.1 1 2 9 75-125 1,2,4-Trichlorobenzene 145.6 1 2 72.8 7-135 1,2,4-Trimethylbenzene 211.7 1 2 16 75-13 1,2-Dibromo-3-chloropropane 152.9 1 2 76.4 6-13 1,2-Dibromoethane 27.3 1 2 14 8-15 1,2-Dichlorobenzene 195.1 1 2 97.6 7-13 1,2-Dichloroethane 215.4 1 2 18 78-125 1,2-Dichloropropane 183.9 1 2 92 75-125 1,3,5-Trimethylbenzene 214.6 1 2 17 75-13 1,3-Dichlorobenzene 22.8 1 2 11 75-13 1,4-Dichlorobenzene 194.4 1 2 97.2 75-13 2-Butanone 148.1 5 2 74 55-15 2-Hexanone 178.7 5 2 89.4 6-135 4-Methyl-2-pentanone 22.7 1 2 11 77-178 Acetone 162 1 2 81 6-16 Acrylonitrile 167.6 1 2 83.8 6-14 Benzene 214.5 1 2 17 85-125 Bromochloromethane 26.6 1 2 13 75-13 Bromodichloromethane 24.5 1 2 12 75-125 Bromoform 177.9 1 2 89 6-125 Bromomethane 67.2 1 2 33.6 3-185 Carbon disulfide 224.1 1 2 112 6-165 Carbon tetrachloride 26.8 1 2 13 65-14 Chlorobenzene 21 1 2 15 8-12 Chloroethane 293.7 1 2 147 5-14 Chloroform 17 1 2 85 8-13 Chloromethane 138.2 1 2 69.1 5-13 cis-1,2-dichloroethene 26.4 1 2 13 75-134 cis-1,3-dichloropropene 22.8 1 2 11 7-13 Dibromochloromethane 212.7 1 2 16 6-115 Dibromomethane 18.7 1 2 9.4 85-125 Dichlorodifluoromethane 176.6 1 2 88.3 2-12 Ethylbenzene 223.6 1 2 112 85-125 Hexachloroethane 172.4 1 2 86.2 5-124 Isopropylbenzene 213.1 1 2 17 8-127 m,p-xylene 463.8 2 4 116 75-13 S QC Page: 1 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Methyl iodide 22.7 1 2 11 6-16 Methyl tert-butyl ether 183.7 1 2 91.8 8-13 Methylene chloride 25.1 5 2 13 75-14 Naphthalene 117.5 5 2 58.8 55-16 n-propylbenzene 212.8 1 2 16 78-12 o-xylene 217.6 1 2 19 8-125 Styrene 211.2 1 2 16 85-125 Tetrachloroethene 24.9 1 2 12 77-138 Toluene 222.1 1 2 111 85-125 trans-1,2-dichloroethene 2.3 1 2 1 8-14 trans-1,3-dichloropropene 21.1 1 2 15 81-123 trans-1,4-dichloro-2-butene 237.5 2 2 119 46-118 Trichloroethene 212.6 1 2 16 84-13 Trichlorofluoromethane 196.5 1 2 98.2 6-14 Vinyl chloride 18.8 1 2 9.4 5-136 Xylenes, Total 681.4 3 6 114 8-126 Surr: 1,2-Dichloroethane-d4 197.1 2 98.6 75-12 Surr: 4-Bromofluorobenzene 26.5 2 13 8-11 Surr: Dibromofluoromethane 198.5 2 99.2 85-115 Surr: Toluene-d8 25.7 2 13 85-11 S QC Page: 11 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B MSD Sample ID: 1511838-4A MSD Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: 3556844 Prep Date: Analysis Date: 11/1/215 9:1 A DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 215 1 2 18 8-13 29.5 2.59 3 1,1,1-Trichloroethane 216.8 1 2 18 75-13 216.5.138 3 1,1,2,2-Tetrachloroethane 176.3 1 2 88.2 75-13 173.7 1.49 3 1,1,2-Trichloroethane 21.6 1 2 11 75-125 2.2.697 3 1,1-Dichloroethane 187.3 1 2 93.6 75-133 185.3 1.7 3 1,1-Dichloroethene 196.7 1 2 98.4 7-145 194.9.919 3 1,2,3-Trichloropropane 176.2 1 2 88.1 75-125 18.1 2.19 3 1,2,4-Trichlorobenzene 178.9 1 2 89.4 7-135 145.6 2.5 3 1,2,4-Trimethylbenzene 214.7 1 2 17 75-13 211.7 1.41 3 1,2-Dibromo-3-chloropropane 166.8 1 2 83.4 6-13 152.9 8.7 3 1,2-Dibromoethane 29.3 1 2 15 8-15 27.3.96 3 1,2-Dichlorobenzene 26.9 1 2 13 7-13 195.1 5.87 3 1,2-Dichloroethane 29.6 1 2 15 78-125 215.4 2.73 3 1,2-Dichloropropane 186.5 1 2 93.2 75-125 183.9 1.4 3 1,3,5-Trimethylbenzene 217.2 1 2 19 75-13 214.6 1.2 3 1,3-Dichlorobenzene 212.1 1 2 16 75-13 22.8 4.48 3 1,4-Dichlorobenzene 2.5 1 2 1 75-13 194.4 3.9 3 2-Butanone 139.5 5 2 69.8 55-15 148.1 5.98 3 2-Hexanone 177.9 5 2 89 6-135 178.7.449 3 4-Methyl-2-pentanone 233.4 1 2 117 77-178 22.7 5.59 3 Acetone 147.1 1 2 73.6 6-16 162 9.64 3 Acrylonitrile 162.2 1 2 81.1 6-14 167.6 3.27 3 Benzene 215.4 1 2 18 85-125 214.5.419 3 Bromochloromethane 213.9 1 2 17 75-13 26.6 3.47 3 Bromodichloromethane 27.3 1 2 14 75-125 24.5 1.36 3 Bromoform 186.2 1 2 93.1 6-125 177.9 4.56 3 Bromomethane 82.9 1 2 41.4 3-185 67.2 2.9 3 Carbon disulfide 227 1 2 114 6-165 224.1 1.29 3 Carbon tetrachloride 215.4 1 2 18 65-14 26.8 4.7 3 Chlorobenzene 21.1 1 2 15 8-12 21.476 3 Chloroethane 24.7 1 2 12 5-14 293.7 19.8 3 Chloroform 171.1 1 2 85.6 8-13 17.645 3 Chloromethane 138.8 1 2 69.4 5-13 138.2.433 3 cis-1,2-dichloroethene 197.8 1 2 98.9 75-134 26.4 4.26 3 cis-1,3-dichloropropene 216.8 1 2 18 7-13 22.8 1.83 3 Dibromochloromethane 212.8 1 2 16 6-115 212.7.47 3 Dibromomethane 188.3 1 2 94.2 85-125 18.7 4.12 3 Dichlorodifluoromethane 18.7 1 2 9.4 2-12 176.6 2.29 3 Ethylbenzene 22.6 1 2 11 85-125 223.6 1.35 3 Hexachloroethane 184.3 1 2 92.2 5-124 172.4 6.67 3 Isopropylbenzene 216.9 1 2 18 8-127 213.1 1.77 3 m,p-xylene 461.9 2 4 115 75-13 463.8.411 3 QC Page: 12 of 13

Client: Merit Energy Work Order: 1511956 Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Methyl iodide 278.5 1 2 139 6-16 22.7 23.2 3 Methyl tert-butyl ether 18.4 1 2 9.2 8-13 183.7 1.81 3 Methylene chloride 23.4 5 2 12 75-14 25.1.832 3 Naphthalene 142.6 5 2 71.3 55-16 117.5 19.3 3 n-propylbenzene 218.1 1 2 19 78-12 212.8 2.46 3 o-xylene 219.6 1 2 11 8-125 217.6.915 3 Styrene 211.7 1 2 16 85-125 211.2.236 3 Tetrachloroethene 241.2 1 2 121 77-138 24.9.124 3 Toluene 224.6 1 2 112 85-125 222.1 1.12 3 trans-1,2-dichloroethene 199 1 2 99.5 8-14 2.3.651 3 trans-1,3-dichloropropene 218 1 2 19 81-123 21.1 3.69 3 trans-1,4-dichloro-2-butene 232.7 2 2 116 46-118 237.5 2.4 3 Trichloroethene 211.4 1 2 16 84-13 212.6.566 3 Trichlorofluoromethane 192.9 1 2 96.4 6-14 196.5 1.85 3 Vinyl chloride 175.8 1 2 87.9 5-136 18.8 2.8 3 Xylenes, Total 681.5 3 6 114 8-126 681.4.147 3 Surr: 1,2-Dichloroethane-d4 2.2 2 1 75-12 197.1 1.56 3 Surr: 4-Bromofluorobenzene 23.9 2 12 8-11 26.5 1.27 3 Surr: Dibromofluoromethane 189.5 2 94.8 85-115 198.5 4.64 3 Surr: Toluene-d8 23.8 2 12 85-11 25.7.928 3 The following samples were analyzed in this batch: 1511956-5B QC Page: 13 of 13

ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant WorkOrder: 1511956 Date: 11-Nov-15 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l mg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter Milligrams per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 31-Oct-15 9:3 Work Order: 1511956 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 31-Oct-15 Reviewed by: esignature Date esignature 2-Nov-15 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 4.8/4.8 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 1/31/215 11:11:41 AM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (1339 Lone Tree Rd - Deep) Work Order: 166871 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 9. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Deep) Work Order: 166871 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166871-1 1339 Lone Tree Rd - Deep Water 6/13/216 13:41 6/15/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Deep) Work Order: 166871 Sample ID: 1339 Lone Tree Rd - Deep Lab ID: 166871-1 Collection Date: 6/13/216 1:41 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Sulfolane 1 µg/l 1 6/16/216 11:5 PM Surr: 2,4,6-Tribromophenol 55.2 38-115 %REC 1 6/16/216 11:5 PM Surr: 2-Fluorobiphenyl 58.1 32-1 %REC 1 6/16/216 11:5 PM Surr: 2-Fluorophenol 37.6 22-59 %REC 1 6/16/216 11:5 PM Surr: 4-Terphenyl-d14 85.2 23-112 %REC 1 6/16/216 11:5 PM Surr: Nitrobenzene-d5 65.6 31-93 %REC 1 6/16/216 11:5 PM Surr: Phenol-d6 22.4 13-36 %REC 1 6/16/216 11:5 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166871 Project: ECT (1339 Lone Tree Rd - Deep) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 2

Client: Merit Energy Work Order: 166871 Project: ECT (1339 Lone Tree Rd - Deep) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Client ID: 1339 Lone Tree Rd - Deep Run ID: SVMS8_16616A Units:µg/L SeqNo:3888552 Analysis Date: 6/16/216 1:45 PM Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 166871-1A QC Page: 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Deep) WorkOrder: 166871 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: 166871 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 2:22:34 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (1339 Lone Tree Rd - Shallow) Work Order: 16687 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 9. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Shallow) Work Order: 16687 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 16687-1 1339 Lone Tree Rd - Shallow Water 6/13/216 13:21 6/15/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Shallow) Work Order: 16687 Sample ID: 1339 Lone Tree Rd - Shallow Lab ID: 16687-1 Collection Date: 6/13/216 1:21 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Sulfolane 11 µg/l 1 6/16/216 1:25 PM Surr: 2,4,6-Tribromophenol 71.3 38-115 %REC 1 6/16/216 1:25 PM Surr: 2-Fluorobiphenyl 68.7 32-1 %REC 1 6/16/216 1:25 PM Surr: 2-Fluorophenol 41.4 22-59 %REC 1 6/16/216 1:25 PM Surr: 4-Terphenyl-d14 96.6 23-112 %REC 1 6/16/216 1:25 PM Surr: Nitrobenzene-d5 81.2 31-93 %REC 1 6/16/216 1:25 PM Surr: Phenol-d6 24.1 13-36 %REC 1 6/16/216 1:25 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 16687 Project: ECT (1339 Lone Tree Rd - Shallow) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Client ID: 1339 Lone Tree Rd - Shallow Run ID: SVMS8_16616A Units:µg/L SeqNo:388855 Analysis Date: 6/16/216 1:5 PM Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 2

Client: Merit Energy Work Order: 16687 Project: ECT (1339 Lone Tree Rd - Shallow) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 16687-1A QC Page: 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Shallow) WorkOrder: 16687 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: 16687 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 2:2:41 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (Hartland - 9 Erin Lane) Work Order: 166476 Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: 166476 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166476-1 9 Erin Lane Water 6/7/216 8:36 6/8/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: 166476 Sample ID: 9 Erin Lane Lab ID: 166476-1 Collection Date: 6/7/216 8:36 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 59 µg/l 1 6/9/216 6:56 PM Sulfolane 12 µg/l 1 6/9/216 6:56 PM Surr: 2,4,6-Tribromophenol 61.2 38-115 %REC 1 6/9/216 6:56 PM Surr: 2-Fluorobiphenyl 52.6 32-1 %REC 1 6/9/216 6:56 PM Surr: 2-Fluorophenol 36.5 22-59 %REC 1 6/9/216 6:56 PM Surr: 4-Terphenyl-d14 7.9 23-112 %REC 1 6/9/216 6:56 PM Surr: Nitrobenzene-d5 65.3 31-93 %REC 1 6/9/216 6:56 PM Surr: Phenol-d6 19. 13-36 %REC 1 6/9/216 6:56 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 5:25 AM 1,1-Dichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1-Dichloroethene 1. µg/l 1 6/9/216 5:25 AM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 5:25 AM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 5:25 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 5:25 AM 1,2-Dibromoethane 1. µg/l 1 6/9/216 5:25 AM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 1,2-Dichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,2-Dichloropropane 1. µg/l 1 6/9/216 5:25 AM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 5:25 AM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 2-Butanone 5. µg/l 1 6/9/216 5:25 AM 2-Hexanone 5. µg/l 1 6/9/216 5:25 AM 2-Methylnaphthalene 5. µg/l 1 6/9/216 5:25 AM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 5:25 AM Acetone 1 µg/l 1 6/9/216 5:25 AM Acrylonitrile 1. µg/l 1 6/9/216 5:25 AM Benzene 1. µg/l 1 6/9/216 5:25 AM Bromochloromethane 1. µg/l 1 6/9/216 5:25 AM Bromodichloromethane 1. µg/l 1 6/9/216 5:25 AM Bromoform 1. µg/l 1 6/9/216 5:25 AM Bromomethane 1. µg/l 1 6/9/216 5:25 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: 166476 Sample ID: 9 Erin Lane Lab ID: 166476-1 Collection Date: 6/7/216 8:36 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 93. 95.2 94.4 94.4 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: 166476 Date: 1-Jun-16 Case Narrative Batch R189191a The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo:387197 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 21.75 5 43.5 38-115 Surr: 2-Fluorobiphenyl 21.56 5 43.1 32-1 Surr: 2-Fluorophenol 16.37 5 32.7 22-59 Surr: 4-Terphenyl-d14 35.69 5 71.4 23-112 Surr: Nitrobenzene-d5 28.3 5 56.1 31-93 Surr: Phenol-d6 7.63 5 15.3 13-36 LCS Sample ID: SLCSW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo:387198 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5.75 5 1 5.75 5-4 Sulfolane 54.53 1 1 54.5 3-1 Surr: 2,4,6-Tribromophenol 27.91 5 55.8 38-115 Surr: 2-Fluorobiphenyl 28.51 5 57 32-1 Surr: 2-Fluorophenol 19.32 5 38.6 22-59 Surr: 4-Terphenyl-d14 37.7 5 75.4 23-112 Surr: Nitrobenzene-d5 35.21 5 7.4 31-93 Surr: Phenol-d6 1.2 5 2 13-36 MS Sample ID: 166476-1B MS Client ID: 9 Erin Lane Run ID: SVMS8_1669A Units:µg/L SeqNo:387199 Analysis Date: 6/9/216 6:36 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 53 16.4 13.2 5-4 Sulfolane 65.27 11 16.4 61.4 3-1 Surr: 2,4,6-Tribromophenol 36.5 53.19 67.8 38-115 Surr: 2-Fluorobiphenyl 31.76 53.19 59.7 32-1 Surr: 2-Fluorophenol 2.45 53.19 38.4 22-59 Surr: 4-Terphenyl-d14 38.93 53.19 73.2 23-112 Surr: Nitrobenzene-d5 38.12 53.19 71.7 31-93 Surr: Phenol-d6 1.87 53.19 2.4 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166478-1B DUP Units:µg/L Analysis Date: 6/9/216 7:16 PM Client ID: Run ID: SVMS8_1669A SeqNo:38721 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 32.53 53.2 61.4 38-115 31.66 2.72 4 Surr: 2-Fluorobiphenyl 29.9 53.2 56.4 32-1 27.39 8.78 4 Surr: 2-Fluorophenol 18.87 53.2 35.6 22-59 16.97 1.6 4 Surr: 4-Terphenyl-d14 35.97 53.2 67.8 23-112 37.85 5.9 4 Surr: Nitrobenzene-d5 35.12 53.2 66.2 31-93 32.88 6.59 4 Surr: Phenol-d6 9.3 53.2 17.5 13-36 8.71 6.55 4 The following samples were analyzed in this batch: 166476-1B QC Page: 2 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MBLK Sample ID: VBLKW2-1668-R189191a Units:µg/L Analysis Date: 6/9/216 2:2 AM Client ID: Run ID: VMS6_1668B SeqNo:3868131 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 18.19 2 91 75-12 Surr: 4-Bromofluorobenzene 19.42 2 97.1 8-11 Surr: Dibromofluoromethane 19.84 2 99.2 85-115 Surr: Toluene-d8 19.6 2 95.3 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B LCS Sample ID: VLCSW2-1668-R189191a Units:µg/L Analysis Date: 6/9/216 1:12 AM Client ID: Run ID: VMS6_1668B SeqNo:3868128 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.57 1. 2 13 8-13 1,1,1-Trichloroethane 2.5 1. 2 12 75-13 1,1,2,2-Tetrachloroethane 21.66 1. 2 18 75-13 1,1,2-Trichloroethane 19.85 1. 2 99.2 75-125 1,1-Dichloroethane 19.12 1. 2 95.6 75-133 1,1-Dichloroethene 19.91 1. 2 99.6 7-145 1,2,3-Trichloropropane 2.71 1. 2 14 75-125 1,2,4-Trichlorobenzene 2.9 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.32 1. 2 12 75-13 1,2-Dibromo-3-chloropropane 18.85 1. 2 94.2 6-13 1,2-Dibromoethane 21.31 1. 2 17 8-15 1,2-Dichlorobenzene 2.37 1. 2 12 7-13 1,2-Dichloroethane 18.84 1. 2 94.2 78-125 1,2-Dichloropropane 2.5 1. 2 1 75-125 1,3,5-Trimethylbenzene 2.7 1. 2 14 75-13 1,3-Dichlorobenzene 2.13 1. 2 11 75-13 1,4-Dichlorobenzene 18.8 1. 2 94 75-13 2-Butanone 18.19 5. 2 91 55-15 2-Hexanone 17.68 5. 2 88.4 6-135 4-Methyl-2-pentanone 24.96 1. 2 125 77-178 Acetone 19.47 1 2 97.4 6-16 Acrylonitrile 18.61 1. 2 93 6-14 Benzene 2.49 1. 2 12 85-125 Bromochloromethane 18.44 1. 2 92.2 75-13 Bromodichloromethane 2.1 1. 2 1 75-125 Bromoform 19.96 1. 2 99.8 6-125 Bromomethane 18.62 1. 2 93.1 3-185 Carbon disulfide 2.24 1. 2 11 6-165 Carbon tetrachloride 19.79 1. 2 99 65-14 Chlorobenzene 19.3 1. 2 96.5 8-12 Chloroethane 23.37 1. 2 117 5-14 Chloroform 18.19 1. 2 91 8-13 Chloromethane 15.16 1. 2 75.8 5-13 cis-1,2-dichloroethene 17.74 1. 2 88.7 75-134 cis-1,3-dichloropropene 2.29 1. 2 11 7-13 Dibromochloromethane 19.2 1. 2 95.1 6-115 Dibromomethane 2.48 1. 2 12 85-125 Dichlorodifluoromethane 19.67 1. 2 98.4 2-12 Ethylbenzene 19.65 1. 2 98.2 85-125 Hexachloroethane 15.39 1. 2 77 5-124 Isopropylbenzene 2.62 1. 2 13 8-127 m,p-xylene 4.98 2. 4 12 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 12.7 1. 2 63.5 6-16 Methyl tert-butyl ether 18 1. 2 9 8-13 Methylene chloride 17.88 5. 2 89.4 75-14 Naphthalene 21.87 5. 2 19 55-16 n-propylbenzene 2.14 1. 2 11 78-12 o-xylene 19.28 1. 2 96.4 8-125 Styrene 21.3 1. 2 15 85-125 Tetrachloroethene 2.34 1. 2 12 77-138 Toluene 19.4 1. 2 97 85-125 trans-1,2-dichloroethene 18.95 1. 2 94.8 8-14 trans-1,3-dichloropropene 16.82 1. 2 84.1 81-123 trans-1,4-dichloro-2-butene 12.14 2. 2 6.7 46-118 Trichloroethene 2.81 1. 2 14 84-13 Trichlorofluoromethane 19.62 1. 2 98.1 6-14 Vinyl chloride 19.82 1. 2 99.1 5-136 Xylenes, Total 6.26 3. 6 1 8-126 Surr: 1,2-Dichloroethane-d4 17.86 2 89.3 75-12 Surr: 4-Bromofluorobenzene 2.13 2 11 8-11 Surr: Dibromofluoromethane 19.75 2 98.8 85-115 Surr: Toluene-d8 18.98 2 94.9 85-11 QC Page: 6 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MS Sample ID: 16641-15A MS Units:µg/L Analysis Date: 6/9/216 1:53 AM Client ID: Run ID: VMS6_1668B SeqNo:3868146 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 227 1 2 11 8-13 1,1,1-Trichloroethane 2176 1 2 19 75-13 1,1,2,2-Tetrachloroethane 298 1 2 15 75-13 1,1,2-Trichloroethane 1988 1 2 99.4 75-125 1,1-Dichloroethane 272 1 2 14 75-133 1,1-Dichloroethene 2225 1 2 111 7-145 1,2,3-Trichloropropane 1968 1 2 98.4 75-125 1,2,4-Trichlorobenzene 1814 1 2 9.7 7-135 1,2,4-Trimethylbenzene 3856 1 2 1781 14 75-13 1,2-Dibromo-3-chloropropane 1598 1 2 79.9 6-13 1,2-Dibromoethane 229 1 2 11 8-15 1,2-Dichlorobenzene 1913 1 2 95.6 7-13 1,2-Dichloroethane 1936 1 2 96.8 78-125 1,2-Dichloropropane 224 1 2 11 75-125 1,3,5-Trimethylbenzene 2485 1 2 44 12 75-13 1,3-Dichlorobenzene 1859 1 2 93 75-13 1,4-Dichlorobenzene 1771 1 2 88.6 75-13 2-Butanone 1554 5 2 77.7 55-15 2-Hexanone 168 5 2 84 6-135 4-Methyl-2-pentanone 2333 1 2 117 77-178 Acetone 2157 1, 2 18 6-16 Acrylonitrile 161 1 2 8.5 6-14 Benzene 151 1 2 7878 132 85-125 Bromochloromethane 1882 1 2 94.1 75-13 Bromodichloromethane 1999 1 2 1 75-125 Bromoform 181 1 2 9 6-125 Bromomethane 787 1 2 39.4 3-185 Carbon disulfide 25 1 2 1 6-165 Carbon tetrachloride 257 1 2 13 65-14 Chlorobenzene 1989 1 2 99.4 8-12 Chloroethane 3158 1 2 158 5-14 Chloroform 1881 1 2 94 8-13 Chloromethane 144 1 2 72 5-13 cis-1,2-dichloroethene 1836 1 2 91.8 75-134 cis-1,3-dichloropropene 1983 1 2 99.2 7-13 Dibromochloromethane 1793 1 2 89.6 6-115 Dibromomethane 27 1 2 14 85-125 Dichlorodifluoromethane 265 1 2 13 2-12 Ethylbenzene 424 1 2 2217 11 85-125 Hexachloroethane 1383 1 2 69.2 5-124 Isopropylbenzene 2155 1 2 9 13 8-127 m,p-xylene 1212 2 4 8137 99.5 75-13 SE S QC Page: 7 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 713 1 2 35.6 6-16 Methyl tert-butyl ether 1823 1 2 91.2 8-13 Methylene chloride 196 5 2 95.3 75-14 Naphthalene 23 5 2 372 96.4 55-16 n-propylbenzene 2251 1 2 243 1 78-12 o-xylene 5588 1 2 3675 95.6 8-125 Styrene 22 1 2 11 85-125 Tetrachloroethene 263 1 2 13 77-138 Toluene 1167 1 2 9459 111 85-125 trans-1,2-dichloroethene 235 1 2 12 8-14 trans-1,3-dichloropropene 158 1 2 79 81-123 trans-1,4-dichloro-2-butene 184 2 2 54.2 46-118 Trichloroethene 2218 1 2 111 84-13 Trichlorofluoromethane 2239 1 2 112 6-14 Vinyl chloride 2122 1 2 16 5-136 Xylenes, Total 1771 3 6 1181 98.2 8-126 Surr: 1,2-Dichloroethane-d4 1818 2 9.9 75-12 Surr: 4-Bromofluorobenzene 211 2 11 8-11 Surr: Dibromofluoromethane 194 2 97 85-115 Surr: Toluene-d8 1912 2 95.6 85-11 S EO S QC Page: 8 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MSD Sample ID: 16641-15A MSD Units:µg/L Analysis Date: 6/9/216 11:18 AM Client ID: Run ID: VMS6_1668B SeqNo:3868147 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2 1 2 1 8-13 227 1.34 3 1,1,1-Trichloroethane 294 1 2 15 75-13 2176 3.84 3 1,1,2,2-Tetrachloroethane 228 1 2 11 75-13 298 3.39 3 1,1,2-Trichloroethane 1862 1 2 93.1 75-125 1988 6.55 3 1,1-Dichloroethane 1943 1 2 97.2 75-133 272 6.43 3 1,1-Dichloroethene 2156 1 2 18 7-145 2225 3.15 3 1,2,3-Trichloropropane 1869 1 2 93.4 75-125 1968 5.16 3 1,2,4-Trichlorobenzene 1877 1 2 93.8 7-135 1814 3.41 3 1,2,4-Trimethylbenzene 552 1 2 1781 186 75-13 3856 35.2 3 1,2-Dibromo-3-chloropropane 1518 1 2 75.9 6-13 1598 5.13 3 1,2-Dibromoethane 196 1 2 98 8-15 229 3.46 3 1,2-Dichlorobenzene 1939 1 2 97 7-13 1913 1.35 3 1,2-Dichloroethane 1818 1 2 9.9 78-125 1936 6.29 3 1,2-Dichloropropane 1959 1 2 98 75-125 224 3.26 3 1,3,5-Trimethylbenzene 2975 1 2 44 127 75-13 2485 17.9 3 1,3-Dichlorobenzene 1918 1 2 95.9 75-13 1859 3.12 3 1,4-Dichlorobenzene 1834 1 2 91.7 75-13 1771 3.5 3 2-Butanone 161 5 2 8.5 55-15 1554 3.54 3 2-Hexanone 167 5 2 8.4 6-135 168 4.44 3 4-Methyl-2-pentanone 223 1 2 112 77-178 2333 4.51 3 Acetone 228 1, 2 11 6-16 2157 2.34 3 Acrylonitrile 1516 1 2 75.8 6-14 161 6.1 3 Benzene 1775 1 2 7878 494 85-125 151 51.3 3 Bromochloromethane 18 1 2 9 75-13 1882 4.45 3 Bromodichloromethane 191 1 2 95.5 75-125 1999 4.55 3 Bromoform 1729 1 2 86.4 6-125 181 4.8 3 Bromomethane 146 1 2 73 3-185 787 59.9 3 Carbon disulfide 213 1 2 11 6-165 25.398 3 Carbon tetrachloride 289 1 2 14 65-14 257 1.54 3 Chlorobenzene 1936 1 2 96.8 8-12 1989 2.7 3 Chloroethane 2892 1 2 145 5-14 3158 8.79 3 Chloroform 1862 1 2 93.1 8-13 1881 1.2 3 Chloromethane 1275 1 2 63.8 5-13 144 12.2 3 cis-1,2-dichloroethene 1769 1 2 88.4 75-134 1836 3.72 3 cis-1,3-dichloropropene 1916 1 2 95.8 7-13 1983 3.44 3 Dibromochloromethane 1762 1 2 88.1 6-115 1793 1.74 3 Dibromomethane 1897 1 2 94.8 85-125 27 8.72 3 Dichlorodifluoromethane 234 1 2 12 2-12 265 1.51 3 Ethylbenzene 6328 1 2 2217 26 85-125 424 39.5 3 Hexachloroethane 1523 1 2 76.2 5-124 1383 9.64 3 Isopropylbenzene 2275 1 2 9 19 8-127 2155 5.42 3 m,p-xylene 1918 2 4 8137 276 75-13 1212 45.1 3 SR SRE R S SR SR QC Page: 9 of 1

Client: Merit Energy Work Order: 166476 Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 98 1 2 49 6-16 713 31.5 3 Methyl tert-butyl ether 1779 1 2 89 8-13 1823 2.44 3 Methylene chloride 1788 5 2 89.4 75-14 196 6.39 3 Naphthalene 2618 5 2 372 112 55-16 23 12.9 3 n-propylbenzene 2511 1 2 243 113 78-12 2251 1.9 3 o-xylene 892 1 2 3675 261 8-125 5588 45.7 3 Styrene 2316 1 2 116 85-125 22 5.14 3 Tetrachloroethene 214 1 2 15 77-138 263 1.97 3 Toluene 1991 1 2 9459 522 85-125 1167 52.1 3 trans-1,2-dichloroethene 1963 1 2 98.2 8-14 235 3.6 3 trans-1,3-dichloropropene 1519 1 2 76 81-123 158 3.94 3 trans-1,4-dichloro-2-butene 12 2 2 51 46-118 184 6.8 3 Trichloroethene 2147 1 2 17 84-13 2218 3.25 3 Trichlorofluoromethane 2213 1 2 111 6-14 2239 1.17 3 Vinyl chloride 1987 1 2 99.4 5-136 2122 6.57 3 Xylenes, Total 288 3 6 1181 271 8-126 1771 45.3 3 Surr: 1,2-Dichloroethane-d4 1793 2 89.6 75-12 1818 1.38 3 Surr: 4-Bromofluorobenzene 211 2 11 8-11 211 3 Surr: Dibromofluoromethane 1965 2 98.2 85-115 194 1.28 3 Surr: Toluene-d8 1896 2 94.8 85-11 1912.84 3 SR SR SREO S SR The following samples were analyzed in this batch: 166476-1A QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) WorkOrder: 166476 Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: 166476 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 3.6/3.6 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:32:23 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (9 Erin Lane Pole Building) Work Order: 16693 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 1: AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 18. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: 16693 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 16693-1 9 Erin Lane Pole Building Water 6/14/216 8:25 6/15/216 1: Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: 16693 Sample ID: 9 Erin Lane Pole Building Lab ID: 16693-1 Collection Date: 6/14/216 8:25 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 59 µg/l 1 6/17/216 3:28 AM Sulfolane 12 µg/l 1 6/17/216 3:28 AM Surr: 2,4,6-Tribromophenol 58.7 38-115 %REC 1 6/17/216 3:28 AM Surr: 2-Fluorobiphenyl 56.9 32-1 %REC 1 6/17/216 3:28 AM Surr: 2-Fluorophenol 41. 22-59 %REC 1 6/17/216 3:28 AM Surr: 4-Terphenyl-d14 87.8 23-112 %REC 1 6/17/216 3:28 AM Surr: Nitrobenzene-d5 63.4 31-93 %REC 1 6/17/216 3:28 AM Surr: Phenol-d6 25. 13-36 %REC 1 6/17/216 3:28 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 6:42 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 6:42 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 6:42 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 6:42 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 6:42 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 6:42 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 6:42 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 6:42 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 2-Butanone 5. µg/l 1 6/21/216 6:42 PM 2-Hexanone 5. µg/l 1 6/21/216 6:42 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 6:42 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 6:42 PM Acetone 1 µg/l 1 6/21/216 6:42 PM Acrylonitrile 1. µg/l 1 6/21/216 6:42 PM Benzene 1. µg/l 1 6/21/216 6:42 PM Bromochloromethane 1. µg/l 1 6/21/216 6:42 PM Bromodichloromethane 1. µg/l 1 6/21/216 6:42 PM Bromoform 1. µg/l 1 6/21/216 6:42 PM Bromomethane 1. µg/l 1 6/21/216 6:42 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: 16693 Sample ID: 9 Erin Lane Pole Building Lab ID: 16693-1 Collection Date: 6/14/216 8:25 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 111 89. 18 93. 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: 16693 Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW2-16621 The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 1.77 5 1 1.8 1-5 Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 18.58 5 1 18.6 1-5 Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 16693-1A QC Page: 2 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-16621-R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo:388617 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 21.46 2 17 75-12 Surr: 4-Bromofluorobenzene 17.99 2 9 8-11 Surr: Dibromofluoromethane 2.43 2 12 85-115 Surr: Toluene-d8 18.84 2 94.2 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW2-16621-R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo:3886169 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.57 1. 2 97.8 8-13 1,1,1-Trichloroethane 22.55 1. 2 113 75-13 1,1,2,2-Tetrachloroethane 18.67 1. 2 93.4 75-13 1,1,2-Trichloroethane 19.87 1. 2 99.4 75-125 1,1-Dichloroethane 21.59 1. 2 18 75-133 1,1-Dichloroethene 24.6 1. 2 123 7-145 1,2,3-Trichloropropane 18.99 1. 2 95 75-125 1,2,4-Trichlorobenzene 2.1 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.83 1. 2 14 75-13 1,2-Dibromo-3-chloropropane 14.85 1. 2 74.2 6-13 1,2-Dibromoethane 21.69 1. 2 18 8-15 1,2-Dichlorobenzene 2.68 1. 2 13 7-13 1,2-Dichloroethane 2.77 1. 2 14 78-125 1,2-Dichloropropane 19.91 1. 2 99.6 75-125 1,3,5-Trimethylbenzene 21.2 1. 2 16 75-13 1,3-Dichlorobenzene 21.55 1. 2 18 75-13 1,4-Dichlorobenzene 2.77 1. 2 14 75-13 2-Butanone 13.56 5. 2 67.8 55-15 2-Hexanone 13.16 5. 2 65.8 6-135 4-Methyl-2-pentanone 17.41 1. 2 87 77-178 Acetone 15.96 1 2 79.8 6-16 Acrylonitrile 15.7 1. 2 78.5 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 18.78 1. 2 93.9 75-13 Bromodichloromethane 2.47 1. 2 12 75-125 Bromoform 16.14 1. 2 8.7 6-125 Bromomethane 27.29 1. 2 136 3-185 Carbon disulfide 22.57 1. 2 113 6-165 Carbon tetrachloride 21.1 1. 2 15 65-14 Chlorobenzene 2.84 1. 2 14 8-12 Chloroethane 23.14 1. 2 116 5-14 Chloroform 19.86 1. 2 99.3 8-13 Chloromethane 14.87 1. 2 74.4 5-13 cis-1,2-dichloroethene 19.63 1. 2 98.2 75-134 cis-1,3-dichloropropene 17.96 1. 2 89.8 7-13 Dibromochloromethane 16.62 1. 2 83.1 6-115 Dibromomethane 2.68 1. 2 13 85-125 Dichlorodifluoromethane 18.35 1. 2 91.8 2-12 Ethylbenzene 21.52 1. 2 18 85-125 Hexachloroethane 14.16 1. 2 7.8 5-124 Isopropylbenzene 2.7 1. 2 14 8-127 m,p-xylene 44.74 2. 4 112 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 4.55 1. 2 23 6-16 Methyl tert-butyl ether 17.94 1. 2 89.7 8-13 Methylene chloride 23.38 5. 2 117 75-14 Naphthalene 16.24 5. 2 81.2 55-16 n-propylbenzene 22.3 1. 2 11 78-12 o-xylene 21.56 1. 2 18 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 22.69 1. 2 113 77-138 Toluene 2.43 1. 2 12 85-125 trans-1,2-dichloroethene 22.8 1. 2 114 8-14 trans-1,3-dichloropropene 16.34 1. 2 81.7 81-123 trans-1,4-dichloro-2-butene 12.84 2. 2 64.2 46-118 Trichloroethene 21.85 1. 2 19 84-13 Trichlorofluoromethane 22.88 1. 2 114 6-14 Vinyl chloride 2.66 1. 2 13 5-136 Xylenes, Total 66.3 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 2.4 2 1 75-12 Surr: 4-Bromofluorobenzene 2.4 2 1 8-11 Surr: Dibromofluoromethane 2.8 2 14 85-115 Surr: Toluene-d8 19.65 2 98.2 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: 166757-21A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo:3886188 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.8 1. 2 1 8-13 1,1,1-Trichloroethane 24.12 1. 2 121 75-13 1,1,2,2-Tetrachloroethane 19.35 1. 2 96.8 75-13 1,1,2-Trichloroethane 2.4 1. 2 12 75-125 1,1-Dichloroethane 2.94 1. 2 15 75-133 1,1-Dichloroethene 25.13 1. 2 126 7-145 1,2,3-Trichloropropane 2.1 1. 2 1 75-125 1,2,4-Trichlorobenzene 19.27 1. 2 96.4 7-135 1,2,4-Trimethylbenzene 2.24 1. 2 11 75-13 1,2-Dibromo-3-chloropropane 15.52 1. 2 77.6 6-13 1,2-Dibromoethane 22.21 1. 2 111 8-15 1,2-Dichlorobenzene 2.36 1. 2 12 7-13 1,2-Dichloroethane 21.3 1. 2 15 78-125 1,2-Dichloropropane 2.59 1. 2 13 75-125 1,3,5-Trimethylbenzene 2.68 1. 2 13 75-13 1,3-Dichlorobenzene 2.95 1. 2 15 75-13 1,4-Dichlorobenzene 2.1 1. 2 1 75-13 2-Butanone 13.96 5. 2 69.8 55-15 2-Hexanone 14.2 5. 2 7.1 6-135 4-Methyl-2-pentanone 18.6 1. 2 93 77-178 Acetone 2.81 1 2 14 6-16 Acrylonitrile 18.32 1. 2 91.6 6-14 Benzene 65.38 1. 2 45.14 11 85-125 Bromochloromethane 18.68 1. 2 93.4 75-13 Bromodichloromethane 21.4 1. 2 15 75-125 Bromoform 16.63 1. 2 83.2 6-125 Bromomethane 14.6 1. 2 7.3 3-185 Carbon disulfide 22.31 1. 2 112 6-165 Carbon tetrachloride 22.91 1. 2 115 65-14 Chlorobenzene 2.68 1. 2 13 8-12 Chloroethane 23.54 1. 2 118 5-14 Chloroform 2.4 1. 2 1 8-13 Chloromethane 21.19 1. 2 1.5 98.4 5-13 cis-1,2-dichloroethene 19.3 1. 2 96.5 75-134 cis-1,3-dichloropropene 17.49 1. 2 87.4 7-13 Dibromochloromethane 16.89 1. 2 84.4 6-115 Dibromomethane 21.31 1. 2 17 85-125 Dichlorodifluoromethane 19.6 1. 2 95.3 2-12 Ethylbenzene 21.13 1. 2 16 85-125 Hexachloroethane 14.2 1. 2 71 5-124 Isopropylbenzene 2.54 1. 2 13 8-127 m,p-xylene 44.6 2. 4 112 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 19.62 1. 2 98.1 6-16 Methyl tert-butyl ether 18.2 1. 2 9.1 8-13 Methylene chloride 22.17 5. 2 111 75-14 Naphthalene 18.34 5. 2 1.74 83 55-16 n-propylbenzene 21.51 1. 2 18 78-12 o-xylene 21.8 1. 2 15 8-125 Styrene 14.3 1. 2 7.2 85-125 Tetrachloroethene 21.58 1. 2 18 77-138 Toluene 2.49 1. 2 12 85-125 trans-1,2-dichloroethene 22.23 1. 2 111 8-14 trans-1,3-dichloropropene 16.8 1. 2 8.4 81-123 trans-1,4-dichloro-2-butene 13.7 2. 2 65.4 46-118 Trichloroethene 21.75 1. 2 19 84-13 Trichlorofluoromethane 24.38 1. 2 122 6-14 Vinyl chloride 21.25 1. 2 16 5-136 Xylenes, Total 65.68 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 2.55 2 13 75-12 Surr: 4-Bromofluorobenzene 2.61 2 13 8-11 Surr: Dibromofluoromethane 21.2 2 16 85-115 Surr: Toluene-d8 19.69 2 98.4 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: 166757-21A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo:3886189 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.66 1. 2 98.3 8-13 2.8 2.11 3 1,1,1-Trichloroethane 23.81 1. 2 119 75-13 24.12 1.29 3 1,1,2,2-Tetrachloroethane 19.8 1. 2 95.4 75-13 19.35 1.41 3 1,1,2-Trichloroethane 19.61 1. 2 98 75-125 2.4 3.95 3 1,1-Dichloroethane 21.5 1. 2 15 75-133 2.94.524 3 1,1-Dichloroethene 25.19 1. 2 126 7-145 25.13.238 3 1,2,3-Trichloropropane 19.29 1. 2 96.4 75-125 2.1 4.11 3 1,2,4-Trichlorobenzene 18.79 1. 2 94 7-135 19.27 2.52 3 1,2,4-Trimethylbenzene 19.71 1. 2 98.6 75-13 2.24 2.65 3 1,2-Dibromo-3-chloropropane 15.21 1. 2 76 6-13 15.52 2.2 3 1,2-Dibromoethane 21.21 1. 2 16 8-15 22.21 4.61 3 1,2-Dichlorobenzene 19.89 1. 2 99.4 7-13 2.36 2.34 3 1,2-Dichloroethane 21.9 1. 2 15 78-125 21.3.285 3 1,2-Dichloropropane 2.26 1. 2 11 75-125 2.59 1.62 3 1,3,5-Trimethylbenzene 2.21 1. 2 11 75-13 2.68 2.3 3 1,3-Dichlorobenzene 2.53 1. 2 13 75-13 2.95 2.3 3 1,4-Dichlorobenzene 19.81 1. 2 99 75-13 2.1 1 3 2-Butanone 13.91 5. 2 69.6 55-15 13.96.359 3 2-Hexanone 13.95 5. 2 69.8 6-135 14.2.51 3 4-Methyl-2-pentanone 17.36 1. 2 86.8 77-178 18.6 6.9 3 Acetone 22.34 1 2 112 6-16 2.81 7.9 3 Acrylonitrile 15.86 1. 2 79.3 6-14 18.32 14.4 3 Benzene 64.83 1. 2 45.14 98.4 85-125 65.38.845 3 Bromochloromethane 18.4 1. 2 9.2 75-13 18.68 3.49 3 Bromodichloromethane 21.13 1. 2 16 75-125 21.4.427 3 Bromoform 16.78 1. 2 83.9 6-125 16.63.898 3 Bromomethane 15.82 1. 2 79.1 3-185 14.6 11.8 3 Carbon disulfide 22.62 1. 2 113 6-165 22.31 1.38 3 Carbon tetrachloride 22.97 1. 2 115 65-14 22.91.262 3 Chlorobenzene 2.33 1. 2 12 8-12 2.68 1.71 3 Chloroethane 23.5 1. 2 115 5-14 23.54 2.1 3 Chloroform 19.83 1. 2 99.2 8-13 2.4 1.5 3 Chloromethane 19.88 1. 2 1.5 91.9 5-13 21.19 6.38 3 cis-1,2-dichloroethene 19.14 1. 2 95.7 75-134 19.3.832 3 cis-1,3-dichloropropene 17.82 1. 2 89.1 7-13 17.49 1.87 3 Dibromochloromethane 16.93 1. 2 84.6 6-115 16.89.237 3 Dibromomethane 21.7 1. 2 15 85-125 21.31 1.13 3 Dichlorodifluoromethane 18.73 1. 2 93.6 2-12 19.6 1.75 3 Ethylbenzene 2.69 1. 2 13 85-125 21.13 2.1 3 Hexachloroethane 14.63 1. 2 73.2 5-124 14.2 2.98 3 Isopropylbenzene 2.21 1. 2 11 8-127 2.54 1.62 3 m,p-xylene 43.56 2. 4 19 75-13 44.6 2.36 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 16693 Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 11.22 1. 2 56.1 6-16 19.62 54.5 3 Methyl tert-butyl ether 17.21 1. 2 86 8-13 18.2 4.6 3 Methylene chloride 2.8 5. 2 14 75-14 22.17 6.38 3 Naphthalene 17.29 5. 2 1.74 77.8 55-16 18.34 5.89 3 n-propylbenzene 21.2 1. 2 15 78-12 21.51 2.3 3 o-xylene 2.71 1. 2 14 8-125 21.8 1.77 3 Styrene 13.72 1. 2 68.6 85-125 14.3 2.23 3 Tetrachloroethene 21 1. 2 15 77-138 21.58 2.72 3 Toluene 2.34 1. 2 12 85-125 2.49.735 3 trans-1,2-dichloroethene 21.22 1. 2 16 8-14 22.23 4.65 3 trans-1,3-dichloropropene 15.7 1. 2 78.5 81-123 16.8 2.39 3 trans-1,4-dichloro-2-butene 12.81 2. 2 64 46-118 13.7 2.1 3 Trichloroethene 21.54 1. 2 18 84-13 21.75.97 3 Trichlorofluoromethane 23.82 1. 2 119 6-14 24.38 2.32 3 Vinyl chloride 2.97 1. 2 15 5-136 21.25 1.33 3 Xylenes, Total 64.27 3. 6 17 8-126 65.68 2.17 3 Surr: 1,2-Dichloroethane-d4 2.59 2 13 75-12 2.55.194 3 Surr: 4-Bromofluorobenzene 2.65 2 13 8-11 2.61.194 3 Surr: Dibromofluoromethane 21.9 2 15 85-115 21.2.52 3 Surr: Toluene-d8 19.75 2 98.8 85-11 19.69.34 3 SR S S The following samples were analyzed in this batch: 16693-1B QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) WorkOrder: 16693 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 1: Work Order: 16693 Received by: MEB Checklist completed by Meghan Broadbent Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: water Carrier name: UPS 16-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 6./6. SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 4:35:37 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (139 Cherry Blossom) Work Order: 166887 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: 166887 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166887-1 139 Cherry Blossom Water 6/13/216 17:39 6/15/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: 166887 Sample ID: 139 Cherry Blossom Lab ID: 166887-1 Collection Date: 6/13/216 5:39 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 53 µg/l 1 6/17/216 2:47 AM Sulfolane 11 µg/l 1 6/17/216 2:47 AM Surr: 2,4,6-Tribromophenol 56.7 38-115 %REC 1 6/17/216 2:47 AM Surr: 2-Fluorobiphenyl 53.3 32-1 %REC 1 6/17/216 2:47 AM Surr: 2-Fluorophenol 36.9 22-59 %REC 1 6/17/216 2:47 AM Surr: 4-Terphenyl-d14 84.1 23-112 %REC 1 6/17/216 2:47 AM Surr: Nitrobenzene-d5 6.4 31-93 %REC 1 6/17/216 2:47 AM Surr: Phenol-d6 22.4 13-36 %REC 1 6/17/216 2:47 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 5:54 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 5:54 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 5:54 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 5:54 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 5:54 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 5:54 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 5:54 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 5:54 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 2-Butanone 5. µg/l 1 6/21/216 5:54 PM 2-Hexanone 5. µg/l 1 6/21/216 5:54 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 5:54 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 5:54 PM Acetone 1 µg/l 1 6/21/216 5:54 PM Acrylonitrile 1. µg/l 1 6/21/216 5:54 PM Benzene 1. µg/l 1 6/21/216 5:54 PM Bromochloromethane 1. µg/l 1 6/21/216 5:54 PM Bromodichloromethane 1. µg/l 1 6/21/216 5:54 PM Bromoform 1. µg/l 1 6/21/216 5:54 PM Bromomethane 1. µg/l 1 6/21/216 5:54 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: 166887 Sample ID: 139 Cherry Blossom Lab ID: 166887-1 Collection Date: 6/13/216 5:39 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 111 9.1 16 94.2 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: 166887 Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW2-16621 The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 1.77 5 1 1.8 1-5 Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 18.58 5 1 18.6 1-5 Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 166887-1A QC Page: 2 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-16621-R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo:388617 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 21.46 2 17 75-12 Surr: 4-Bromofluorobenzene 17.99 2 9 8-11 Surr: Dibromofluoromethane 2.43 2 12 85-115 Surr: Toluene-d8 18.84 2 94.2 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW2-16621-R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo:3886169 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.57 1. 2 97.8 8-13 1,1,1-Trichloroethane 22.55 1. 2 113 75-13 1,1,2,2-Tetrachloroethane 18.67 1. 2 93.4 75-13 1,1,2-Trichloroethane 19.87 1. 2 99.4 75-125 1,1-Dichloroethane 21.59 1. 2 18 75-133 1,1-Dichloroethene 24.6 1. 2 123 7-145 1,2,3-Trichloropropane 18.99 1. 2 95 75-125 1,2,4-Trichlorobenzene 2.1 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.83 1. 2 14 75-13 1,2-Dibromo-3-chloropropane 14.85 1. 2 74.2 6-13 1,2-Dibromoethane 21.69 1. 2 18 8-15 1,2-Dichlorobenzene 2.68 1. 2 13 7-13 1,2-Dichloroethane 2.77 1. 2 14 78-125 1,2-Dichloropropane 19.91 1. 2 99.6 75-125 1,3,5-Trimethylbenzene 21.2 1. 2 16 75-13 1,3-Dichlorobenzene 21.55 1. 2 18 75-13 1,4-Dichlorobenzene 2.77 1. 2 14 75-13 2-Butanone 13.56 5. 2 67.8 55-15 2-Hexanone 13.16 5. 2 65.8 6-135 4-Methyl-2-pentanone 17.41 1. 2 87 77-178 Acetone 15.96 1 2 79.8 6-16 Acrylonitrile 15.7 1. 2 78.5 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 18.78 1. 2 93.9 75-13 Bromodichloromethane 2.47 1. 2 12 75-125 Bromoform 16.14 1. 2 8.7 6-125 Bromomethane 27.29 1. 2 136 3-185 Carbon disulfide 22.57 1. 2 113 6-165 Carbon tetrachloride 21.1 1. 2 15 65-14 Chlorobenzene 2.84 1. 2 14 8-12 Chloroethane 23.14 1. 2 116 5-14 Chloroform 19.86 1. 2 99.3 8-13 Chloromethane 14.87 1. 2 74.4 5-13 cis-1,2-dichloroethene 19.63 1. 2 98.2 75-134 cis-1,3-dichloropropene 17.96 1. 2 89.8 7-13 Dibromochloromethane 16.62 1. 2 83.1 6-115 Dibromomethane 2.68 1. 2 13 85-125 Dichlorodifluoromethane 18.35 1. 2 91.8 2-12 Ethylbenzene 21.52 1. 2 18 85-125 Hexachloroethane 14.16 1. 2 7.8 5-124 Isopropylbenzene 2.7 1. 2 14 8-127 m,p-xylene 44.74 2. 4 112 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 4.55 1. 2 23 6-16 Methyl tert-butyl ether 17.94 1. 2 89.7 8-13 Methylene chloride 23.38 5. 2 117 75-14 Naphthalene 16.24 5. 2 81.2 55-16 n-propylbenzene 22.3 1. 2 11 78-12 o-xylene 21.56 1. 2 18 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 22.69 1. 2 113 77-138 Toluene 2.43 1. 2 12 85-125 trans-1,2-dichloroethene 22.8 1. 2 114 8-14 trans-1,3-dichloropropene 16.34 1. 2 81.7 81-123 trans-1,4-dichloro-2-butene 12.84 2. 2 64.2 46-118 Trichloroethene 21.85 1. 2 19 84-13 Trichlorofluoromethane 22.88 1. 2 114 6-14 Vinyl chloride 2.66 1. 2 13 5-136 Xylenes, Total 66.3 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 2.4 2 1 75-12 Surr: 4-Bromofluorobenzene 2.4 2 1 8-11 Surr: Dibromofluoromethane 2.8 2 14 85-115 Surr: Toluene-d8 19.65 2 98.2 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: 166757-21A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo:3886188 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.8 1. 2 1 8-13 1,1,1-Trichloroethane 24.12 1. 2 121 75-13 1,1,2,2-Tetrachloroethane 19.35 1. 2 96.8 75-13 1,1,2-Trichloroethane 2.4 1. 2 12 75-125 1,1-Dichloroethane 2.94 1. 2 15 75-133 1,1-Dichloroethene 25.13 1. 2 126 7-145 1,2,3-Trichloropropane 2.1 1. 2 1 75-125 1,2,4-Trichlorobenzene 19.27 1. 2 96.4 7-135 1,2,4-Trimethylbenzene 2.24 1. 2 11 75-13 1,2-Dibromo-3-chloropropane 15.52 1. 2 77.6 6-13 1,2-Dibromoethane 22.21 1. 2 111 8-15 1,2-Dichlorobenzene 2.36 1. 2 12 7-13 1,2-Dichloroethane 21.3 1. 2 15 78-125 1,2-Dichloropropane 2.59 1. 2 13 75-125 1,3,5-Trimethylbenzene 2.68 1. 2 13 75-13 1,3-Dichlorobenzene 2.95 1. 2 15 75-13 1,4-Dichlorobenzene 2.1 1. 2 1 75-13 2-Butanone 13.96 5. 2 69.8 55-15 2-Hexanone 14.2 5. 2 7.1 6-135 4-Methyl-2-pentanone 18.6 1. 2 93 77-178 Acetone 2.81 1 2 14 6-16 Acrylonitrile 18.32 1. 2 91.6 6-14 Benzene 65.38 1. 2 45.14 11 85-125 Bromochloromethane 18.68 1. 2 93.4 75-13 Bromodichloromethane 21.4 1. 2 15 75-125 Bromoform 16.63 1. 2 83.2 6-125 Bromomethane 14.6 1. 2 7.3 3-185 Carbon disulfide 22.31 1. 2 112 6-165 Carbon tetrachloride 22.91 1. 2 115 65-14 Chlorobenzene 2.68 1. 2 13 8-12 Chloroethane 23.54 1. 2 118 5-14 Chloroform 2.4 1. 2 1 8-13 Chloromethane 21.19 1. 2 1.5 98.4 5-13 cis-1,2-dichloroethene 19.3 1. 2 96.5 75-134 cis-1,3-dichloropropene 17.49 1. 2 87.4 7-13 Dibromochloromethane 16.89 1. 2 84.4 6-115 Dibromomethane 21.31 1. 2 17 85-125 Dichlorodifluoromethane 19.6 1. 2 95.3 2-12 Ethylbenzene 21.13 1. 2 16 85-125 Hexachloroethane 14.2 1. 2 71 5-124 Isopropylbenzene 2.54 1. 2 13 8-127 m,p-xylene 44.6 2. 4 112 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 19.62 1. 2 98.1 6-16 Methyl tert-butyl ether 18.2 1. 2 9.1 8-13 Methylene chloride 22.17 5. 2 111 75-14 Naphthalene 18.34 5. 2 1.74 83 55-16 n-propylbenzene 21.51 1. 2 18 78-12 o-xylene 21.8 1. 2 15 8-125 Styrene 14.3 1. 2 7.2 85-125 Tetrachloroethene 21.58 1. 2 18 77-138 Toluene 2.49 1. 2 12 85-125 trans-1,2-dichloroethene 22.23 1. 2 111 8-14 trans-1,3-dichloropropene 16.8 1. 2 8.4 81-123 trans-1,4-dichloro-2-butene 13.7 2. 2 65.4 46-118 Trichloroethene 21.75 1. 2 19 84-13 Trichlorofluoromethane 24.38 1. 2 122 6-14 Vinyl chloride 21.25 1. 2 16 5-136 Xylenes, Total 65.68 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 2.55 2 13 75-12 Surr: 4-Bromofluorobenzene 2.61 2 13 8-11 Surr: Dibromofluoromethane 21.2 2 16 85-115 Surr: Toluene-d8 19.69 2 98.4 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: 166757-21A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo:3886189 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.66 1. 2 98.3 8-13 2.8 2.11 3 1,1,1-Trichloroethane 23.81 1. 2 119 75-13 24.12 1.29 3 1,1,2,2-Tetrachloroethane 19.8 1. 2 95.4 75-13 19.35 1.41 3 1,1,2-Trichloroethane 19.61 1. 2 98 75-125 2.4 3.95 3 1,1-Dichloroethane 21.5 1. 2 15 75-133 2.94.524 3 1,1-Dichloroethene 25.19 1. 2 126 7-145 25.13.238 3 1,2,3-Trichloropropane 19.29 1. 2 96.4 75-125 2.1 4.11 3 1,2,4-Trichlorobenzene 18.79 1. 2 94 7-135 19.27 2.52 3 1,2,4-Trimethylbenzene 19.71 1. 2 98.6 75-13 2.24 2.65 3 1,2-Dibromo-3-chloropropane 15.21 1. 2 76 6-13 15.52 2.2 3 1,2-Dibromoethane 21.21 1. 2 16 8-15 22.21 4.61 3 1,2-Dichlorobenzene 19.89 1. 2 99.4 7-13 2.36 2.34 3 1,2-Dichloroethane 21.9 1. 2 15 78-125 21.3.285 3 1,2-Dichloropropane 2.26 1. 2 11 75-125 2.59 1.62 3 1,3,5-Trimethylbenzene 2.21 1. 2 11 75-13 2.68 2.3 3 1,3-Dichlorobenzene 2.53 1. 2 13 75-13 2.95 2.3 3 1,4-Dichlorobenzene 19.81 1. 2 99 75-13 2.1 1 3 2-Butanone 13.91 5. 2 69.6 55-15 13.96.359 3 2-Hexanone 13.95 5. 2 69.8 6-135 14.2.51 3 4-Methyl-2-pentanone 17.36 1. 2 86.8 77-178 18.6 6.9 3 Acetone 22.34 1 2 112 6-16 2.81 7.9 3 Acrylonitrile 15.86 1. 2 79.3 6-14 18.32 14.4 3 Benzene 64.83 1. 2 45.14 98.4 85-125 65.38.845 3 Bromochloromethane 18.4 1. 2 9.2 75-13 18.68 3.49 3 Bromodichloromethane 21.13 1. 2 16 75-125 21.4.427 3 Bromoform 16.78 1. 2 83.9 6-125 16.63.898 3 Bromomethane 15.82 1. 2 79.1 3-185 14.6 11.8 3 Carbon disulfide 22.62 1. 2 113 6-165 22.31 1.38 3 Carbon tetrachloride 22.97 1. 2 115 65-14 22.91.262 3 Chlorobenzene 2.33 1. 2 12 8-12 2.68 1.71 3 Chloroethane 23.5 1. 2 115 5-14 23.54 2.1 3 Chloroform 19.83 1. 2 99.2 8-13 2.4 1.5 3 Chloromethane 19.88 1. 2 1.5 91.9 5-13 21.19 6.38 3 cis-1,2-dichloroethene 19.14 1. 2 95.7 75-134 19.3.832 3 cis-1,3-dichloropropene 17.82 1. 2 89.1 7-13 17.49 1.87 3 Dibromochloromethane 16.93 1. 2 84.6 6-115 16.89.237 3 Dibromomethane 21.7 1. 2 15 85-125 21.31 1.13 3 Dichlorodifluoromethane 18.73 1. 2 93.6 2-12 19.6 1.75 3 Ethylbenzene 2.69 1. 2 13 85-125 21.13 2.1 3 Hexachloroethane 14.63 1. 2 73.2 5-124 14.2 2.98 3 Isopropylbenzene 2.21 1. 2 11 8-127 2.54 1.62 3 m,p-xylene 43.56 2. 4 19 75-13 44.6 2.36 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 166887 Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 11.22 1. 2 56.1 6-16 19.62 54.5 3 Methyl tert-butyl ether 17.21 1. 2 86 8-13 18.2 4.6 3 Methylene chloride 2.8 5. 2 14 75-14 22.17 6.38 3 Naphthalene 17.29 5. 2 1.74 77.8 55-16 18.34 5.89 3 n-propylbenzene 21.2 1. 2 15 78-12 21.51 2.3 3 o-xylene 2.71 1. 2 14 8-125 21.8 1.77 3 Styrene 13.72 1. 2 68.6 85-125 14.3 2.23 3 Tetrachloroethene 21 1. 2 15 77-138 21.58 2.72 3 Toluene 2.34 1. 2 12 85-125 2.49.735 3 trans-1,2-dichloroethene 21.22 1. 2 16 8-14 22.23 4.65 3 trans-1,3-dichloropropene 15.7 1. 2 78.5 81-123 16.8 2.39 3 trans-1,4-dichloro-2-butene 12.81 2. 2 64 46-118 13.7 2.1 3 Trichloroethene 21.54 1. 2 18 84-13 21.75.97 3 Trichlorofluoromethane 23.82 1. 2 119 6-14 24.38 2.32 3 Vinyl chloride 2.97 1. 2 15 5-136 21.25 1.33 3 Xylenes, Total 64.27 3. 6 17 8-126 65.68 2.17 3 Surr: 1,2-Dichloroethane-d4 2.59 2 13 75-12 2.55.194 3 Surr: 4-Bromofluorobenzene 2.65 2 13 8-11 2.61.194 3 Surr: Dibromofluoromethane 21.9 2 15 85-115 21.2.52 3 Surr: Toluene-d8 19.75 2 98.8 85-11 19.69.34 3 SR S S The following samples were analyzed in this batch: 166887-1B QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (139 Cherry Blossom) WorkOrder: 166887 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: 166887 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 3:2:37 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (Hartland - 1385 Cherry Blossom) Work Order: 166479 Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 1385 Cherry Blossom) Work Order: 166479 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166479-1 1385 Cherry Blossom Water 6/6/216 7:26 6/8/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 1385 Cherry Blossom) Work Order: 166479 Sample ID: 1385 Cherry Blossom Lab ID: 166479-1 Collection Date: 6/6/216 7:26 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 7:57 PM Sulfolane 1 µg/l 1 6/9/216 7:57 PM Surr: 2,4,6-Tribromophenol 64. 38-115 %REC 1 6/9/216 7:57 PM Surr: 2-Fluorobiphenyl 52.7 32-1 %REC 1 6/9/216 7:57 PM Surr: 2-Fluorophenol 31.7 22-59 %REC 1 6/9/216 7:57 PM Surr: 4-Terphenyl-d14 71.6 23-112 %REC 1 6/9/216 7:57 PM Surr: Nitrobenzene-d5 6.2 31-93 %REC 1 6/9/216 7:57 PM Surr: Phenol-d6 16.1 13-36 %REC 1 6/9/216 7:57 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 6:15 AM 1,1-Dichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1-Dichloroethene 1. µg/l 1 6/9/216 6:15 AM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 6:15 AM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 6:15 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 6:15 AM 1,2-Dibromoethane 1. µg/l 1 6/9/216 6:15 AM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 1,2-Dichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,2-Dichloropropane 1. µg/l 1 6/9/216 6:15 AM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 6:15 AM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 2-Butanone 5. µg/l 1 6/9/216 6:15 AM 2-Hexanone 5. µg/l 1 6/9/216 6:15 AM 2-Methylnaphthalene 5. µg/l 1 6/9/216 6:15 AM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 6:15 AM Acetone 1 µg/l 1 6/9/216 6:15 AM Acrylonitrile 1. µg/l 1 6/9/216 6:15 AM Benzene 1. µg/l 1 6/9/216 6:15 AM Bromochloromethane 1. µg/l 1 6/9/216 6:15 AM Bromodichloromethane 1. µg/l 1 6/9/216 6:15 AM Bromoform 1. µg/l 1 6/9/216 6:15 AM Bromomethane 1. µg/l 1 6/9/216 6:15 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 1385 Cherry Blossom) Work Order: 166479 Sample ID: 1385 Cherry Blossom Lab ID: 166479-1 Collection Date: 6/6/216 7:26 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 92.6 93.8 95.6 95.4 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 1385 Cherry Blossom) Work Order: 166479 Date: 1-Jun-16 Case Narrative Batch R189191a The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo:387197 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 21.75 5 43.5 38-115 Surr: 2-Fluorobiphenyl 21.56 5 43.1 32-1 Surr: 2-Fluorophenol 16.37 5 32.7 22-59 Surr: 4-Terphenyl-d14 35.69 5 71.4 23-112 Surr: Nitrobenzene-d5 28.3 5 56.1 31-93 Surr: Phenol-d6 7.63 5 15.3 13-36 LCS Sample ID: SLCSW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo:387198 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5.75 5 1 5.75 5-4 Sulfolane 54.53 1 1 54.5 3-1 Surr: 2,4,6-Tribromophenol 27.91 5 55.8 38-115 Surr: 2-Fluorobiphenyl 28.51 5 57 32-1 Surr: 2-Fluorophenol 19.32 5 38.6 22-59 Surr: 4-Terphenyl-d14 37.7 5 75.4 23-112 Surr: Nitrobenzene-d5 35.21 5 7.4 31-93 Surr: Phenol-d6 1.2 5 2 13-36 MS Sample ID: 166476-1B MS Units:µg/L Analysis Date: 6/9/216 6:36 PM Client ID: Run ID: SVMS8_1669A SeqNo:387199 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 53 16.4 13.2 5-4 Sulfolane 65.27 11 16.4 61.4 3-1 Surr: 2,4,6-Tribromophenol 36.5 53.19 67.8 38-115 Surr: 2-Fluorobiphenyl 31.76 53.19 59.7 32-1 Surr: 2-Fluorophenol 2.45 53.19 38.4 22-59 Surr: 4-Terphenyl-d14 38.93 53.19 73.2 23-112 Surr: Nitrobenzene-d5 38.12 53.19 71.7 31-93 Surr: Phenol-d6 1.87 53.19 2.4 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166478-1B DUP Units:µg/L Analysis Date: 6/9/216 7:16 PM Client ID: Run ID: SVMS8_1669A SeqNo:38721 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 32.53 53.2 61.4 38-115 31.66 2.72 4 Surr: 2-Fluorobiphenyl 29.9 53.2 56.4 32-1 27.39 8.78 4 Surr: 2-Fluorophenol 18.87 53.2 35.6 22-59 16.97 1.6 4 Surr: 4-Terphenyl-d14 35.97 53.2 67.8 23-112 37.85 5.9 4 Surr: Nitrobenzene-d5 35.12 53.2 66.2 31-93 32.88 6.59 4 Surr: Phenol-d6 9.3 53.2 17.5 13-36 8.71 6.55 4 The following samples were analyzed in this batch: 166479-1B QC Page: 2 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MBLK Sample ID: VBLKW2-1668-R189191a Units:µg/L Analysis Date: 6/9/216 2:2 AM Client ID: Run ID: VMS6_1668B SeqNo:3868131 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 18.19 2 91 75-12 Surr: 4-Bromofluorobenzene 19.42 2 97.1 8-11 Surr: Dibromofluoromethane 19.84 2 99.2 85-115 Surr: Toluene-d8 19.6 2 95.3 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B LCS Sample ID: VLCSW2-1668-R189191a Units:µg/L Analysis Date: 6/9/216 1:12 AM Client ID: Run ID: VMS6_1668B SeqNo:3868128 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.57 1. 2 13 8-13 1,1,1-Trichloroethane 2.5 1. 2 12 75-13 1,1,2,2-Tetrachloroethane 21.66 1. 2 18 75-13 1,1,2-Trichloroethane 19.85 1. 2 99.2 75-125 1,1-Dichloroethane 19.12 1. 2 95.6 75-133 1,1-Dichloroethene 19.91 1. 2 99.6 7-145 1,2,3-Trichloropropane 2.71 1. 2 14 75-125 1,2,4-Trichlorobenzene 2.9 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.32 1. 2 12 75-13 1,2-Dibromo-3-chloropropane 18.85 1. 2 94.2 6-13 1,2-Dibromoethane 21.31 1. 2 17 8-15 1,2-Dichlorobenzene 2.37 1. 2 12 7-13 1,2-Dichloroethane 18.84 1. 2 94.2 78-125 1,2-Dichloropropane 2.5 1. 2 1 75-125 1,3,5-Trimethylbenzene 2.7 1. 2 14 75-13 1,3-Dichlorobenzene 2.13 1. 2 11 75-13 1,4-Dichlorobenzene 18.8 1. 2 94 75-13 2-Butanone 18.19 5. 2 91 55-15 2-Hexanone 17.68 5. 2 88.4 6-135 4-Methyl-2-pentanone 24.96 1. 2 125 77-178 Acetone 19.47 1 2 97.4 6-16 Acrylonitrile 18.61 1. 2 93 6-14 Benzene 2.49 1. 2 12 85-125 Bromochloromethane 18.44 1. 2 92.2 75-13 Bromodichloromethane 2.1 1. 2 1 75-125 Bromoform 19.96 1. 2 99.8 6-125 Bromomethane 18.62 1. 2 93.1 3-185 Carbon disulfide 2.24 1. 2 11 6-165 Carbon tetrachloride 19.79 1. 2 99 65-14 Chlorobenzene 19.3 1. 2 96.5 8-12 Chloroethane 23.37 1. 2 117 5-14 Chloroform 18.19 1. 2 91 8-13 Chloromethane 15.16 1. 2 75.8 5-13 cis-1,2-dichloroethene 17.74 1. 2 88.7 75-134 cis-1,3-dichloropropene 2.29 1. 2 11 7-13 Dibromochloromethane 19.2 1. 2 95.1 6-115 Dibromomethane 2.48 1. 2 12 85-125 Dichlorodifluoromethane 19.67 1. 2 98.4 2-12 Ethylbenzene 19.65 1. 2 98.2 85-125 Hexachloroethane 15.39 1. 2 77 5-124 Isopropylbenzene 2.62 1. 2 13 8-127 m,p-xylene 4.98 2. 4 12 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 12.7 1. 2 63.5 6-16 Methyl tert-butyl ether 18 1. 2 9 8-13 Methylene chloride 17.88 5. 2 89.4 75-14 Naphthalene 21.87 5. 2 19 55-16 n-propylbenzene 2.14 1. 2 11 78-12 o-xylene 19.28 1. 2 96.4 8-125 Styrene 21.3 1. 2 15 85-125 Tetrachloroethene 2.34 1. 2 12 77-138 Toluene 19.4 1. 2 97 85-125 trans-1,2-dichloroethene 18.95 1. 2 94.8 8-14 trans-1,3-dichloropropene 16.82 1. 2 84.1 81-123 trans-1,4-dichloro-2-butene 12.14 2. 2 6.7 46-118 Trichloroethene 2.81 1. 2 14 84-13 Trichlorofluoromethane 19.62 1. 2 98.1 6-14 Vinyl chloride 19.82 1. 2 99.1 5-136 Xylenes, Total 6.26 3. 6 1 8-126 Surr: 1,2-Dichloroethane-d4 17.86 2 89.3 75-12 Surr: 4-Bromofluorobenzene 2.13 2 11 8-11 Surr: Dibromofluoromethane 19.75 2 98.8 85-115 Surr: Toluene-d8 18.98 2 94.9 85-11 QC Page: 6 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MS Sample ID: 16641-15A MS Units:µg/L Analysis Date: 6/9/216 1:53 AM Client ID: Run ID: VMS6_1668B SeqNo:3868146 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 227 1 2 11 8-13 1,1,1-Trichloroethane 2176 1 2 19 75-13 1,1,2,2-Tetrachloroethane 298 1 2 15 75-13 1,1,2-Trichloroethane 1988 1 2 99.4 75-125 1,1-Dichloroethane 272 1 2 14 75-133 1,1-Dichloroethene 2225 1 2 111 7-145 1,2,3-Trichloropropane 1968 1 2 98.4 75-125 1,2,4-Trichlorobenzene 1814 1 2 9.7 7-135 1,2,4-Trimethylbenzene 3856 1 2 1781 14 75-13 1,2-Dibromo-3-chloropropane 1598 1 2 79.9 6-13 1,2-Dibromoethane 229 1 2 11 8-15 1,2-Dichlorobenzene 1913 1 2 95.6 7-13 1,2-Dichloroethane 1936 1 2 96.8 78-125 1,2-Dichloropropane 224 1 2 11 75-125 1,3,5-Trimethylbenzene 2485 1 2 44 12 75-13 1,3-Dichlorobenzene 1859 1 2 93 75-13 1,4-Dichlorobenzene 1771 1 2 88.6 75-13 2-Butanone 1554 5 2 77.7 55-15 2-Hexanone 168 5 2 84 6-135 4-Methyl-2-pentanone 2333 1 2 117 77-178 Acetone 2157 1, 2 18 6-16 Acrylonitrile 161 1 2 8.5 6-14 Benzene 151 1 2 7878 132 85-125 Bromochloromethane 1882 1 2 94.1 75-13 Bromodichloromethane 1999 1 2 1 75-125 Bromoform 181 1 2 9 6-125 Bromomethane 787 1 2 39.4 3-185 Carbon disulfide 25 1 2 1 6-165 Carbon tetrachloride 257 1 2 13 65-14 Chlorobenzene 1989 1 2 99.4 8-12 Chloroethane 3158 1 2 158 5-14 Chloroform 1881 1 2 94 8-13 Chloromethane 144 1 2 72 5-13 cis-1,2-dichloroethene 1836 1 2 91.8 75-134 cis-1,3-dichloropropene 1983 1 2 99.2 7-13 Dibromochloromethane 1793 1 2 89.6 6-115 Dibromomethane 27 1 2 14 85-125 Dichlorodifluoromethane 265 1 2 13 2-12 Ethylbenzene 424 1 2 2217 11 85-125 Hexachloroethane 1383 1 2 69.2 5-124 Isopropylbenzene 2155 1 2 9 13 8-127 m,p-xylene 1212 2 4 8137 99.5 75-13 SE S QC Page: 7 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 713 1 2 35.6 6-16 Methyl tert-butyl ether 1823 1 2 91.2 8-13 Methylene chloride 196 5 2 95.3 75-14 Naphthalene 23 5 2 372 96.4 55-16 n-propylbenzene 2251 1 2 243 1 78-12 o-xylene 5588 1 2 3675 95.6 8-125 Styrene 22 1 2 11 85-125 Tetrachloroethene 263 1 2 13 77-138 Toluene 1167 1 2 9459 111 85-125 trans-1,2-dichloroethene 235 1 2 12 8-14 trans-1,3-dichloropropene 158 1 2 79 81-123 trans-1,4-dichloro-2-butene 184 2 2 54.2 46-118 Trichloroethene 2218 1 2 111 84-13 Trichlorofluoromethane 2239 1 2 112 6-14 Vinyl chloride 2122 1 2 16 5-136 Xylenes, Total 1771 3 6 1181 98.2 8-126 Surr: 1,2-Dichloroethane-d4 1818 2 9.9 75-12 Surr: 4-Bromofluorobenzene 211 2 11 8-11 Surr: Dibromofluoromethane 194 2 97 85-115 Surr: Toluene-d8 1912 2 95.6 85-11 S EO S QC Page: 8 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MSD Sample ID: 16641-15A MSD Units:µg/L Analysis Date: 6/9/216 11:18 AM Client ID: Run ID: VMS6_1668B SeqNo:3868147 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2 1 2 1 8-13 227 1.34 3 1,1,1-Trichloroethane 294 1 2 15 75-13 2176 3.84 3 1,1,2,2-Tetrachloroethane 228 1 2 11 75-13 298 3.39 3 1,1,2-Trichloroethane 1862 1 2 93.1 75-125 1988 6.55 3 1,1-Dichloroethane 1943 1 2 97.2 75-133 272 6.43 3 1,1-Dichloroethene 2156 1 2 18 7-145 2225 3.15 3 1,2,3-Trichloropropane 1869 1 2 93.4 75-125 1968 5.16 3 1,2,4-Trichlorobenzene 1877 1 2 93.8 7-135 1814 3.41 3 1,2,4-Trimethylbenzene 552 1 2 1781 186 75-13 3856 35.2 3 1,2-Dibromo-3-chloropropane 1518 1 2 75.9 6-13 1598 5.13 3 1,2-Dibromoethane 196 1 2 98 8-15 229 3.46 3 1,2-Dichlorobenzene 1939 1 2 97 7-13 1913 1.35 3 1,2-Dichloroethane 1818 1 2 9.9 78-125 1936 6.29 3 1,2-Dichloropropane 1959 1 2 98 75-125 224 3.26 3 1,3,5-Trimethylbenzene 2975 1 2 44 127 75-13 2485 17.9 3 1,3-Dichlorobenzene 1918 1 2 95.9 75-13 1859 3.12 3 1,4-Dichlorobenzene 1834 1 2 91.7 75-13 1771 3.5 3 2-Butanone 161 5 2 8.5 55-15 1554 3.54 3 2-Hexanone 167 5 2 8.4 6-135 168 4.44 3 4-Methyl-2-pentanone 223 1 2 112 77-178 2333 4.51 3 Acetone 228 1, 2 11 6-16 2157 2.34 3 Acrylonitrile 1516 1 2 75.8 6-14 161 6.1 3 Benzene 1775 1 2 7878 494 85-125 151 51.3 3 Bromochloromethane 18 1 2 9 75-13 1882 4.45 3 Bromodichloromethane 191 1 2 95.5 75-125 1999 4.55 3 Bromoform 1729 1 2 86.4 6-125 181 4.8 3 Bromomethane 146 1 2 73 3-185 787 59.9 3 Carbon disulfide 213 1 2 11 6-165 25.398 3 Carbon tetrachloride 289 1 2 14 65-14 257 1.54 3 Chlorobenzene 1936 1 2 96.8 8-12 1989 2.7 3 Chloroethane 2892 1 2 145 5-14 3158 8.79 3 Chloroform 1862 1 2 93.1 8-13 1881 1.2 3 Chloromethane 1275 1 2 63.8 5-13 144 12.2 3 cis-1,2-dichloroethene 1769 1 2 88.4 75-134 1836 3.72 3 cis-1,3-dichloropropene 1916 1 2 95.8 7-13 1983 3.44 3 Dibromochloromethane 1762 1 2 88.1 6-115 1793 1.74 3 Dibromomethane 1897 1 2 94.8 85-125 27 8.72 3 Dichlorodifluoromethane 234 1 2 12 2-12 265 1.51 3 Ethylbenzene 6328 1 2 2217 26 85-125 424 39.5 3 Hexachloroethane 1523 1 2 76.2 5-124 1383 9.64 3 Isopropylbenzene 2275 1 2 9 19 8-127 2155 5.42 3 m,p-xylene 1918 2 4 8137 276 75-13 1212 45.1 3 SR SRE R S SR SR QC Page: 9 of 1

Client: Merit Energy Work Order: 166479 Project: ECT (Hartland - 1385 Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 98 1 2 49 6-16 713 31.5 3 Methyl tert-butyl ether 1779 1 2 89 8-13 1823 2.44 3 Methylene chloride 1788 5 2 89.4 75-14 196 6.39 3 Naphthalene 2618 5 2 372 112 55-16 23 12.9 3 n-propylbenzene 2511 1 2 243 113 78-12 2251 1.9 3 o-xylene 892 1 2 3675 261 8-125 5588 45.7 3 Styrene 2316 1 2 116 85-125 22 5.14 3 Tetrachloroethene 214 1 2 15 77-138 263 1.97 3 Toluene 1991 1 2 9459 522 85-125 1167 52.1 3 trans-1,2-dichloroethene 1963 1 2 98.2 8-14 235 3.6 3 trans-1,3-dichloropropene 1519 1 2 76 81-123 158 3.94 3 trans-1,4-dichloro-2-butene 12 2 2 51 46-118 184 6.8 3 Trichloroethene 2147 1 2 17 84-13 2218 3.25 3 Trichlorofluoromethane 2213 1 2 111 6-14 2239 1.17 3 Vinyl chloride 1987 1 2 99.4 5-136 2122 6.57 3 Xylenes, Total 288 3 6 1181 271 8-126 1771 45.3 3 Surr: 1,2-Dichloroethane-d4 1793 2 89.6 75-12 1818 1.38 3 Surr: 4-Bromofluorobenzene 211 2 11 8-11 211 3 Surr: Dibromofluoromethane 1965 2 98.2 85-115 194 1.28 3 Surr: Toluene-d8 1896 2 94.8 85-11 1912.84 3 SR SR SREO S SR The following samples were analyzed in this batch: 166479-1A QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 1385 Cherry Blossom) WorkOrder: 166479 Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: 166479 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 3.6/3.6 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:37:4 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (Hartland - 13593 Sheila Lane) Work Order: 166481 Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13593 Sheila Lane) Work Order: 166481 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166481-1 13593 Sheila Lane Water 6/6/216 17:56 6/8/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13593 Sheila Lane) Work Order: 166481 Sample ID: 13593 Sheila Lane Lab ID: 166481-1 Collection Date: 6/6/216 5:56 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 8:38 PM Sulfolane 1 µg/l 1 6/9/216 8:38 PM Surr: 2,4,6-Tribromophenol 59.9 38-115 %REC 1 6/9/216 8:38 PM Surr: 2-Fluorobiphenyl 53.8 32-1 %REC 1 6/9/216 8:38 PM Surr: 2-Fluorophenol 33.2 22-59 %REC 1 6/9/216 8:38 PM Surr: 4-Terphenyl-d14 73.1 23-112 %REC 1 6/9/216 8:38 PM Surr: Nitrobenzene-d5 61.9 31-93 %REC 1 6/9/216 8:38 PM Surr: Phenol-d6 17.2 13-36 %REC 1 6/9/216 8:38 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 2:51 PM 1,1-Dichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1-Dichloroethene 1. µg/l 1 6/9/216 2:51 PM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 2:51 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 2:51 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 2:51 PM 1,2-Dibromoethane 1. µg/l 1 6/9/216 2:51 PM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 1,2-Dichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,2-Dichloropropane 1. µg/l 1 6/9/216 2:51 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 2:51 PM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 2-Butanone 5. µg/l 1 6/9/216 2:51 PM 2-Hexanone 5. µg/l 1 6/9/216 2:51 PM 2-Methylnaphthalene 5. µg/l 1 6/9/216 2:51 PM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 2:51 PM Acetone 1 µg/l 1 6/9/216 2:51 PM Acrylonitrile 1. µg/l 1 6/9/216 2:51 PM Benzene 1. µg/l 1 6/9/216 2:51 PM Bromochloromethane 1. µg/l 1 6/9/216 2:51 PM Bromodichloromethane 1. µg/l 1 6/9/216 2:51 PM Bromoform 1. µg/l 1 6/9/216 2:51 PM Bromomethane 1. µg/l 1 6/9/216 2:51 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13593 Sheila Lane) Work Order: 166481 Sample ID: 13593 Sheila Lane Lab ID: 166481-1 Collection Date: 6/6/216 5:56 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 16 91.2 11 97. 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 13593 Sheila Lane) Work Order: 166481 Date: 1-Jun-16 Case Narrative Batch R189219 Sample VLCSW1-1669 The LCS recovery for volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were non-detect. No qualification is necessary for this analyte. Batch R189219 The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo:387197 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 21.75 5 43.5 38-115 Surr: 2-Fluorobiphenyl 21.56 5 43.1 32-1 Surr: 2-Fluorophenol 16.37 5 32.7 22-59 Surr: 4-Terphenyl-d14 35.69 5 71.4 23-112 Surr: Nitrobenzene-d5 28.3 5 56.1 31-93 Surr: Phenol-d6 7.63 5 15.3 13-36 LCS Sample ID: SLCSW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo:387198 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5.75 5 1 5.75 5-4 Sulfolane 54.53 1 1 54.5 3-1 Surr: 2,4,6-Tribromophenol 27.91 5 55.8 38-115 Surr: 2-Fluorobiphenyl 28.51 5 57 32-1 Surr: 2-Fluorophenol 19.32 5 38.6 22-59 Surr: 4-Terphenyl-d14 37.7 5 75.4 23-112 Surr: Nitrobenzene-d5 35.21 5 7.4 31-93 Surr: Phenol-d6 1.2 5 2 13-36 MS Sample ID: 166476-1B MS Units:µg/L Analysis Date: 6/9/216 6:36 PM Client ID: Run ID: SVMS8_1669A SeqNo:387199 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 53 16.4 13.2 5-4 Sulfolane 65.27 11 16.4 61.4 3-1 Surr: 2,4,6-Tribromophenol 36.5 53.19 67.8 38-115 Surr: 2-Fluorobiphenyl 31.76 53.19 59.7 32-1 Surr: 2-Fluorophenol 2.45 53.19 38.4 22-59 Surr: 4-Terphenyl-d14 38.93 53.19 73.2 23-112 Surr: Nitrobenzene-d5 38.12 53.19 71.7 31-93 Surr: Phenol-d6 1.87 53.19 2.4 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166478-1B DUP Units:µg/L Analysis Date: 6/9/216 7:16 PM Client ID: Run ID: SVMS8_1669A SeqNo:38721 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 32.53 53.2 61.4 38-115 31.66 2.72 4 Surr: 2-Fluorobiphenyl 29.9 53.2 56.4 32-1 27.39 8.78 4 Surr: 2-Fluorophenol 18.87 53.2 35.6 22-59 16.97 1.6 4 Surr: 4-Terphenyl-d14 35.97 53.2 67.8 23-112 37.85 5.9 4 Surr: Nitrobenzene-d5 35.12 53.2 66.2 31-93 32.88 6.59 4 Surr: Phenol-d6 9.3 53.2 17.5 13-36 8.71 6.55 4 The following samples were analyzed in this batch: 166481-1B QC Page: 2 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-1669-R189219 Units:µg/L Analysis Date: 6/9/216 1:38 PM Client ID: Run ID: VMS1_1669A SeqNo:3868762 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 2.49 2 12 75-12 Surr: 4-Bromofluorobenzene 18.47 2 92.4 8-11 Surr: Dibromofluoromethane 2 2 1 85-115 Surr: Toluene-d8 19.62 2 98.1 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW1-1669-R189219 Units:µg/L Analysis Date: 6/9/216 1:58 AM Client ID: Run ID: VMS1_1669A SeqNo:3868761 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.21 1. 2 11 8-13 1,1,1-Trichloroethane 21.58 1. 2 18 75-13 1,1,2,2-Tetrachloroethane 19.6 1. 2 98 75-13 1,1,2-Trichloroethane 2.68 1. 2 13 75-125 1,1-Dichloroethane 2.39 1. 2 12 75-133 1,1-Dichloroethene 21.68 1. 2 18 7-145 1,2,3-Trichloropropane 19.27 1. 2 96.4 75-125 1,2,4-Trichlorobenzene 21.3 1. 2 15 7-135 1,2,4-Trimethylbenzene 21.28 1. 2 16 75-13 1,2-Dibromo-3-chloropropane 15.2 1. 2 75.1 6-13 1,2-Dibromoethane 22.66 1. 2 113 8-15 1,2-Dichlorobenzene 2.98 1. 2 15 7-13 1,2-Dichloroethane 19.47 1. 2 97.4 78-125 1,2-Dichloropropane 2.58 1. 2 13 75-125 1,3,5-Trimethylbenzene 21.96 1. 2 11 75-13 1,3-Dichlorobenzene 21.37 1. 2 17 75-13 1,4-Dichlorobenzene 21.12 1. 2 16 75-13 2-Butanone 16.22 5. 2 81.1 55-15 2-Hexanone 16.77 5. 2 83.8 6-135 4-Methyl-2-pentanone 22.16 1. 2 111 77-178 Acetone 14.1 1 2 7.5 6-16 Acrylonitrile 15.91 1. 2 79.6 6-14 Benzene 2.51 1. 2 13 85-125 Bromochloromethane 2.81 1. 2 14 75-13 Bromodichloromethane 2.49 1. 2 12 75-125 Bromoform 16.4 1. 2 8.2 6-125 Bromomethane 23.77 1. 2 119 3-185 Carbon disulfide 2.48 1. 2 12 6-165 Carbon tetrachloride 19.28 1. 2 96.4 65-14 Chlorobenzene 21.38 1. 2 17 8-12 Chloroethane 17.38 1. 2 86.9 5-14 Chloroform 19.58 1. 2 97.9 8-13 Chloromethane 19.42 1. 2 97.1 5-13 cis-1,2-dichloroethene 2.11 1. 2 11 75-134 cis-1,3-dichloropropene 18.96 1. 2 94.8 7-13 Dibromochloromethane 16.82 1. 2 84.1 6-115 Dibromomethane 2.77 1. 2 14 85-125 Dichlorodifluoromethane 18.28 1. 2 91.4 2-12 Ethylbenzene 22.59 1. 2 113 85-125 Hexachloroethane 15.37 1. 2 76.8 5-124 Isopropylbenzene 21.69 1. 2 18 8-127 m,p-xylene 46.1 2. 4 115 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B Methyl iodide 34.3 1. 2 17 6-16 Methyl tert-butyl ether 16.14 1. 2 8.7 8-13 Methylene chloride 22.58 5. 2 113 75-14 Naphthalene 18.11 5. 2 9.6 55-16 n-propylbenzene 23.4 1. 2 115 78-12 o-xylene 22.43 1. 2 112 8-125 Styrene 21.5 1. 2 18 85-125 Tetrachloroethene 21.91 1. 2 11 77-138 Toluene 21.48 1. 2 17 85-125 trans-1,2-dichloroethene 19.45 1. 2 97.2 8-14 trans-1,3-dichloropropene 17.2 1. 2 86 81-123 trans-1,4-dichloro-2-butene 14.3 2. 2 71.5 46-118 Trichloroethene 2.6 1. 2 13 84-13 Trichlorofluoromethane 18.89 1. 2 94.4 6-14 Vinyl chloride 21.52 1. 2 18 5-136 Xylenes, Total 68.53 3. 6 114 8-126 Surr: 1,2-Dichloroethane-d4 19.12 2 95.6 75-12 Surr: 4-Bromofluorobenzene 2.33 2 12 8-11 Surr: Dibromofluoromethane 19.89 2 99.4 85-115 Surr: Toluene-d8 2.23 2 11 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B MS Sample ID: 166558-2A MS Units:µg/L Analysis Date: 6/9/216 8:55 PM Client ID: Run ID: VMS1_1669A SeqNo:3868779 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.91 1. 2 99.6 8-13 1,1,1-Trichloroethane 22.74 1. 2 114 75-13 1,1,2,2-Tetrachloroethane 2.1 1. 2 1 75-13 1,1,2-Trichloroethane 2.39 1. 2 12 75-125 1,1-Dichloroethane 2.78 1. 2 14 75-133 1,1-Dichloroethene 22.55 1. 2 113 7-145 1,2,3-Trichloropropane 19.76 1. 2 98.8 75-125 1,2,4-Trichlorobenzene 17.66 1. 2 88.3 7-135 1,2,4-Trimethylbenzene 2.34 1. 2 12 75-13 1,2-Dibromo-3-chloropropane 15.54 1. 2 77.7 6-13 1,2-Dibromoethane 21.99 1. 2 11 8-15 1,2-Dichlorobenzene 19.41 1. 2 97 7-13 1,2-Dichloroethane 19.69 1. 2 98.4 78-125 1,2-Dichloropropane 2.47 1. 2 12 75-125 1,3,5-Trimethylbenzene 2.95 1. 2 15 75-13 1,3-Dichlorobenzene 19.66 1. 2 98.3 75-13 1,4-Dichlorobenzene 19.42 1. 2 97.1 75-13 2-Butanone 17.13 5. 2 85.6 55-15 2-Hexanone 17.53 5. 2 87.6 6-135 4-Methyl-2-pentanone 23.94 1. 2 12 77-178 Acetone 15.73 1 2 78.6 6-16 Acrylonitrile 16.8 1. 2 8.4 6-14 Benzene 2.5 1. 2 12 85-125 Bromochloromethane 2.6 1. 2 1 75-13 Bromodichloromethane 2.33 1. 2 12 75-125 Bromoform 16.8 1. 2 8.4 6-125 Bromomethane 13.6 1. 2 65.3 3-185 Carbon disulfide 19.45 1. 2 97.2 6-165 Carbon tetrachloride 2.6 1. 2 13 65-14 Chlorobenzene 2.58 1. 2 13 8-12 Chloroethane 17.32 1. 2 86.6 5-14 Chloroform 19.49 1. 2 97.4 8-13 Chloromethane 15.54 1. 2 77.7 5-13 cis-1,2-dichloroethene 19.51 1. 2 97.6 75-134 cis-1,3-dichloropropene 17.65 1. 2 88.2 7-13 Dibromochloromethane 16.56 1. 2 82.8 6-115 Dibromomethane 21.4 1. 2 17 85-125 Dichlorodifluoromethane 2.4 1. 2 1 2-12 Ethylbenzene 21.47 1. 2 17 85-125 Hexachloroethane 14.27 1. 2 71.4 5-124 Isopropylbenzene 2.87 1. 2 14 8-127 m,p-xylene 44.4 2. 4 111 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B Methyl iodide 23.54 1. 2 118 6-16 Methyl tert-butyl ether 14.86 1. 2 74.3 8-13 Methylene chloride 21.31 5. 2 17 75-14 Naphthalene 16.44 5. 2 82.2 55-16 n-propylbenzene 22.6 1. 2 11 78-12 o-xylene 21.17 1. 2 16 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 21.47 1. 2 17 77-138 Toluene 2.64 1. 2 13 85-125 trans-1,2-dichloroethene 18.86 1. 2 94.3 8-14 trans-1,3-dichloropropene 15.89 1. 2 79.4 81-123 trans-1,4-dichloro-2-butene 13.66 2. 2 68.3 46-118 Trichloroethene 2.83 1. 2 14 84-13 Trichlorofluoromethane 21.1 1. 2 15 6-14 Vinyl chloride 2.56 1. 2 13 5-136 Xylenes, Total 65.57 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 19.77 2 98.8 75-12 Surr: 4-Bromofluorobenzene 2.44 2 12 8-11 Surr: Dibromofluoromethane 2.89 2 14 85-115 Surr: Toluene-d8 2.2 2 11 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B MSD Sample ID: 166558-2A MSD Units:µg/L Analysis Date: 6/9/216 9:2 PM Client ID: Run ID: VMS1_1669A SeqNo:386878 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.11 1. 2 11 8-13 19.91 1 3 1,1,1-Trichloroethane 22.9 1. 2 114 75-13 22.74.71 3 1,1,2,2-Tetrachloroethane 2.56 1. 2 13 75-13 2.1 2.26 3 1,1,2-Trichloroethane 2.55 1. 2 13 75-125 2.39.782 3 1,1-Dichloroethane 2.95 1. 2 15 75-133 2.78.815 3 1,1-Dichloroethene 22.67 1. 2 113 7-145 22.55.531 3 1,2,3-Trichloropropane 2.16 1. 2 11 75-125 19.76 2 3 1,2,4-Trichlorobenzene 18.68 1. 2 93.4 7-135 17.66 5.61 3 1,2,4-Trimethylbenzene 2.5 1. 2 12 75-13 2.34.784 3 1,2-Dibromo-3-chloropropane 15.86 1. 2 79.3 6-13 15.54 2.4 3 1,2-Dibromoethane 22.75 1. 2 114 8-15 21.99 3.4 3 1,2-Dichlorobenzene 19.86 1. 2 99.3 7-13 19.41 2.29 3 1,2-Dichloroethane 19.98 1. 2 99.9 78-125 19.69 1.46 3 1,2-Dichloropropane 21.2 1. 2 15 75-125 2.47 2.65 3 1,3,5-Trimethylbenzene 21.29 1. 2 16 75-13 2.95 1.61 3 1,3-Dichlorobenzene 2.35 1. 2 12 75-13 19.66 3.45 3 1,4-Dichlorobenzene 2.2 1. 2 1 75-13 19.42 3.4 3 2-Butanone 17.28 5. 2 86.4 55-15 17.13.872 3 2-Hexanone 18.94 5. 2 94.7 6-135 17.53 7.73 3 4-Methyl-2-pentanone 24.55 1. 2 123 77-178 23.94 2.52 3 Acetone 18.66 1 2 93.3 6-16 15.73 17 3 Acrylonitrile 17.19 1. 2 86 6-14 16.8 6.67 3 Benzene 2.99 1. 2 15 85-125 2.5 2.36 3 Bromochloromethane 2.41 1. 2 12 75-13 2.6 1.73 3 Bromodichloromethane 2.96 1. 2 15 75-125 2.33 3.5 3 Bromoform 16.62 1. 2 83.1 6-125 16.8 3.3 3 Bromomethane 13.9 1. 2 69.5 3-185 13.6 6.23 3 Carbon disulfide 19.92 1. 2 99.6 6-165 19.45 2.39 3 Carbon tetrachloride 21.29 1. 2 16 65-14 2.6 3.29 3 Chlorobenzene 2.77 1. 2 14 8-12 2.58.919 3 Chloroethane 17.91 1. 2 89.6 5-14 17.32 3.35 3 Chloroform 19.79 1. 2 99 8-13 19.49 1.53 3 Chloromethane 16.15 1. 2 8.8 5-13 15.54 3.85 3 cis-1,2-dichloroethene 19.48 1. 2 97.4 75-134 19.51.154 3 cis-1,3-dichloropropene 18.32 1. 2 91.6 7-13 17.65 3.73 3 Dibromochloromethane 16.55 1. 2 82.8 6-115 16.56.64 3 Dibromomethane 21.6 1. 2 15 85-125 21.4 1.6 3 Dichlorodifluoromethane 2.32 1. 2 12 2-12 2.4 1.39 3 Ethylbenzene 22.3 1. 2 11 85-125 21.47 2.57 3 Hexachloroethane 14.86 1. 2 74.3 5-124 14.27 4.5 3 Isopropylbenzene 21.45 1. 2 17 8-127 2.87 2.74 3 m,p-xylene 45.43 2. 4 114 75-13 44.4 2.29 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 166481 Project: ECT (Hartland - 13593 Sheila Lane) Batch ID: R189219 Instrument ID VMS1 Method: SW826B Methyl iodide 26.31 1. 2 132 6-16 23.54 11.1 3 Methyl tert-butyl ether 15.3 1. 2 76.5 8-13 14.86 2.92 3 Methylene chloride 21.12 5. 2 16 75-14 21.31.896 3 Naphthalene 17.63 5. 2 88.2 55-16 16.44 6.99 3 n-propylbenzene 22.37 1. 2 112 78-12 22.6 1.4 3 o-xylene 21.75 1. 2 19 8-125 21.17 2.7 3 Styrene 2.92 1. 2 15 85-125 2.41 2.47 3 Tetrachloroethene 22.11 1. 2 111 77-138 21.47 2.94 3 Toluene 21.1 1. 2 15 85-125 2.64 1.78 3 trans-1,2-dichloroethene 19.3 1. 2 96.5 8-14 18.86 2.31 3 trans-1,3-dichloropropene 16.14 1. 2 8.7 81-123 15.89 1.56 3 trans-1,4-dichloro-2-butene 14.4 2. 2 7.2 46-118 13.66 2.74 3 Trichloroethene 21.45 1. 2 17 84-13 2.83 2.93 3 Trichlorofluoromethane 2.7 1. 2 14 6-14 21.1 1.49 3 Vinyl chloride 21.1 1. 2 16 5-136 2.56 2.59 3 Xylenes, Total 67.18 3. 6 112 8-126 65.57 2.43 3 Surr: 1,2-Dichloroethane-d4 2.3 2 1 75-12 19.77 1.31 3 Surr: 4-Bromofluorobenzene 2.25 2 11 8-11 2.44.934 3 Surr: Dibromofluoromethane 2.68 2 13 85-115 2.89 1.1 3 Surr: Toluene-d8 2.9 2 1 85-11 2.2.546 3 S S The following samples were analyzed in this batch: 166481-1A QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 13593 Sheila Lane) WorkOrder: 166481 Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: 166481 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.4/2.4 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:48:37 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (46 Jeni Lane) Work Order: 166873 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: 166873 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166873-1 46 Jeni Lane Water 6/13/216 15:31 6/15/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: 166873 Sample ID: 46 Jeni Lane Lab ID: 166873-1 Collection Date: 6/13/216 3:31 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/17/216 1:47 AM Sulfolane 1 µg/l 1 6/17/216 1:47 AM Surr: 2,4,6-Tribromophenol 65.1 38-115 %REC 1 6/17/216 1:47 AM Surr: 2-Fluorobiphenyl 63.2 32-1 %REC 1 6/17/216 1:47 AM Surr: 2-Fluorophenol 44.2 22-59 %REC 1 6/17/216 1:47 AM Surr: 4-Terphenyl-d14 91.9 23-112 %REC 1 6/17/216 1:47 AM Surr: Nitrobenzene-d5 73.5 31-93 %REC 1 6/17/216 1:47 AM Surr: Phenol-d6 26.4 13-36 %REC 1 6/17/216 1:47 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 4:41 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 4:41 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 4:41 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 4:41 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 4:41 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 4:41 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 4:41 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 4:41 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 2-Butanone 5. µg/l 1 6/21/216 4:41 PM 2-Hexanone 5. µg/l 1 6/21/216 4:41 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 4:41 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 4:41 PM Acetone 1 µg/l 1 6/21/216 4:41 PM Acrylonitrile 1. µg/l 1 6/21/216 4:41 PM Benzene 1. µg/l 1 6/21/216 4:41 PM Bromochloromethane 1. µg/l 1 6/21/216 4:41 PM Bromodichloromethane 1. µg/l 1 6/21/216 4:41 PM Bromoform 1. µg/l 1 6/21/216 4:41 PM Bromomethane 1. µg/l 1 6/21/216 4:41 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: 166873 Sample ID: 46 Jeni Lane Lab ID: 166873-1 Collection Date: 6/13/216 3:31 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 19 9.2 16 93.8 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: 166873 Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW2-16621 The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 1.77 5 1 1.8 1-5 Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 18.58 5 1 18.6 1-5 Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 166873-1A QC Page: 2 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-16621-R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo:388617 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 21.46 2 17 75-12 Surr: 4-Bromofluorobenzene 17.99 2 9 8-11 Surr: Dibromofluoromethane 2.43 2 12 85-115 Surr: Toluene-d8 18.84 2 94.2 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW2-16621-R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo:3886169 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.57 1. 2 97.8 8-13 1,1,1-Trichloroethane 22.55 1. 2 113 75-13 1,1,2,2-Tetrachloroethane 18.67 1. 2 93.4 75-13 1,1,2-Trichloroethane 19.87 1. 2 99.4 75-125 1,1-Dichloroethane 21.59 1. 2 18 75-133 1,1-Dichloroethene 24.6 1. 2 123 7-145 1,2,3-Trichloropropane 18.99 1. 2 95 75-125 1,2,4-Trichlorobenzene 2.1 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.83 1. 2 14 75-13 1,2-Dibromo-3-chloropropane 14.85 1. 2 74.2 6-13 1,2-Dibromoethane 21.69 1. 2 18 8-15 1,2-Dichlorobenzene 2.68 1. 2 13 7-13 1,2-Dichloroethane 2.77 1. 2 14 78-125 1,2-Dichloropropane 19.91 1. 2 99.6 75-125 1,3,5-Trimethylbenzene 21.2 1. 2 16 75-13 1,3-Dichlorobenzene 21.55 1. 2 18 75-13 1,4-Dichlorobenzene 2.77 1. 2 14 75-13 2-Butanone 13.56 5. 2 67.8 55-15 2-Hexanone 13.16 5. 2 65.8 6-135 4-Methyl-2-pentanone 17.41 1. 2 87 77-178 Acetone 15.96 1 2 79.8 6-16 Acrylonitrile 15.7 1. 2 78.5 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 18.78 1. 2 93.9 75-13 Bromodichloromethane 2.47 1. 2 12 75-125 Bromoform 16.14 1. 2 8.7 6-125 Bromomethane 27.29 1. 2 136 3-185 Carbon disulfide 22.57 1. 2 113 6-165 Carbon tetrachloride 21.1 1. 2 15 65-14 Chlorobenzene 2.84 1. 2 14 8-12 Chloroethane 23.14 1. 2 116 5-14 Chloroform 19.86 1. 2 99.3 8-13 Chloromethane 14.87 1. 2 74.4 5-13 cis-1,2-dichloroethene 19.63 1. 2 98.2 75-134 cis-1,3-dichloropropene 17.96 1. 2 89.8 7-13 Dibromochloromethane 16.62 1. 2 83.1 6-115 Dibromomethane 2.68 1. 2 13 85-125 Dichlorodifluoromethane 18.35 1. 2 91.8 2-12 Ethylbenzene 21.52 1. 2 18 85-125 Hexachloroethane 14.16 1. 2 7.8 5-124 Isopropylbenzene 2.7 1. 2 14 8-127 m,p-xylene 44.74 2. 4 112 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 4.55 1. 2 23 6-16 Methyl tert-butyl ether 17.94 1. 2 89.7 8-13 Methylene chloride 23.38 5. 2 117 75-14 Naphthalene 16.24 5. 2 81.2 55-16 n-propylbenzene 22.3 1. 2 11 78-12 o-xylene 21.56 1. 2 18 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 22.69 1. 2 113 77-138 Toluene 2.43 1. 2 12 85-125 trans-1,2-dichloroethene 22.8 1. 2 114 8-14 trans-1,3-dichloropropene 16.34 1. 2 81.7 81-123 trans-1,4-dichloro-2-butene 12.84 2. 2 64.2 46-118 Trichloroethene 21.85 1. 2 19 84-13 Trichlorofluoromethane 22.88 1. 2 114 6-14 Vinyl chloride 2.66 1. 2 13 5-136 Xylenes, Total 66.3 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 2.4 2 1 75-12 Surr: 4-Bromofluorobenzene 2.4 2 1 8-11 Surr: Dibromofluoromethane 2.8 2 14 85-115 Surr: Toluene-d8 19.65 2 98.2 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: 166757-21A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo:3886188 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.8 1. 2 1 8-13 1,1,1-Trichloroethane 24.12 1. 2 121 75-13 1,1,2,2-Tetrachloroethane 19.35 1. 2 96.8 75-13 1,1,2-Trichloroethane 2.4 1. 2 12 75-125 1,1-Dichloroethane 2.94 1. 2 15 75-133 1,1-Dichloroethene 25.13 1. 2 126 7-145 1,2,3-Trichloropropane 2.1 1. 2 1 75-125 1,2,4-Trichlorobenzene 19.27 1. 2 96.4 7-135 1,2,4-Trimethylbenzene 2.24 1. 2 11 75-13 1,2-Dibromo-3-chloropropane 15.52 1. 2 77.6 6-13 1,2-Dibromoethane 22.21 1. 2 111 8-15 1,2-Dichlorobenzene 2.36 1. 2 12 7-13 1,2-Dichloroethane 21.3 1. 2 15 78-125 1,2-Dichloropropane 2.59 1. 2 13 75-125 1,3,5-Trimethylbenzene 2.68 1. 2 13 75-13 1,3-Dichlorobenzene 2.95 1. 2 15 75-13 1,4-Dichlorobenzene 2.1 1. 2 1 75-13 2-Butanone 13.96 5. 2 69.8 55-15 2-Hexanone 14.2 5. 2 7.1 6-135 4-Methyl-2-pentanone 18.6 1. 2 93 77-178 Acetone 2.81 1 2 14 6-16 Acrylonitrile 18.32 1. 2 91.6 6-14 Benzene 65.38 1. 2 45.14 11 85-125 Bromochloromethane 18.68 1. 2 93.4 75-13 Bromodichloromethane 21.4 1. 2 15 75-125 Bromoform 16.63 1. 2 83.2 6-125 Bromomethane 14.6 1. 2 7.3 3-185 Carbon disulfide 22.31 1. 2 112 6-165 Carbon tetrachloride 22.91 1. 2 115 65-14 Chlorobenzene 2.68 1. 2 13 8-12 Chloroethane 23.54 1. 2 118 5-14 Chloroform 2.4 1. 2 1 8-13 Chloromethane 21.19 1. 2 1.5 98.4 5-13 cis-1,2-dichloroethene 19.3 1. 2 96.5 75-134 cis-1,3-dichloropropene 17.49 1. 2 87.4 7-13 Dibromochloromethane 16.89 1. 2 84.4 6-115 Dibromomethane 21.31 1. 2 17 85-125 Dichlorodifluoromethane 19.6 1. 2 95.3 2-12 Ethylbenzene 21.13 1. 2 16 85-125 Hexachloroethane 14.2 1. 2 71 5-124 Isopropylbenzene 2.54 1. 2 13 8-127 m,p-xylene 44.6 2. 4 112 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 19.62 1. 2 98.1 6-16 Methyl tert-butyl ether 18.2 1. 2 9.1 8-13 Methylene chloride 22.17 5. 2 111 75-14 Naphthalene 18.34 5. 2 1.74 83 55-16 n-propylbenzene 21.51 1. 2 18 78-12 o-xylene 21.8 1. 2 15 8-125 Styrene 14.3 1. 2 7.2 85-125 Tetrachloroethene 21.58 1. 2 18 77-138 Toluene 2.49 1. 2 12 85-125 trans-1,2-dichloroethene 22.23 1. 2 111 8-14 trans-1,3-dichloropropene 16.8 1. 2 8.4 81-123 trans-1,4-dichloro-2-butene 13.7 2. 2 65.4 46-118 Trichloroethene 21.75 1. 2 19 84-13 Trichlorofluoromethane 24.38 1. 2 122 6-14 Vinyl chloride 21.25 1. 2 16 5-136 Xylenes, Total 65.68 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 2.55 2 13 75-12 Surr: 4-Bromofluorobenzene 2.61 2 13 8-11 Surr: Dibromofluoromethane 21.2 2 16 85-115 Surr: Toluene-d8 19.69 2 98.4 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: 166757-21A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo:3886189 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.66 1. 2 98.3 8-13 2.8 2.11 3 1,1,1-Trichloroethane 23.81 1. 2 119 75-13 24.12 1.29 3 1,1,2,2-Tetrachloroethane 19.8 1. 2 95.4 75-13 19.35 1.41 3 1,1,2-Trichloroethane 19.61 1. 2 98 75-125 2.4 3.95 3 1,1-Dichloroethane 21.5 1. 2 15 75-133 2.94.524 3 1,1-Dichloroethene 25.19 1. 2 126 7-145 25.13.238 3 1,2,3-Trichloropropane 19.29 1. 2 96.4 75-125 2.1 4.11 3 1,2,4-Trichlorobenzene 18.79 1. 2 94 7-135 19.27 2.52 3 1,2,4-Trimethylbenzene 19.71 1. 2 98.6 75-13 2.24 2.65 3 1,2-Dibromo-3-chloropropane 15.21 1. 2 76 6-13 15.52 2.2 3 1,2-Dibromoethane 21.21 1. 2 16 8-15 22.21 4.61 3 1,2-Dichlorobenzene 19.89 1. 2 99.4 7-13 2.36 2.34 3 1,2-Dichloroethane 21.9 1. 2 15 78-125 21.3.285 3 1,2-Dichloropropane 2.26 1. 2 11 75-125 2.59 1.62 3 1,3,5-Trimethylbenzene 2.21 1. 2 11 75-13 2.68 2.3 3 1,3-Dichlorobenzene 2.53 1. 2 13 75-13 2.95 2.3 3 1,4-Dichlorobenzene 19.81 1. 2 99 75-13 2.1 1 3 2-Butanone 13.91 5. 2 69.6 55-15 13.96.359 3 2-Hexanone 13.95 5. 2 69.8 6-135 14.2.51 3 4-Methyl-2-pentanone 17.36 1. 2 86.8 77-178 18.6 6.9 3 Acetone 22.34 1 2 112 6-16 2.81 7.9 3 Acrylonitrile 15.86 1. 2 79.3 6-14 18.32 14.4 3 Benzene 64.83 1. 2 45.14 98.4 85-125 65.38.845 3 Bromochloromethane 18.4 1. 2 9.2 75-13 18.68 3.49 3 Bromodichloromethane 21.13 1. 2 16 75-125 21.4.427 3 Bromoform 16.78 1. 2 83.9 6-125 16.63.898 3 Bromomethane 15.82 1. 2 79.1 3-185 14.6 11.8 3 Carbon disulfide 22.62 1. 2 113 6-165 22.31 1.38 3 Carbon tetrachloride 22.97 1. 2 115 65-14 22.91.262 3 Chlorobenzene 2.33 1. 2 12 8-12 2.68 1.71 3 Chloroethane 23.5 1. 2 115 5-14 23.54 2.1 3 Chloroform 19.83 1. 2 99.2 8-13 2.4 1.5 3 Chloromethane 19.88 1. 2 1.5 91.9 5-13 21.19 6.38 3 cis-1,2-dichloroethene 19.14 1. 2 95.7 75-134 19.3.832 3 cis-1,3-dichloropropene 17.82 1. 2 89.1 7-13 17.49 1.87 3 Dibromochloromethane 16.93 1. 2 84.6 6-115 16.89.237 3 Dibromomethane 21.7 1. 2 15 85-125 21.31 1.13 3 Dichlorodifluoromethane 18.73 1. 2 93.6 2-12 19.6 1.75 3 Ethylbenzene 2.69 1. 2 13 85-125 21.13 2.1 3 Hexachloroethane 14.63 1. 2 73.2 5-124 14.2 2.98 3 Isopropylbenzene 2.21 1. 2 11 8-127 2.54 1.62 3 m,p-xylene 43.56 2. 4 19 75-13 44.6 2.36 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 166873 Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 11.22 1. 2 56.1 6-16 19.62 54.5 3 Methyl tert-butyl ether 17.21 1. 2 86 8-13 18.2 4.6 3 Methylene chloride 2.8 5. 2 14 75-14 22.17 6.38 3 Naphthalene 17.29 5. 2 1.74 77.8 55-16 18.34 5.89 3 n-propylbenzene 21.2 1. 2 15 78-12 21.51 2.3 3 o-xylene 2.71 1. 2 14 8-125 21.8 1.77 3 Styrene 13.72 1. 2 68.6 85-125 14.3 2.23 3 Tetrachloroethene 21 1. 2 15 77-138 21.58 2.72 3 Toluene 2.34 1. 2 12 85-125 2.49.735 3 trans-1,2-dichloroethene 21.22 1. 2 16 8-14 22.23 4.65 3 trans-1,3-dichloropropene 15.7 1. 2 78.5 81-123 16.8 2.39 3 trans-1,4-dichloro-2-butene 12.81 2. 2 64 46-118 13.7 2.1 3 Trichloroethene 21.54 1. 2 18 84-13 21.75.97 3 Trichlorofluoromethane 23.82 1. 2 119 6-14 24.38 2.32 3 Vinyl chloride 2.97 1. 2 15 5-136 21.25 1.33 3 Xylenes, Total 64.27 3. 6 17 8-126 65.68 2.17 3 Surr: 1,2-Dichloroethane-d4 2.59 2 13 75-12 2.55.194 3 Surr: 4-Bromofluorobenzene 2.65 2 13 8-11 2.61.194 3 Surr: Dibromofluoromethane 21.9 2 15 85-115 21.2.52 3 Surr: Toluene-d8 19.75 2 98.8 85-11 19.69.34 3 SR S S The following samples were analyzed in this batch: 166873-1B QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (46 Jeni Lane) WorkOrder: 166873 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: 166873 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 2:24:54 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (731 Jeni Lane) Work Order: 16692 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 1: AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: 16692 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 16692-1 731 Jenni Lane Water 6/14/216 7:35 6/15/216 1: Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: 16692 Sample ID: 731 Jenni Lane Lab ID: 16692-1 Collection Date: 6/14/216 7:35 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/17/216 3:7 AM Sulfolane 1 µg/l 1 6/17/216 3:7 AM Surr: 2,4,6-Tribromophenol 56.1 38-115 %REC 1 6/17/216 3:7 AM Surr: 2-Fluorobiphenyl 55.3 32-1 %REC 1 6/17/216 3:7 AM Surr: 2-Fluorophenol 35.7 22-59 %REC 1 6/17/216 3:7 AM Surr: 4-Terphenyl-d14 85.6 23-112 %REC 1 6/17/216 3:7 AM Surr: Nitrobenzene-d5 61.9 31-93 %REC 1 6/17/216 3:7 AM Surr: Phenol-d6 21.4 13-36 %REC 1 6/17/216 3:7 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 6:18 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 6:18 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 6:18 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 6:18 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 6:18 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 6:18 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 6:18 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 6:18 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 2-Butanone 5. µg/l 1 6/21/216 6:18 PM 2-Hexanone 5. µg/l 1 6/21/216 6:18 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 6:18 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 6:18 PM Acetone 1 µg/l 1 6/21/216 6:18 PM Acrylonitrile 1. µg/l 1 6/21/216 6:18 PM Benzene 1. µg/l 1 6/21/216 6:18 PM Bromochloromethane 1. µg/l 1 6/21/216 6:18 PM Bromodichloromethane 1. µg/l 1 6/21/216 6:18 PM Bromoform 1. µg/l 1 6/21/216 6:18 PM Bromomethane 1. µg/l 1 6/21/216 6:18 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: 16692 Sample ID: 731 Jenni Lane Lab ID: 16692-1 Collection Date: 6/14/216 7:35 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 112 88.9 17 94. 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: 16692 Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW2-16621 The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 1.77 5 1 1.8 1-5 Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 18.58 5 1 18.6 1-5 Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 16692-1A QC Page: 2 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-16621-R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo:388617 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 21.46 2 17 75-12 Surr: 4-Bromofluorobenzene 17.99 2 9 8-11 Surr: Dibromofluoromethane 2.43 2 12 85-115 Surr: Toluene-d8 18.84 2 94.2 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW2-16621-R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo:3886169 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.57 1. 2 97.8 8-13 1,1,1-Trichloroethane 22.55 1. 2 113 75-13 1,1,2,2-Tetrachloroethane 18.67 1. 2 93.4 75-13 1,1,2-Trichloroethane 19.87 1. 2 99.4 75-125 1,1-Dichloroethane 21.59 1. 2 18 75-133 1,1-Dichloroethene 24.6 1. 2 123 7-145 1,2,3-Trichloropropane 18.99 1. 2 95 75-125 1,2,4-Trichlorobenzene 2.1 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.83 1. 2 14 75-13 1,2-Dibromo-3-chloropropane 14.85 1. 2 74.2 6-13 1,2-Dibromoethane 21.69 1. 2 18 8-15 1,2-Dichlorobenzene 2.68 1. 2 13 7-13 1,2-Dichloroethane 2.77 1. 2 14 78-125 1,2-Dichloropropane 19.91 1. 2 99.6 75-125 1,3,5-Trimethylbenzene 21.2 1. 2 16 75-13 1,3-Dichlorobenzene 21.55 1. 2 18 75-13 1,4-Dichlorobenzene 2.77 1. 2 14 75-13 2-Butanone 13.56 5. 2 67.8 55-15 2-Hexanone 13.16 5. 2 65.8 6-135 4-Methyl-2-pentanone 17.41 1. 2 87 77-178 Acetone 15.96 1 2 79.8 6-16 Acrylonitrile 15.7 1. 2 78.5 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 18.78 1. 2 93.9 75-13 Bromodichloromethane 2.47 1. 2 12 75-125 Bromoform 16.14 1. 2 8.7 6-125 Bromomethane 27.29 1. 2 136 3-185 Carbon disulfide 22.57 1. 2 113 6-165 Carbon tetrachloride 21.1 1. 2 15 65-14 Chlorobenzene 2.84 1. 2 14 8-12 Chloroethane 23.14 1. 2 116 5-14 Chloroform 19.86 1. 2 99.3 8-13 Chloromethane 14.87 1. 2 74.4 5-13 cis-1,2-dichloroethene 19.63 1. 2 98.2 75-134 cis-1,3-dichloropropene 17.96 1. 2 89.8 7-13 Dibromochloromethane 16.62 1. 2 83.1 6-115 Dibromomethane 2.68 1. 2 13 85-125 Dichlorodifluoromethane 18.35 1. 2 91.8 2-12 Ethylbenzene 21.52 1. 2 18 85-125 Hexachloroethane 14.16 1. 2 7.8 5-124 Isopropylbenzene 2.7 1. 2 14 8-127 m,p-xylene 44.74 2. 4 112 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 4.55 1. 2 23 6-16 Methyl tert-butyl ether 17.94 1. 2 89.7 8-13 Methylene chloride 23.38 5. 2 117 75-14 Naphthalene 16.24 5. 2 81.2 55-16 n-propylbenzene 22.3 1. 2 11 78-12 o-xylene 21.56 1. 2 18 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 22.69 1. 2 113 77-138 Toluene 2.43 1. 2 12 85-125 trans-1,2-dichloroethene 22.8 1. 2 114 8-14 trans-1,3-dichloropropene 16.34 1. 2 81.7 81-123 trans-1,4-dichloro-2-butene 12.84 2. 2 64.2 46-118 Trichloroethene 21.85 1. 2 19 84-13 Trichlorofluoromethane 22.88 1. 2 114 6-14 Vinyl chloride 2.66 1. 2 13 5-136 Xylenes, Total 66.3 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 2.4 2 1 75-12 Surr: 4-Bromofluorobenzene 2.4 2 1 8-11 Surr: Dibromofluoromethane 2.8 2 14 85-115 Surr: Toluene-d8 19.65 2 98.2 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: 166757-21A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo:3886188 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.8 1. 2 1 8-13 1,1,1-Trichloroethane 24.12 1. 2 121 75-13 1,1,2,2-Tetrachloroethane 19.35 1. 2 96.8 75-13 1,1,2-Trichloroethane 2.4 1. 2 12 75-125 1,1-Dichloroethane 2.94 1. 2 15 75-133 1,1-Dichloroethene 25.13 1. 2 126 7-145 1,2,3-Trichloropropane 2.1 1. 2 1 75-125 1,2,4-Trichlorobenzene 19.27 1. 2 96.4 7-135 1,2,4-Trimethylbenzene 2.24 1. 2 11 75-13 1,2-Dibromo-3-chloropropane 15.52 1. 2 77.6 6-13 1,2-Dibromoethane 22.21 1. 2 111 8-15 1,2-Dichlorobenzene 2.36 1. 2 12 7-13 1,2-Dichloroethane 21.3 1. 2 15 78-125 1,2-Dichloropropane 2.59 1. 2 13 75-125 1,3,5-Trimethylbenzene 2.68 1. 2 13 75-13 1,3-Dichlorobenzene 2.95 1. 2 15 75-13 1,4-Dichlorobenzene 2.1 1. 2 1 75-13 2-Butanone 13.96 5. 2 69.8 55-15 2-Hexanone 14.2 5. 2 7.1 6-135 4-Methyl-2-pentanone 18.6 1. 2 93 77-178 Acetone 2.81 1 2 14 6-16 Acrylonitrile 18.32 1. 2 91.6 6-14 Benzene 65.38 1. 2 45.14 11 85-125 Bromochloromethane 18.68 1. 2 93.4 75-13 Bromodichloromethane 21.4 1. 2 15 75-125 Bromoform 16.63 1. 2 83.2 6-125 Bromomethane 14.6 1. 2 7.3 3-185 Carbon disulfide 22.31 1. 2 112 6-165 Carbon tetrachloride 22.91 1. 2 115 65-14 Chlorobenzene 2.68 1. 2 13 8-12 Chloroethane 23.54 1. 2 118 5-14 Chloroform 2.4 1. 2 1 8-13 Chloromethane 21.19 1. 2 1.5 98.4 5-13 cis-1,2-dichloroethene 19.3 1. 2 96.5 75-134 cis-1,3-dichloropropene 17.49 1. 2 87.4 7-13 Dibromochloromethane 16.89 1. 2 84.4 6-115 Dibromomethane 21.31 1. 2 17 85-125 Dichlorodifluoromethane 19.6 1. 2 95.3 2-12 Ethylbenzene 21.13 1. 2 16 85-125 Hexachloroethane 14.2 1. 2 71 5-124 Isopropylbenzene 2.54 1. 2 13 8-127 m,p-xylene 44.6 2. 4 112 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 19.62 1. 2 98.1 6-16 Methyl tert-butyl ether 18.2 1. 2 9.1 8-13 Methylene chloride 22.17 5. 2 111 75-14 Naphthalene 18.34 5. 2 1.74 83 55-16 n-propylbenzene 21.51 1. 2 18 78-12 o-xylene 21.8 1. 2 15 8-125 Styrene 14.3 1. 2 7.2 85-125 Tetrachloroethene 21.58 1. 2 18 77-138 Toluene 2.49 1. 2 12 85-125 trans-1,2-dichloroethene 22.23 1. 2 111 8-14 trans-1,3-dichloropropene 16.8 1. 2 8.4 81-123 trans-1,4-dichloro-2-butene 13.7 2. 2 65.4 46-118 Trichloroethene 21.75 1. 2 19 84-13 Trichlorofluoromethane 24.38 1. 2 122 6-14 Vinyl chloride 21.25 1. 2 16 5-136 Xylenes, Total 65.68 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 2.55 2 13 75-12 Surr: 4-Bromofluorobenzene 2.61 2 13 8-11 Surr: Dibromofluoromethane 21.2 2 16 85-115 Surr: Toluene-d8 19.69 2 98.4 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: 166757-21A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo:3886189 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.66 1. 2 98.3 8-13 2.8 2.11 3 1,1,1-Trichloroethane 23.81 1. 2 119 75-13 24.12 1.29 3 1,1,2,2-Tetrachloroethane 19.8 1. 2 95.4 75-13 19.35 1.41 3 1,1,2-Trichloroethane 19.61 1. 2 98 75-125 2.4 3.95 3 1,1-Dichloroethane 21.5 1. 2 15 75-133 2.94.524 3 1,1-Dichloroethene 25.19 1. 2 126 7-145 25.13.238 3 1,2,3-Trichloropropane 19.29 1. 2 96.4 75-125 2.1 4.11 3 1,2,4-Trichlorobenzene 18.79 1. 2 94 7-135 19.27 2.52 3 1,2,4-Trimethylbenzene 19.71 1. 2 98.6 75-13 2.24 2.65 3 1,2-Dibromo-3-chloropropane 15.21 1. 2 76 6-13 15.52 2.2 3 1,2-Dibromoethane 21.21 1. 2 16 8-15 22.21 4.61 3 1,2-Dichlorobenzene 19.89 1. 2 99.4 7-13 2.36 2.34 3 1,2-Dichloroethane 21.9 1. 2 15 78-125 21.3.285 3 1,2-Dichloropropane 2.26 1. 2 11 75-125 2.59 1.62 3 1,3,5-Trimethylbenzene 2.21 1. 2 11 75-13 2.68 2.3 3 1,3-Dichlorobenzene 2.53 1. 2 13 75-13 2.95 2.3 3 1,4-Dichlorobenzene 19.81 1. 2 99 75-13 2.1 1 3 2-Butanone 13.91 5. 2 69.6 55-15 13.96.359 3 2-Hexanone 13.95 5. 2 69.8 6-135 14.2.51 3 4-Methyl-2-pentanone 17.36 1. 2 86.8 77-178 18.6 6.9 3 Acetone 22.34 1 2 112 6-16 2.81 7.9 3 Acrylonitrile 15.86 1. 2 79.3 6-14 18.32 14.4 3 Benzene 64.83 1. 2 45.14 98.4 85-125 65.38.845 3 Bromochloromethane 18.4 1. 2 9.2 75-13 18.68 3.49 3 Bromodichloromethane 21.13 1. 2 16 75-125 21.4.427 3 Bromoform 16.78 1. 2 83.9 6-125 16.63.898 3 Bromomethane 15.82 1. 2 79.1 3-185 14.6 11.8 3 Carbon disulfide 22.62 1. 2 113 6-165 22.31 1.38 3 Carbon tetrachloride 22.97 1. 2 115 65-14 22.91.262 3 Chlorobenzene 2.33 1. 2 12 8-12 2.68 1.71 3 Chloroethane 23.5 1. 2 115 5-14 23.54 2.1 3 Chloroform 19.83 1. 2 99.2 8-13 2.4 1.5 3 Chloromethane 19.88 1. 2 1.5 91.9 5-13 21.19 6.38 3 cis-1,2-dichloroethene 19.14 1. 2 95.7 75-134 19.3.832 3 cis-1,3-dichloropropene 17.82 1. 2 89.1 7-13 17.49 1.87 3 Dibromochloromethane 16.93 1. 2 84.6 6-115 16.89.237 3 Dibromomethane 21.7 1. 2 15 85-125 21.31 1.13 3 Dichlorodifluoromethane 18.73 1. 2 93.6 2-12 19.6 1.75 3 Ethylbenzene 2.69 1. 2 13 85-125 21.13 2.1 3 Hexachloroethane 14.63 1. 2 73.2 5-124 14.2 2.98 3 Isopropylbenzene 2.21 1. 2 11 8-127 2.54 1.62 3 m,p-xylene 43.56 2. 4 19 75-13 44.6 2.36 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 16692 Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 11.22 1. 2 56.1 6-16 19.62 54.5 3 Methyl tert-butyl ether 17.21 1. 2 86 8-13 18.2 4.6 3 Methylene chloride 2.8 5. 2 14 75-14 22.17 6.38 3 Naphthalene 17.29 5. 2 1.74 77.8 55-16 18.34 5.89 3 n-propylbenzene 21.2 1. 2 15 78-12 21.51 2.3 3 o-xylene 2.71 1. 2 14 8-125 21.8 1.77 3 Styrene 13.72 1. 2 68.6 85-125 14.3 2.23 3 Tetrachloroethene 21 1. 2 15 77-138 21.58 2.72 3 Toluene 2.34 1. 2 12 85-125 2.49.735 3 trans-1,2-dichloroethene 21.22 1. 2 16 8-14 22.23 4.65 3 trans-1,3-dichloropropene 15.7 1. 2 78.5 81-123 16.8 2.39 3 trans-1,4-dichloro-2-butene 12.81 2. 2 64 46-118 13.7 2.1 3 Trichloroethene 21.54 1. 2 18 84-13 21.75.97 3 Trichlorofluoromethane 23.82 1. 2 119 6-14 24.38 2.32 3 Vinyl chloride 2.97 1. 2 15 5-136 21.25 1.33 3 Xylenes, Total 64.27 3. 6 17 8-126 65.68 2.17 3 Surr: 1,2-Dichloroethane-d4 2.59 2 13 75-12 2.55.194 3 Surr: 4-Bromofluorobenzene 2.65 2 13 8-11 2.61.194 3 Surr: Dibromofluoromethane 21.9 2 15 85-115 21.2.52 3 Surr: Toluene-d8 19.75 2 98.8 85-11 19.69.34 3 SR S S The following samples were analyzed in this batch: 16692-1B QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (731 Jeni Lane) WorkOrder: 16692 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 1: Work Order: 16692 Received by: MEB Checklist completed by Meghan Broadbent Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: water Carrier name: UPS 16-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 6./6. SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 4:33:22 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (477 Jeni Lane) Work Order: 166884 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: 166884 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166884-1 477 Jeni Lane Water 6/13/216 16:1 6/15/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: 166884 Sample ID: 477 Jeni Lane Lab ID: 166884-1 Collection Date: 6/13/216 4:1 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/17/216 2:7 AM Sulfolane 1 µg/l 1 6/17/216 2:7 AM Surr: 2,4,6-Tribromophenol 58. 38-115 %REC 1 6/17/216 2:7 AM Surr: 2-Fluorobiphenyl 52.3 32-1 %REC 1 6/17/216 2:7 AM Surr: 2-Fluorophenol 37.1 22-59 %REC 1 6/17/216 2:7 AM Surr: 4-Terphenyl-d14 85.7 23-112 %REC 1 6/17/216 2:7 AM Surr: Nitrobenzene-d5 6.1 31-93 %REC 1 6/17/216 2:7 AM Surr: Phenol-d6 22.3 13-36 %REC 1 6/17/216 2:7 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 5:5 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 5:5 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 5:5 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 5:5 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 5:5 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 5:5 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 5:5 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 5:5 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 2-Butanone 5. µg/l 1 6/21/216 5:5 PM 2-Hexanone 5. µg/l 1 6/21/216 5:5 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 5:5 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 5:5 PM Acetone 1 µg/l 1 6/21/216 5:5 PM Acrylonitrile 1. µg/l 1 6/21/216 5:5 PM Benzene 1. µg/l 1 6/21/216 5:5 PM Bromochloromethane 1. µg/l 1 6/21/216 5:5 PM Bromodichloromethane 1. µg/l 1 6/21/216 5:5 PM Bromoform 1. µg/l 1 6/21/216 5:5 PM Bromomethane 1. µg/l 1 6/21/216 5:5 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: 166884 Sample ID: 477 Jeni Lane Lab ID: 166884-1 Collection Date: 6/13/216 4:1 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 11 91.6 18 95.3 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: 166884 Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW2-16621 The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 1.77 5 1 1.8 1-5 Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 18.58 5 1 18.6 1-5 Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 166884-1A QC Page: 2 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-16621-R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo:388617 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 21.46 2 17 75-12 Surr: 4-Bromofluorobenzene 17.99 2 9 8-11 Surr: Dibromofluoromethane 2.43 2 12 85-115 Surr: Toluene-d8 18.84 2 94.2 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW2-16621-R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo:3886169 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.57 1. 2 97.8 8-13 1,1,1-Trichloroethane 22.55 1. 2 113 75-13 1,1,2,2-Tetrachloroethane 18.67 1. 2 93.4 75-13 1,1,2-Trichloroethane 19.87 1. 2 99.4 75-125 1,1-Dichloroethane 21.59 1. 2 18 75-133 1,1-Dichloroethene 24.6 1. 2 123 7-145 1,2,3-Trichloropropane 18.99 1. 2 95 75-125 1,2,4-Trichlorobenzene 2.1 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.83 1. 2 14 75-13 1,2-Dibromo-3-chloropropane 14.85 1. 2 74.2 6-13 1,2-Dibromoethane 21.69 1. 2 18 8-15 1,2-Dichlorobenzene 2.68 1. 2 13 7-13 1,2-Dichloroethane 2.77 1. 2 14 78-125 1,2-Dichloropropane 19.91 1. 2 99.6 75-125 1,3,5-Trimethylbenzene 21.2 1. 2 16 75-13 1,3-Dichlorobenzene 21.55 1. 2 18 75-13 1,4-Dichlorobenzene 2.77 1. 2 14 75-13 2-Butanone 13.56 5. 2 67.8 55-15 2-Hexanone 13.16 5. 2 65.8 6-135 4-Methyl-2-pentanone 17.41 1. 2 87 77-178 Acetone 15.96 1 2 79.8 6-16 Acrylonitrile 15.7 1. 2 78.5 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 18.78 1. 2 93.9 75-13 Bromodichloromethane 2.47 1. 2 12 75-125 Bromoform 16.14 1. 2 8.7 6-125 Bromomethane 27.29 1. 2 136 3-185 Carbon disulfide 22.57 1. 2 113 6-165 Carbon tetrachloride 21.1 1. 2 15 65-14 Chlorobenzene 2.84 1. 2 14 8-12 Chloroethane 23.14 1. 2 116 5-14 Chloroform 19.86 1. 2 99.3 8-13 Chloromethane 14.87 1. 2 74.4 5-13 cis-1,2-dichloroethene 19.63 1. 2 98.2 75-134 cis-1,3-dichloropropene 17.96 1. 2 89.8 7-13 Dibromochloromethane 16.62 1. 2 83.1 6-115 Dibromomethane 2.68 1. 2 13 85-125 Dichlorodifluoromethane 18.35 1. 2 91.8 2-12 Ethylbenzene 21.52 1. 2 18 85-125 Hexachloroethane 14.16 1. 2 7.8 5-124 Isopropylbenzene 2.7 1. 2 14 8-127 m,p-xylene 44.74 2. 4 112 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 4.55 1. 2 23 6-16 Methyl tert-butyl ether 17.94 1. 2 89.7 8-13 Methylene chloride 23.38 5. 2 117 75-14 Naphthalene 16.24 5. 2 81.2 55-16 n-propylbenzene 22.3 1. 2 11 78-12 o-xylene 21.56 1. 2 18 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 22.69 1. 2 113 77-138 Toluene 2.43 1. 2 12 85-125 trans-1,2-dichloroethene 22.8 1. 2 114 8-14 trans-1,3-dichloropropene 16.34 1. 2 81.7 81-123 trans-1,4-dichloro-2-butene 12.84 2. 2 64.2 46-118 Trichloroethene 21.85 1. 2 19 84-13 Trichlorofluoromethane 22.88 1. 2 114 6-14 Vinyl chloride 2.66 1. 2 13 5-136 Xylenes, Total 66.3 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 2.4 2 1 75-12 Surr: 4-Bromofluorobenzene 2.4 2 1 8-11 Surr: Dibromofluoromethane 2.8 2 14 85-115 Surr: Toluene-d8 19.65 2 98.2 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: 166757-21A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo:3886188 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.8 1. 2 1 8-13 1,1,1-Trichloroethane 24.12 1. 2 121 75-13 1,1,2,2-Tetrachloroethane 19.35 1. 2 96.8 75-13 1,1,2-Trichloroethane 2.4 1. 2 12 75-125 1,1-Dichloroethane 2.94 1. 2 15 75-133 1,1-Dichloroethene 25.13 1. 2 126 7-145 1,2,3-Trichloropropane 2.1 1. 2 1 75-125 1,2,4-Trichlorobenzene 19.27 1. 2 96.4 7-135 1,2,4-Trimethylbenzene 2.24 1. 2 11 75-13 1,2-Dibromo-3-chloropropane 15.52 1. 2 77.6 6-13 1,2-Dibromoethane 22.21 1. 2 111 8-15 1,2-Dichlorobenzene 2.36 1. 2 12 7-13 1,2-Dichloroethane 21.3 1. 2 15 78-125 1,2-Dichloropropane 2.59 1. 2 13 75-125 1,3,5-Trimethylbenzene 2.68 1. 2 13 75-13 1,3-Dichlorobenzene 2.95 1. 2 15 75-13 1,4-Dichlorobenzene 2.1 1. 2 1 75-13 2-Butanone 13.96 5. 2 69.8 55-15 2-Hexanone 14.2 5. 2 7.1 6-135 4-Methyl-2-pentanone 18.6 1. 2 93 77-178 Acetone 2.81 1 2 14 6-16 Acrylonitrile 18.32 1. 2 91.6 6-14 Benzene 65.38 1. 2 45.14 11 85-125 Bromochloromethane 18.68 1. 2 93.4 75-13 Bromodichloromethane 21.4 1. 2 15 75-125 Bromoform 16.63 1. 2 83.2 6-125 Bromomethane 14.6 1. 2 7.3 3-185 Carbon disulfide 22.31 1. 2 112 6-165 Carbon tetrachloride 22.91 1. 2 115 65-14 Chlorobenzene 2.68 1. 2 13 8-12 Chloroethane 23.54 1. 2 118 5-14 Chloroform 2.4 1. 2 1 8-13 Chloromethane 21.19 1. 2 1.5 98.4 5-13 cis-1,2-dichloroethene 19.3 1. 2 96.5 75-134 cis-1,3-dichloropropene 17.49 1. 2 87.4 7-13 Dibromochloromethane 16.89 1. 2 84.4 6-115 Dibromomethane 21.31 1. 2 17 85-125 Dichlorodifluoromethane 19.6 1. 2 95.3 2-12 Ethylbenzene 21.13 1. 2 16 85-125 Hexachloroethane 14.2 1. 2 71 5-124 Isopropylbenzene 2.54 1. 2 13 8-127 m,p-xylene 44.6 2. 4 112 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 19.62 1. 2 98.1 6-16 Methyl tert-butyl ether 18.2 1. 2 9.1 8-13 Methylene chloride 22.17 5. 2 111 75-14 Naphthalene 18.34 5. 2 1.74 83 55-16 n-propylbenzene 21.51 1. 2 18 78-12 o-xylene 21.8 1. 2 15 8-125 Styrene 14.3 1. 2 7.2 85-125 Tetrachloroethene 21.58 1. 2 18 77-138 Toluene 2.49 1. 2 12 85-125 trans-1,2-dichloroethene 22.23 1. 2 111 8-14 trans-1,3-dichloropropene 16.8 1. 2 8.4 81-123 trans-1,4-dichloro-2-butene 13.7 2. 2 65.4 46-118 Trichloroethene 21.75 1. 2 19 84-13 Trichlorofluoromethane 24.38 1. 2 122 6-14 Vinyl chloride 21.25 1. 2 16 5-136 Xylenes, Total 65.68 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 2.55 2 13 75-12 Surr: 4-Bromofluorobenzene 2.61 2 13 8-11 Surr: Dibromofluoromethane 21.2 2 16 85-115 Surr: Toluene-d8 19.69 2 98.4 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: 166757-21A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo:3886189 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.66 1. 2 98.3 8-13 2.8 2.11 3 1,1,1-Trichloroethane 23.81 1. 2 119 75-13 24.12 1.29 3 1,1,2,2-Tetrachloroethane 19.8 1. 2 95.4 75-13 19.35 1.41 3 1,1,2-Trichloroethane 19.61 1. 2 98 75-125 2.4 3.95 3 1,1-Dichloroethane 21.5 1. 2 15 75-133 2.94.524 3 1,1-Dichloroethene 25.19 1. 2 126 7-145 25.13.238 3 1,2,3-Trichloropropane 19.29 1. 2 96.4 75-125 2.1 4.11 3 1,2,4-Trichlorobenzene 18.79 1. 2 94 7-135 19.27 2.52 3 1,2,4-Trimethylbenzene 19.71 1. 2 98.6 75-13 2.24 2.65 3 1,2-Dibromo-3-chloropropane 15.21 1. 2 76 6-13 15.52 2.2 3 1,2-Dibromoethane 21.21 1. 2 16 8-15 22.21 4.61 3 1,2-Dichlorobenzene 19.89 1. 2 99.4 7-13 2.36 2.34 3 1,2-Dichloroethane 21.9 1. 2 15 78-125 21.3.285 3 1,2-Dichloropropane 2.26 1. 2 11 75-125 2.59 1.62 3 1,3,5-Trimethylbenzene 2.21 1. 2 11 75-13 2.68 2.3 3 1,3-Dichlorobenzene 2.53 1. 2 13 75-13 2.95 2.3 3 1,4-Dichlorobenzene 19.81 1. 2 99 75-13 2.1 1 3 2-Butanone 13.91 5. 2 69.6 55-15 13.96.359 3 2-Hexanone 13.95 5. 2 69.8 6-135 14.2.51 3 4-Methyl-2-pentanone 17.36 1. 2 86.8 77-178 18.6 6.9 3 Acetone 22.34 1 2 112 6-16 2.81 7.9 3 Acrylonitrile 15.86 1. 2 79.3 6-14 18.32 14.4 3 Benzene 64.83 1. 2 45.14 98.4 85-125 65.38.845 3 Bromochloromethane 18.4 1. 2 9.2 75-13 18.68 3.49 3 Bromodichloromethane 21.13 1. 2 16 75-125 21.4.427 3 Bromoform 16.78 1. 2 83.9 6-125 16.63.898 3 Bromomethane 15.82 1. 2 79.1 3-185 14.6 11.8 3 Carbon disulfide 22.62 1. 2 113 6-165 22.31 1.38 3 Carbon tetrachloride 22.97 1. 2 115 65-14 22.91.262 3 Chlorobenzene 2.33 1. 2 12 8-12 2.68 1.71 3 Chloroethane 23.5 1. 2 115 5-14 23.54 2.1 3 Chloroform 19.83 1. 2 99.2 8-13 2.4 1.5 3 Chloromethane 19.88 1. 2 1.5 91.9 5-13 21.19 6.38 3 cis-1,2-dichloroethene 19.14 1. 2 95.7 75-134 19.3.832 3 cis-1,3-dichloropropene 17.82 1. 2 89.1 7-13 17.49 1.87 3 Dibromochloromethane 16.93 1. 2 84.6 6-115 16.89.237 3 Dibromomethane 21.7 1. 2 15 85-125 21.31 1.13 3 Dichlorodifluoromethane 18.73 1. 2 93.6 2-12 19.6 1.75 3 Ethylbenzene 2.69 1. 2 13 85-125 21.13 2.1 3 Hexachloroethane 14.63 1. 2 73.2 5-124 14.2 2.98 3 Isopropylbenzene 2.21 1. 2 11 8-127 2.54 1.62 3 m,p-xylene 43.56 2. 4 19 75-13 44.6 2.36 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 166884 Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 11.22 1. 2 56.1 6-16 19.62 54.5 3 Methyl tert-butyl ether 17.21 1. 2 86 8-13 18.2 4.6 3 Methylene chloride 2.8 5. 2 14 75-14 22.17 6.38 3 Naphthalene 17.29 5. 2 1.74 77.8 55-16 18.34 5.89 3 n-propylbenzene 21.2 1. 2 15 78-12 21.51 2.3 3 o-xylene 2.71 1. 2 14 8-125 21.8 1.77 3 Styrene 13.72 1. 2 68.6 85-125 14.3 2.23 3 Tetrachloroethene 21 1. 2 15 77-138 21.58 2.72 3 Toluene 2.34 1. 2 12 85-125 2.49.735 3 trans-1,2-dichloroethene 21.22 1. 2 16 8-14 22.23 4.65 3 trans-1,3-dichloropropene 15.7 1. 2 78.5 81-123 16.8 2.39 3 trans-1,4-dichloro-2-butene 12.81 2. 2 64 46-118 13.7 2.1 3 Trichloroethene 21.54 1. 2 18 84-13 21.75.97 3 Trichlorofluoromethane 23.82 1. 2 119 6-14 24.38 2.32 3 Vinyl chloride 2.97 1. 2 15 5-136 21.25 1.33 3 Xylenes, Total 64.27 3. 6 17 8-126 65.68 2.17 3 Surr: 1,2-Dichloroethane-d4 2.59 2 13 75-12 2.55.194 3 Surr: 4-Bromofluorobenzene 2.65 2 13 8-11 2.61.194 3 Surr: Dibromofluoromethane 21.9 2 15 85-115 21.2.52 3 Surr: Toluene-d8 19.75 2 98.8 85-11 19.69.34 3 SR S S The following samples were analyzed in this batch: 166884-1B QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (477 Jeni Lane) WorkOrder: 166884 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: 166884 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 3:15:3 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (Hartland - 495 Jeni Lane) Work Order: 166478 Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 495 Jeni Lane) Work Order: 166478 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166478-1 495 Jeni Lane Water 6/6/216 18:36 6/8/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 495 Jeni Lane) Work Order: 166478 Sample ID: 495 Jeni Lane Lab ID: 166478-1 Collection Date: 6/6/216 6:36 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 7:37 PM Sulfolane 1 µg/l 1 6/9/216 7:37 PM Surr: 2,4,6-Tribromophenol 63.3 38-115 %REC 1 6/9/216 7:37 PM Surr: 2-Fluorobiphenyl 54.8 32-1 %REC 1 6/9/216 7:37 PM Surr: 2-Fluorophenol 33.9 22-59 %REC 1 6/9/216 7:37 PM Surr: 4-Terphenyl-d14 75.7 23-112 %REC 1 6/9/216 7:37 PM Surr: Nitrobenzene-d5 65.8 31-93 %REC 1 6/9/216 7:37 PM Surr: Phenol-d6 17.4 13-36 %REC 1 6/9/216 7:37 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 5:5 AM 1,1-Dichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1-Dichloroethene 1. µg/l 1 6/9/216 5:5 AM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 5:5 AM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 5:5 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 5:5 AM 1,2-Dibromoethane 1. µg/l 1 6/9/216 5:5 AM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 1,2-Dichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,2-Dichloropropane 1. µg/l 1 6/9/216 5:5 AM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 5:5 AM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 2-Butanone 5. µg/l 1 6/9/216 5:5 AM 2-Hexanone 5. µg/l 1 6/9/216 5:5 AM 2-Methylnaphthalene 5. µg/l 1 6/9/216 5:5 AM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 5:5 AM Acetone 1 µg/l 1 6/9/216 5:5 AM Acrylonitrile 1. µg/l 1 6/9/216 5:5 AM Benzene 1. µg/l 1 6/9/216 5:5 AM Bromochloromethane 1. µg/l 1 6/9/216 5:5 AM Bromodichloromethane 1. µg/l 1 6/9/216 5:5 AM Bromoform 1. µg/l 1 6/9/216 5:5 AM Bromomethane 1. µg/l 1 6/9/216 5:5 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 495 Jeni Lane) Work Order: 166478 Sample ID: 495 Jeni Lane Lab ID: 166478-1 Collection Date: 6/6/216 6:36 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 92.2 94.8 96.6 94. 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 495 Jeni Lane) Work Order: 166478 Date: 1-Jun-16 Case Narrative Batch R189191a The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo:387197 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 21.75 5 43.5 38-115 Surr: 2-Fluorobiphenyl 21.56 5 43.1 32-1 Surr: 2-Fluorophenol 16.37 5 32.7 22-59 Surr: 4-Terphenyl-d14 35.69 5 71.4 23-112 Surr: Nitrobenzene-d5 28.3 5 56.1 31-93 Surr: Phenol-d6 7.63 5 15.3 13-36 LCS Sample ID: SLCSW1-8717-8717 Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo:387198 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5.75 5 1 5.75 5-4 Sulfolane 54.53 1 1 54.5 3-1 Surr: 2,4,6-Tribromophenol 27.91 5 55.8 38-115 Surr: 2-Fluorobiphenyl 28.51 5 57 32-1 Surr: 2-Fluorophenol 19.32 5 38.6 22-59 Surr: 4-Terphenyl-d14 37.7 5 75.4 23-112 Surr: Nitrobenzene-d5 35.21 5 7.4 31-93 Surr: Phenol-d6 1.2 5 2 13-36 MS Sample ID: 166476-1B MS Units:µg/L Analysis Date: 6/9/216 6:36 PM Client ID: Run ID: SVMS8_1669A SeqNo:387199 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 53 16.4 13.2 5-4 Sulfolane 65.27 11 16.4 61.4 3-1 Surr: 2,4,6-Tribromophenol 36.5 53.19 67.8 38-115 Surr: 2-Fluorobiphenyl 31.76 53.19 59.7 32-1 Surr: 2-Fluorophenol 2.45 53.19 38.4 22-59 Surr: 4-Terphenyl-d14 38.93 53.19 73.2 23-112 Surr: Nitrobenzene-d5 38.12 53.19 71.7 31-93 Surr: Phenol-d6 1.87 53.19 2.4 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: 8717 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166478-1B DUP Client ID: 495 Jeni Lane Run ID: SVMS8_1669A Units:µg/L SeqNo:38721 Analysis Date: 6/9/216 7:16 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 32.53 53.2 61.4 38-115 31.66 2.72 4 Surr: 2-Fluorobiphenyl 29.9 53.2 56.4 32-1 27.39 8.78 4 Surr: 2-Fluorophenol 18.87 53.2 35.6 22-59 16.97 1.6 4 Surr: 4-Terphenyl-d14 35.97 53.2 67.8 23-112 37.85 5.9 4 Surr: Nitrobenzene-d5 35.12 53.2 66.2 31-93 32.88 6.59 4 Surr: Phenol-d6 9.3 53.2 17.5 13-36 8.71 6.55 4 The following samples were analyzed in this batch: 166478-1B QC Page: 2 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MBLK Sample ID: VBLKW2-1668-R189191a Units:µg/L Analysis Date: 6/9/216 2:2 AM Client ID: Run ID: VMS6_1668B SeqNo:3868131 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 18.19 2 91 75-12 Surr: 4-Bromofluorobenzene 19.42 2 97.1 8-11 Surr: Dibromofluoromethane 19.84 2 99.2 85-115 Surr: Toluene-d8 19.6 2 95.3 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B LCS Sample ID: VLCSW2-1668-R189191a Units:µg/L Analysis Date: 6/9/216 1:12 AM Client ID: Run ID: VMS6_1668B SeqNo:3868128 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.57 1. 2 13 8-13 1,1,1-Trichloroethane 2.5 1. 2 12 75-13 1,1,2,2-Tetrachloroethane 21.66 1. 2 18 75-13 1,1,2-Trichloroethane 19.85 1. 2 99.2 75-125 1,1-Dichloroethane 19.12 1. 2 95.6 75-133 1,1-Dichloroethene 19.91 1. 2 99.6 7-145 1,2,3-Trichloropropane 2.71 1. 2 14 75-125 1,2,4-Trichlorobenzene 2.9 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.32 1. 2 12 75-13 1,2-Dibromo-3-chloropropane 18.85 1. 2 94.2 6-13 1,2-Dibromoethane 21.31 1. 2 17 8-15 1,2-Dichlorobenzene 2.37 1. 2 12 7-13 1,2-Dichloroethane 18.84 1. 2 94.2 78-125 1,2-Dichloropropane 2.5 1. 2 1 75-125 1,3,5-Trimethylbenzene 2.7 1. 2 14 75-13 1,3-Dichlorobenzene 2.13 1. 2 11 75-13 1,4-Dichlorobenzene 18.8 1. 2 94 75-13 2-Butanone 18.19 5. 2 91 55-15 2-Hexanone 17.68 5. 2 88.4 6-135 4-Methyl-2-pentanone 24.96 1. 2 125 77-178 Acetone 19.47 1 2 97.4 6-16 Acrylonitrile 18.61 1. 2 93 6-14 Benzene 2.49 1. 2 12 85-125 Bromochloromethane 18.44 1. 2 92.2 75-13 Bromodichloromethane 2.1 1. 2 1 75-125 Bromoform 19.96 1. 2 99.8 6-125 Bromomethane 18.62 1. 2 93.1 3-185 Carbon disulfide 2.24 1. 2 11 6-165 Carbon tetrachloride 19.79 1. 2 99 65-14 Chlorobenzene 19.3 1. 2 96.5 8-12 Chloroethane 23.37 1. 2 117 5-14 Chloroform 18.19 1. 2 91 8-13 Chloromethane 15.16 1. 2 75.8 5-13 cis-1,2-dichloroethene 17.74 1. 2 88.7 75-134 cis-1,3-dichloropropene 2.29 1. 2 11 7-13 Dibromochloromethane 19.2 1. 2 95.1 6-115 Dibromomethane 2.48 1. 2 12 85-125 Dichlorodifluoromethane 19.67 1. 2 98.4 2-12 Ethylbenzene 19.65 1. 2 98.2 85-125 Hexachloroethane 15.39 1. 2 77 5-124 Isopropylbenzene 2.62 1. 2 13 8-127 m,p-xylene 4.98 2. 4 12 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 12.7 1. 2 63.5 6-16 Methyl tert-butyl ether 18 1. 2 9 8-13 Methylene chloride 17.88 5. 2 89.4 75-14 Naphthalene 21.87 5. 2 19 55-16 n-propylbenzene 2.14 1. 2 11 78-12 o-xylene 19.28 1. 2 96.4 8-125 Styrene 21.3 1. 2 15 85-125 Tetrachloroethene 2.34 1. 2 12 77-138 Toluene 19.4 1. 2 97 85-125 trans-1,2-dichloroethene 18.95 1. 2 94.8 8-14 trans-1,3-dichloropropene 16.82 1. 2 84.1 81-123 trans-1,4-dichloro-2-butene 12.14 2. 2 6.7 46-118 Trichloroethene 2.81 1. 2 14 84-13 Trichlorofluoromethane 19.62 1. 2 98.1 6-14 Vinyl chloride 19.82 1. 2 99.1 5-136 Xylenes, Total 6.26 3. 6 1 8-126 Surr: 1,2-Dichloroethane-d4 17.86 2 89.3 75-12 Surr: 4-Bromofluorobenzene 2.13 2 11 8-11 Surr: Dibromofluoromethane 19.75 2 98.8 85-115 Surr: Toluene-d8 18.98 2 94.9 85-11 QC Page: 6 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MS Sample ID: 16641-15A MS Units:µg/L Analysis Date: 6/9/216 1:53 AM Client ID: Run ID: VMS6_1668B SeqNo:3868146 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 227 1 2 11 8-13 1,1,1-Trichloroethane 2176 1 2 19 75-13 1,1,2,2-Tetrachloroethane 298 1 2 15 75-13 1,1,2-Trichloroethane 1988 1 2 99.4 75-125 1,1-Dichloroethane 272 1 2 14 75-133 1,1-Dichloroethene 2225 1 2 111 7-145 1,2,3-Trichloropropane 1968 1 2 98.4 75-125 1,2,4-Trichlorobenzene 1814 1 2 9.7 7-135 1,2,4-Trimethylbenzene 3856 1 2 1781 14 75-13 1,2-Dibromo-3-chloropropane 1598 1 2 79.9 6-13 1,2-Dibromoethane 229 1 2 11 8-15 1,2-Dichlorobenzene 1913 1 2 95.6 7-13 1,2-Dichloroethane 1936 1 2 96.8 78-125 1,2-Dichloropropane 224 1 2 11 75-125 1,3,5-Trimethylbenzene 2485 1 2 44 12 75-13 1,3-Dichlorobenzene 1859 1 2 93 75-13 1,4-Dichlorobenzene 1771 1 2 88.6 75-13 2-Butanone 1554 5 2 77.7 55-15 2-Hexanone 168 5 2 84 6-135 4-Methyl-2-pentanone 2333 1 2 117 77-178 Acetone 2157 1, 2 18 6-16 Acrylonitrile 161 1 2 8.5 6-14 Benzene 151 1 2 7878 132 85-125 Bromochloromethane 1882 1 2 94.1 75-13 Bromodichloromethane 1999 1 2 1 75-125 Bromoform 181 1 2 9 6-125 Bromomethane 787 1 2 39.4 3-185 Carbon disulfide 25 1 2 1 6-165 Carbon tetrachloride 257 1 2 13 65-14 Chlorobenzene 1989 1 2 99.4 8-12 Chloroethane 3158 1 2 158 5-14 Chloroform 1881 1 2 94 8-13 Chloromethane 144 1 2 72 5-13 cis-1,2-dichloroethene 1836 1 2 91.8 75-134 cis-1,3-dichloropropene 1983 1 2 99.2 7-13 Dibromochloromethane 1793 1 2 89.6 6-115 Dibromomethane 27 1 2 14 85-125 Dichlorodifluoromethane 265 1 2 13 2-12 Ethylbenzene 424 1 2 2217 11 85-125 Hexachloroethane 1383 1 2 69.2 5-124 Isopropylbenzene 2155 1 2 9 13 8-127 m,p-xylene 1212 2 4 8137 99.5 75-13 SE S QC Page: 7 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 713 1 2 35.6 6-16 Methyl tert-butyl ether 1823 1 2 91.2 8-13 Methylene chloride 196 5 2 95.3 75-14 Naphthalene 23 5 2 372 96.4 55-16 n-propylbenzene 2251 1 2 243 1 78-12 o-xylene 5588 1 2 3675 95.6 8-125 Styrene 22 1 2 11 85-125 Tetrachloroethene 263 1 2 13 77-138 Toluene 1167 1 2 9459 111 85-125 trans-1,2-dichloroethene 235 1 2 12 8-14 trans-1,3-dichloropropene 158 1 2 79 81-123 trans-1,4-dichloro-2-butene 184 2 2 54.2 46-118 Trichloroethene 2218 1 2 111 84-13 Trichlorofluoromethane 2239 1 2 112 6-14 Vinyl chloride 2122 1 2 16 5-136 Xylenes, Total 1771 3 6 1181 98.2 8-126 Surr: 1,2-Dichloroethane-d4 1818 2 9.9 75-12 Surr: 4-Bromofluorobenzene 211 2 11 8-11 Surr: Dibromofluoromethane 194 2 97 85-115 Surr: Toluene-d8 1912 2 95.6 85-11 S EO S QC Page: 8 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MSD Sample ID: 16641-15A MSD Units:µg/L Analysis Date: 6/9/216 11:18 AM Client ID: Run ID: VMS6_1668B SeqNo:3868147 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2 1 2 1 8-13 227 1.34 3 1,1,1-Trichloroethane 294 1 2 15 75-13 2176 3.84 3 1,1,2,2-Tetrachloroethane 228 1 2 11 75-13 298 3.39 3 1,1,2-Trichloroethane 1862 1 2 93.1 75-125 1988 6.55 3 1,1-Dichloroethane 1943 1 2 97.2 75-133 272 6.43 3 1,1-Dichloroethene 2156 1 2 18 7-145 2225 3.15 3 1,2,3-Trichloropropane 1869 1 2 93.4 75-125 1968 5.16 3 1,2,4-Trichlorobenzene 1877 1 2 93.8 7-135 1814 3.41 3 1,2,4-Trimethylbenzene 552 1 2 1781 186 75-13 3856 35.2 3 1,2-Dibromo-3-chloropropane 1518 1 2 75.9 6-13 1598 5.13 3 1,2-Dibromoethane 196 1 2 98 8-15 229 3.46 3 1,2-Dichlorobenzene 1939 1 2 97 7-13 1913 1.35 3 1,2-Dichloroethane 1818 1 2 9.9 78-125 1936 6.29 3 1,2-Dichloropropane 1959 1 2 98 75-125 224 3.26 3 1,3,5-Trimethylbenzene 2975 1 2 44 127 75-13 2485 17.9 3 1,3-Dichlorobenzene 1918 1 2 95.9 75-13 1859 3.12 3 1,4-Dichlorobenzene 1834 1 2 91.7 75-13 1771 3.5 3 2-Butanone 161 5 2 8.5 55-15 1554 3.54 3 2-Hexanone 167 5 2 8.4 6-135 168 4.44 3 4-Methyl-2-pentanone 223 1 2 112 77-178 2333 4.51 3 Acetone 228 1, 2 11 6-16 2157 2.34 3 Acrylonitrile 1516 1 2 75.8 6-14 161 6.1 3 Benzene 1775 1 2 7878 494 85-125 151 51.3 3 Bromochloromethane 18 1 2 9 75-13 1882 4.45 3 Bromodichloromethane 191 1 2 95.5 75-125 1999 4.55 3 Bromoform 1729 1 2 86.4 6-125 181 4.8 3 Bromomethane 146 1 2 73 3-185 787 59.9 3 Carbon disulfide 213 1 2 11 6-165 25.398 3 Carbon tetrachloride 289 1 2 14 65-14 257 1.54 3 Chlorobenzene 1936 1 2 96.8 8-12 1989 2.7 3 Chloroethane 2892 1 2 145 5-14 3158 8.79 3 Chloroform 1862 1 2 93.1 8-13 1881 1.2 3 Chloromethane 1275 1 2 63.8 5-13 144 12.2 3 cis-1,2-dichloroethene 1769 1 2 88.4 75-134 1836 3.72 3 cis-1,3-dichloropropene 1916 1 2 95.8 7-13 1983 3.44 3 Dibromochloromethane 1762 1 2 88.1 6-115 1793 1.74 3 Dibromomethane 1897 1 2 94.8 85-125 27 8.72 3 Dichlorodifluoromethane 234 1 2 12 2-12 265 1.51 3 Ethylbenzene 6328 1 2 2217 26 85-125 424 39.5 3 Hexachloroethane 1523 1 2 76.2 5-124 1383 9.64 3 Isopropylbenzene 2275 1 2 9 19 8-127 2155 5.42 3 m,p-xylene 1918 2 4 8137 276 75-13 1212 45.1 3 SR SRE R S SR SR QC Page: 9 of 1

Client: Merit Energy Work Order: 166478 Project: ECT (Hartland - 495 Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide 98 1 2 49 6-16 713 31.5 3 Methyl tert-butyl ether 1779 1 2 89 8-13 1823 2.44 3 Methylene chloride 1788 5 2 89.4 75-14 196 6.39 3 Naphthalene 2618 5 2 372 112 55-16 23 12.9 3 n-propylbenzene 2511 1 2 243 113 78-12 2251 1.9 3 o-xylene 892 1 2 3675 261 8-125 5588 45.7 3 Styrene 2316 1 2 116 85-125 22 5.14 3 Tetrachloroethene 214 1 2 15 77-138 263 1.97 3 Toluene 1991 1 2 9459 522 85-125 1167 52.1 3 trans-1,2-dichloroethene 1963 1 2 98.2 8-14 235 3.6 3 trans-1,3-dichloropropene 1519 1 2 76 81-123 158 3.94 3 trans-1,4-dichloro-2-butene 12 2 2 51 46-118 184 6.8 3 Trichloroethene 2147 1 2 17 84-13 2218 3.25 3 Trichlorofluoromethane 2213 1 2 111 6-14 2239 1.17 3 Vinyl chloride 1987 1 2 99.4 5-136 2122 6.57 3 Xylenes, Total 288 3 6 1181 271 8-126 1771 45.3 3 Surr: 1,2-Dichloroethane-d4 1793 2 89.6 75-12 1818 1.38 3 Surr: 4-Bromofluorobenzene 211 2 11 8-11 211 3 Surr: Dibromofluoromethane 1965 2 98.2 85-115 194 1.28 3 Surr: Toluene-d8 1896 2 94.8 85-11 1912.84 3 SR SR SREO S SR The following samples were analyzed in this batch: 166478-1A QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 495 Jeni Lane) WorkOrder: 166478 Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: 166478 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 3.6/3.6 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:34:43 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (869 N. Pleasant Valley) Work Order: 166886 Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: 166886 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166886-1 869 N. Pleasant Valley Water 6/13/216 16:54 6/15/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: 166886 Sample ID: 869 N. Pleasant Valley Lab ID: 166886-1 Collection Date: 6/13/216 4:54 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 54 µg/l 1 6/17/216 2:27 AM Sulfolane 11 µg/l 1 6/17/216 2:27 AM Surr: 2,4,6-Tribromophenol 46.4 38-115 %REC 1 6/17/216 2:27 AM Surr: 2-Fluorobiphenyl 45.7 32-1 %REC 1 6/17/216 2:27 AM Surr: 2-Fluorophenol 3.1 22-59 %REC 1 6/17/216 2:27 AM Surr: 4-Terphenyl-d14 82.8 23-112 %REC 1 6/17/216 2:27 AM Surr: Nitrobenzene-d5 51. 31-93 %REC 1 6/17/216 2:27 AM Surr: Phenol-d6 18. 13-36 %REC 1 6/17/216 2:27 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 5:29 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 5:29 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 5:29 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 5:29 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 5:29 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 5:29 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 5:29 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 5:29 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 2-Butanone 5. µg/l 1 6/21/216 5:29 PM 2-Hexanone 5. µg/l 1 6/21/216 5:29 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 5:29 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 5:29 PM Acetone 1 µg/l 1 6/21/216 5:29 PM Acrylonitrile 1. µg/l 1 6/21/216 5:29 PM Benzene 1. µg/l 1 6/21/216 5:29 PM Bromochloromethane 1. µg/l 1 6/21/216 5:29 PM Bromodichloromethane 1. µg/l 1 6/21/216 5:29 PM Bromoform 1. µg/l 1 6/21/216 5:29 PM Bromomethane 1. µg/l 1 6/21/216 5:29 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: 166886 Sample ID: 869 N. Pleasant Valley Lab ID: 166886-1 Collection Date: 6/13/216 4:54 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 18 91.6 14 94.6 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: 166886 Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW2-16621 The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Date: 23-Jun-16 Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888548 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 34.42 5 68.8 38-115 Surr: 2-Fluorobiphenyl 34.19 5 68.4 32-1 Surr: 2-Fluorophenol 22.38 5 44.8 22-59 Surr: 4-Terphenyl-d14 46.53 5 93.1 23-112 Surr: Nitrobenzene-d5 39.51 5 79 31-93 Surr: Phenol-d6 13.42 5 26.8 13-36 LCS Sample ID: SLCSW1-87384-87384 Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888549 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 1.77 5 1 1.8 1-5 Sulfolane 53.27 1 1 53.3 3-1 Surr: 2,4,6-Tribromophenol 35.21 5 7.4 38-115 Surr: 2-Fluorobiphenyl 35.78 5 71.6 32-1 Surr: 2-Fluorophenol 21.28 5 42.6 22-59 Surr: 4-Terphenyl-d14 49.6 5 98.1 23-112 Surr: Nitrobenzene-d5 4.25 5 8.5 31-93 Surr: Phenol-d6 12.62 5 25.2 13-36 MS Sample ID: 16687-1A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo:388855 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 18.58 5 1 18.6 1-5 Sulfolane 59.25 1 1 59.2 3-1 Surr: 2,4,6-Tribromophenol 33.1 5 66 38-115 Surr: 2-Fluorobiphenyl 34.57 5 69.1 32-1 Surr: 2-Fluorophenol 2.6 5 4.1 22-59 Surr: 4-Terphenyl-d14 46.56 5 93.1 23-112 Surr: Nitrobenzene-d5 39.7 5 79.4 31-93 Surr: Phenol-d6 11.64 5 23.3 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: 87384 Instrument ID SVMS8 Method: SW846 827D DUP Sample ID: 166871-1A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo:3888552 Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 28.89 52.63 54.9 38-115 27.6 4.58 4 Surr: 2-Fluorobiphenyl 29.71 52.63 56.4 32-1 29.6 2.2 4 Surr: 2-Fluorophenol 19.71 52.63 37.4 22-59 18.78 4.81 4 Surr: 4-Terphenyl-d14 45.1 52.63 85.5 23-112 42.59 5.53 4 Surr: Nitrobenzene-d5 32.43 52.63 61.6 31-93 32.8 1.13 4 Surr: Phenol-d6 11.48 52.63 21.8 13-36 11.2 2.51 4 The following samples were analyzed in this batch: 166886-1A QC Page: 2 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW1-16621-R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo:388617 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 21.46 2 17 75-12 Surr: 4-Bromofluorobenzene 17.99 2 9 8-11 Surr: Dibromofluoromethane 2.43 2 12 85-115 Surr: Toluene-d8 18.84 2 94.2 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW2-16621-R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo:3886169 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.57 1. 2 97.8 8-13 1,1,1-Trichloroethane 22.55 1. 2 113 75-13 1,1,2,2-Tetrachloroethane 18.67 1. 2 93.4 75-13 1,1,2-Trichloroethane 19.87 1. 2 99.4 75-125 1,1-Dichloroethane 21.59 1. 2 18 75-133 1,1-Dichloroethene 24.6 1. 2 123 7-145 1,2,3-Trichloropropane 18.99 1. 2 95 75-125 1,2,4-Trichlorobenzene 2.1 1. 2 1 7-135 1,2,4-Trimethylbenzene 2.83 1. 2 14 75-13 1,2-Dibromo-3-chloropropane 14.85 1. 2 74.2 6-13 1,2-Dibromoethane 21.69 1. 2 18 8-15 1,2-Dichlorobenzene 2.68 1. 2 13 7-13 1,2-Dichloroethane 2.77 1. 2 14 78-125 1,2-Dichloropropane 19.91 1. 2 99.6 75-125 1,3,5-Trimethylbenzene 21.2 1. 2 16 75-13 1,3-Dichlorobenzene 21.55 1. 2 18 75-13 1,4-Dichlorobenzene 2.77 1. 2 14 75-13 2-Butanone 13.56 5. 2 67.8 55-15 2-Hexanone 13.16 5. 2 65.8 6-135 4-Methyl-2-pentanone 17.41 1. 2 87 77-178 Acetone 15.96 1 2 79.8 6-16 Acrylonitrile 15.7 1. 2 78.5 6-14 Benzene 2.6 1. 2 13 85-125 Bromochloromethane 18.78 1. 2 93.9 75-13 Bromodichloromethane 2.47 1. 2 12 75-125 Bromoform 16.14 1. 2 8.7 6-125 Bromomethane 27.29 1. 2 136 3-185 Carbon disulfide 22.57 1. 2 113 6-165 Carbon tetrachloride 21.1 1. 2 15 65-14 Chlorobenzene 2.84 1. 2 14 8-12 Chloroethane 23.14 1. 2 116 5-14 Chloroform 19.86 1. 2 99.3 8-13 Chloromethane 14.87 1. 2 74.4 5-13 cis-1,2-dichloroethene 19.63 1. 2 98.2 75-134 cis-1,3-dichloropropene 17.96 1. 2 89.8 7-13 Dibromochloromethane 16.62 1. 2 83.1 6-115 Dibromomethane 2.68 1. 2 13 85-125 Dichlorodifluoromethane 18.35 1. 2 91.8 2-12 Ethylbenzene 21.52 1. 2 18 85-125 Hexachloroethane 14.16 1. 2 7.8 5-124 Isopropylbenzene 2.7 1. 2 14 8-127 m,p-xylene 44.74 2. 4 112 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 4.55 1. 2 23 6-16 Methyl tert-butyl ether 17.94 1. 2 89.7 8-13 Methylene chloride 23.38 5. 2 117 75-14 Naphthalene 16.24 5. 2 81.2 55-16 n-propylbenzene 22.3 1. 2 11 78-12 o-xylene 21.56 1. 2 18 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 22.69 1. 2 113 77-138 Toluene 2.43 1. 2 12 85-125 trans-1,2-dichloroethene 22.8 1. 2 114 8-14 trans-1,3-dichloropropene 16.34 1. 2 81.7 81-123 trans-1,4-dichloro-2-butene 12.84 2. 2 64.2 46-118 Trichloroethene 21.85 1. 2 19 84-13 Trichlorofluoromethane 22.88 1. 2 114 6-14 Vinyl chloride 2.66 1. 2 13 5-136 Xylenes, Total 66.3 3. 6 11 8-126 Surr: 1,2-Dichloroethane-d4 2.4 2 1 75-12 Surr: 4-Bromofluorobenzene 2.4 2 1 8-11 Surr: Dibromofluoromethane 2.8 2 14 85-115 Surr: Toluene-d8 19.65 2 98.2 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: 166757-21A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo:3886188 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.8 1. 2 1 8-13 1,1,1-Trichloroethane 24.12 1. 2 121 75-13 1,1,2,2-Tetrachloroethane 19.35 1. 2 96.8 75-13 1,1,2-Trichloroethane 2.4 1. 2 12 75-125 1,1-Dichloroethane 2.94 1. 2 15 75-133 1,1-Dichloroethene 25.13 1. 2 126 7-145 1,2,3-Trichloropropane 2.1 1. 2 1 75-125 1,2,4-Trichlorobenzene 19.27 1. 2 96.4 7-135 1,2,4-Trimethylbenzene 2.24 1. 2 11 75-13 1,2-Dibromo-3-chloropropane 15.52 1. 2 77.6 6-13 1,2-Dibromoethane 22.21 1. 2 111 8-15 1,2-Dichlorobenzene 2.36 1. 2 12 7-13 1,2-Dichloroethane 21.3 1. 2 15 78-125 1,2-Dichloropropane 2.59 1. 2 13 75-125 1,3,5-Trimethylbenzene 2.68 1. 2 13 75-13 1,3-Dichlorobenzene 2.95 1. 2 15 75-13 1,4-Dichlorobenzene 2.1 1. 2 1 75-13 2-Butanone 13.96 5. 2 69.8 55-15 2-Hexanone 14.2 5. 2 7.1 6-135 4-Methyl-2-pentanone 18.6 1. 2 93 77-178 Acetone 2.81 1 2 14 6-16 Acrylonitrile 18.32 1. 2 91.6 6-14 Benzene 65.38 1. 2 45.14 11 85-125 Bromochloromethane 18.68 1. 2 93.4 75-13 Bromodichloromethane 21.4 1. 2 15 75-125 Bromoform 16.63 1. 2 83.2 6-125 Bromomethane 14.6 1. 2 7.3 3-185 Carbon disulfide 22.31 1. 2 112 6-165 Carbon tetrachloride 22.91 1. 2 115 65-14 Chlorobenzene 2.68 1. 2 13 8-12 Chloroethane 23.54 1. 2 118 5-14 Chloroform 2.4 1. 2 1 8-13 Chloromethane 21.19 1. 2 1.5 98.4 5-13 cis-1,2-dichloroethene 19.3 1. 2 96.5 75-134 cis-1,3-dichloropropene 17.49 1. 2 87.4 7-13 Dibromochloromethane 16.89 1. 2 84.4 6-115 Dibromomethane 21.31 1. 2 17 85-125 Dichlorodifluoromethane 19.6 1. 2 95.3 2-12 Ethylbenzene 21.13 1. 2 16 85-125 Hexachloroethane 14.2 1. 2 71 5-124 Isopropylbenzene 2.54 1. 2 13 8-127 m,p-xylene 44.6 2. 4 112 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 19.62 1. 2 98.1 6-16 Methyl tert-butyl ether 18.2 1. 2 9.1 8-13 Methylene chloride 22.17 5. 2 111 75-14 Naphthalene 18.34 5. 2 1.74 83 55-16 n-propylbenzene 21.51 1. 2 18 78-12 o-xylene 21.8 1. 2 15 8-125 Styrene 14.3 1. 2 7.2 85-125 Tetrachloroethene 21.58 1. 2 18 77-138 Toluene 2.49 1. 2 12 85-125 trans-1,2-dichloroethene 22.23 1. 2 111 8-14 trans-1,3-dichloropropene 16.8 1. 2 8.4 81-123 trans-1,4-dichloro-2-butene 13.7 2. 2 65.4 46-118 Trichloroethene 21.75 1. 2 19 84-13 Trichlorofluoromethane 24.38 1. 2 122 6-14 Vinyl chloride 21.25 1. 2 16 5-136 Xylenes, Total 65.68 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 2.55 2 13 75-12 Surr: 4-Bromofluorobenzene 2.61 2 13 8-11 Surr: Dibromofluoromethane 21.2 2 16 85-115 Surr: Toluene-d8 19.69 2 98.4 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: 166757-21A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo:3886189 Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.66 1. 2 98.3 8-13 2.8 2.11 3 1,1,1-Trichloroethane 23.81 1. 2 119 75-13 24.12 1.29 3 1,1,2,2-Tetrachloroethane 19.8 1. 2 95.4 75-13 19.35 1.41 3 1,1,2-Trichloroethane 19.61 1. 2 98 75-125 2.4 3.95 3 1,1-Dichloroethane 21.5 1. 2 15 75-133 2.94.524 3 1,1-Dichloroethene 25.19 1. 2 126 7-145 25.13.238 3 1,2,3-Trichloropropane 19.29 1. 2 96.4 75-125 2.1 4.11 3 1,2,4-Trichlorobenzene 18.79 1. 2 94 7-135 19.27 2.52 3 1,2,4-Trimethylbenzene 19.71 1. 2 98.6 75-13 2.24 2.65 3 1,2-Dibromo-3-chloropropane 15.21 1. 2 76 6-13 15.52 2.2 3 1,2-Dibromoethane 21.21 1. 2 16 8-15 22.21 4.61 3 1,2-Dichlorobenzene 19.89 1. 2 99.4 7-13 2.36 2.34 3 1,2-Dichloroethane 21.9 1. 2 15 78-125 21.3.285 3 1,2-Dichloropropane 2.26 1. 2 11 75-125 2.59 1.62 3 1,3,5-Trimethylbenzene 2.21 1. 2 11 75-13 2.68 2.3 3 1,3-Dichlorobenzene 2.53 1. 2 13 75-13 2.95 2.3 3 1,4-Dichlorobenzene 19.81 1. 2 99 75-13 2.1 1 3 2-Butanone 13.91 5. 2 69.6 55-15 13.96.359 3 2-Hexanone 13.95 5. 2 69.8 6-135 14.2.51 3 4-Methyl-2-pentanone 17.36 1. 2 86.8 77-178 18.6 6.9 3 Acetone 22.34 1 2 112 6-16 2.81 7.9 3 Acrylonitrile 15.86 1. 2 79.3 6-14 18.32 14.4 3 Benzene 64.83 1. 2 45.14 98.4 85-125 65.38.845 3 Bromochloromethane 18.4 1. 2 9.2 75-13 18.68 3.49 3 Bromodichloromethane 21.13 1. 2 16 75-125 21.4.427 3 Bromoform 16.78 1. 2 83.9 6-125 16.63.898 3 Bromomethane 15.82 1. 2 79.1 3-185 14.6 11.8 3 Carbon disulfide 22.62 1. 2 113 6-165 22.31 1.38 3 Carbon tetrachloride 22.97 1. 2 115 65-14 22.91.262 3 Chlorobenzene 2.33 1. 2 12 8-12 2.68 1.71 3 Chloroethane 23.5 1. 2 115 5-14 23.54 2.1 3 Chloroform 19.83 1. 2 99.2 8-13 2.4 1.5 3 Chloromethane 19.88 1. 2 1.5 91.9 5-13 21.19 6.38 3 cis-1,2-dichloroethene 19.14 1. 2 95.7 75-134 19.3.832 3 cis-1,3-dichloropropene 17.82 1. 2 89.1 7-13 17.49 1.87 3 Dibromochloromethane 16.93 1. 2 84.6 6-115 16.89.237 3 Dibromomethane 21.7 1. 2 15 85-125 21.31 1.13 3 Dichlorodifluoromethane 18.73 1. 2 93.6 2-12 19.6 1.75 3 Ethylbenzene 2.69 1. 2 13 85-125 21.13 2.1 3 Hexachloroethane 14.63 1. 2 73.2 5-124 14.2 2.98 3 Isopropylbenzene 2.21 1. 2 11 8-127 2.54 1.62 3 m,p-xylene 43.56 2. 4 19 75-13 44.6 2.36 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 166886 Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide 11.22 1. 2 56.1 6-16 19.62 54.5 3 Methyl tert-butyl ether 17.21 1. 2 86 8-13 18.2 4.6 3 Methylene chloride 2.8 5. 2 14 75-14 22.17 6.38 3 Naphthalene 17.29 5. 2 1.74 77.8 55-16 18.34 5.89 3 n-propylbenzene 21.2 1. 2 15 78-12 21.51 2.3 3 o-xylene 2.71 1. 2 14 8-125 21.8 1.77 3 Styrene 13.72 1. 2 68.6 85-125 14.3 2.23 3 Tetrachloroethene 21 1. 2 15 77-138 21.58 2.72 3 Toluene 2.34 1. 2 12 85-125 2.49.735 3 trans-1,2-dichloroethene 21.22 1. 2 16 8-14 22.23 4.65 3 trans-1,3-dichloropropene 15.7 1. 2 78.5 81-123 16.8 2.39 3 trans-1,4-dichloro-2-butene 12.81 2. 2 64 46-118 13.7 2.1 3 Trichloroethene 21.54 1. 2 18 84-13 21.75.97 3 Trichlorofluoromethane 23.82 1. 2 119 6-14 24.38 2.32 3 Vinyl chloride 2.97 1. 2 15 5-136 21.25 1.33 3 Xylenes, Total 64.27 3. 6 17 8-126 65.68 2.17 3 Surr: 1,2-Dichloroethane-d4 2.59 2 13 75-12 2.55.194 3 Surr: 4-Bromofluorobenzene 2.65 2 13 8-11 2.61.194 3 Surr: Dibromofluoromethane 21.9 2 15 85-115 21.2.52 3 Surr: Toluene-d8 19.75 2 98.8 85-11 19.69.34 3 SR S S The following samples were analyzed in this batch: 166886-1B QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (869 N. Pleasant Valley) WorkOrder: 166886 Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: 166886 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 3:17:42 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (Hartland - 13223 Lone Tree Rd) Work Order: 16648 Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13223 Lone Tree Rd) Work Order: 16648 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 16648-1 13223 Lone Tree Rd Water 6/7/216 7:16 6/8/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13223 Lone Tree Rd) Work Order: 16648 Sample ID: 13223 Lone Tree Rd Lab ID: 16648-1 Collection Date: 6/7/216 7:16 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 58 µg/l 1 6/9/216 8:17 PM Sulfolane 12 µg/l 1 6/9/216 8:17 PM Surr: 2,4,6-Tribromophenol 62.8 38-115 %REC 1 6/9/216 8:17 PM Surr: 2-Fluorobiphenyl 56.5 32-1 %REC 1 6/9/216 8:17 PM Surr: 2-Fluorophenol 37.6 22-59 %REC 1 6/9/216 8:17 PM Surr: 4-Terphenyl-d14 69.9 23-112 %REC 1 6/9/216 8:17 PM Surr: Nitrobenzene-d5 66.5 31-93 %REC 1 6/9/216 8:17 PM Surr: Phenol-d6 19.6 13-36 %REC 1 6/9/216 8:17 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 2:26 PM 1,1-Dichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1-Dichloroethene 1. µg/l 1 6/9/216 2:26 PM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 2:26 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 2:26 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 2:26 PM 1,2-Dibromoethane 1. µg/l 1 6/9/216 2:26 PM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 1,2-Dichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,2-Dichloropropane 1. µg/l 1 6/9/216 2:26 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 2:26 PM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 2-Butanone 5. µg/l 1 6/9/216 2:26 PM 2-Hexanone 5. µg/l 1 6/9/216 2:26 PM 2-Methylnaphthalene 5. µg/l 1 6/9/216 2:26 PM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 2:26 PM Acetone 1 µg/l 1 6/9/216 2:26 PM Acrylonitrile 1. µg/l 1 6/9/216 2:26 PM Benzene 1. µg/l 1 6/9/216 2:26 PM Bromochloromethane 1. µg/l 1 6/9/216 2:26 PM Bromodichloromethane 1. µg/l 1 6/9/216 2:26 PM Bromoform 1. µg/l 1 6/9/216 2:26 PM Bromomethane 1. µg/l 1 6/9/216 2:26 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13223 Lone Tree Rd) Work Order: 16648 Sample ID: 13223 Lone Tree Rd Lab ID: 16648-1 Collection Date: 6/7/216 7:16 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 14 9.6 98.4 97.5 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 13223 Lone Tree Rd) Work Order: 16648 Date: 1-Jun-16 Case Narrative Batch R189219 Sample VLCSW1-1669 The LCS recovery for volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were non-detect. No qualification is necessary for this analyte. Batch R189219 The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Date: 1-Jun-16 Batch ID: 8717 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8717-8717 Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 387197 Analysis Date: 6/9/216 3:25 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 21.75 5 43.5 38-115 Surr: 2-Fluorobiphenyl 21.56 5 43.1 32-1 Surr: 2-Fluorophenol 16.37 5 32.7 22-59 Surr: 4-Terphenyl-d14 35.69 5 71.4 23-112 Surr: Nitrobenzene-d5 28.3 5 56.1 31-93 Surr: Phenol-d6 7.63 5 15.3 13-36 LCS Sample ID: SLCSW1-8717-8717 Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 387198 Analysis Date: 6/9/216 3:45 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5.75 5 1 5.75 5-4 Sulfolane 54.53 1 1 54.5 3-1 Surr: 2,4,6-Tribromophenol 27.91 5 55.8 38-115 Surr: 2-Fluorobiphenyl 28.51 5 57 32-1 Surr: 2-Fluorophenol 19.32 5 38.6 22-59 Surr: 4-Terphenyl-d14 37.7 5 75.4 23-112 Surr: Nitrobenzene-d5 35.21 5 7.4 31-93 Surr: Phenol-d6 1.2 5 2 13-36 MS Sample ID: 166476-1B MS Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 387199 Analysis Date: 6/9/216 6:36 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 53 16.4 13.2 5-4 Sulfolane 65.27 11 16.4 61.4 3-1 Surr: 2,4,6-Tribromophenol 36.5 53.19 67.8 38-115 Surr: 2-Fluorobiphenyl 31.76 53.19 59.7 32-1 Surr: 2-Fluorophenol 2.45 53.19 38.4 22-59 Surr: 4-Terphenyl-d14 38.93 53.19 73.2 23-112 Surr: Nitrobenzene-d5 38.12 53.19 71.7 31-93 Surr: Phenol-d6 1.87 53.19 2.4 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: 8717 Instrument ID: SVMS8 Method: SW846 827D DUP Sample ID: 166478-1B DUP Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 38721 Analysis Date: 6/9/216 7:16 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 32.53 53.2 61.4 38-115 31.66 2.72 4 Surr: 2-Fluorobiphenyl 29.9 53.2 56.4 32-1 27.39 8.78 4 Surr: 2-Fluorophenol 18.87 53.2 35.6 22-59 16.97 1.6 4 Surr: 4-Terphenyl-d14 35.97 53.2 67.8 23-112 37.85 5.9 4 Surr: Nitrobenzene-d5 35.12 53.2 66.2 31-93 32.88 6.59 4 Surr: Phenol-d6 9.3 53.2 17.5 13-36 8.71 6.55 4 The following samples were analyzed in this batch: 16648-1B QC Page: 2 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B MBLK Sample ID: VBLKW1-1669-R189219 Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 3868762 Prep Date: Analysis Date: 6/9/216 1:38 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 2.49 2 12 75-12 Surr: 4-Bromofluorobenzene 18.47 2 92.4 8-11 Surr: Dibromofluoromethane 2 2 1 85-115 Surr: Toluene-d8 19.62 2 98.1 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B LCS Sample ID: VLCSW1-1669-R189219 Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 3868761 Prep Date: Analysis Date: 6/9/216 1:58 AM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.21 1. 2 11 8-13 1,1,1-Trichloroethane 21.58 1. 2 18 75-13 1,1,2,2-Tetrachloroethane 19.6 1. 2 98 75-13 1,1,2-Trichloroethane 2.68 1. 2 13 75-125 1,1-Dichloroethane 2.39 1. 2 12 75-133 1,1-Dichloroethene 21.68 1. 2 18 7-145 1,2,3-Trichloropropane 19.27 1. 2 96.4 75-125 1,2,4-Trichlorobenzene 21.3 1. 2 15 7-135 1,2,4-Trimethylbenzene 21.28 1. 2 16 75-13 1,2-Dibromo-3-chloropropane 15.2 1. 2 75.1 6-13 1,2-Dibromoethane 22.66 1. 2 113 8-15 1,2-Dichlorobenzene 2.98 1. 2 15 7-13 1,2-Dichloroethane 19.47 1. 2 97.4 78-125 1,2-Dichloropropane 2.58 1. 2 13 75-125 1,3,5-Trimethylbenzene 21.96 1. 2 11 75-13 1,3-Dichlorobenzene 21.37 1. 2 17 75-13 1,4-Dichlorobenzene 21.12 1. 2 16 75-13 2-Butanone 16.22 5. 2 81.1 55-15 2-Hexanone 16.77 5. 2 83.8 6-135 4-Methyl-2-pentanone 22.16 1. 2 111 77-178 Acetone 14.1 1 2 7.5 6-16 Acrylonitrile 15.91 1. 2 79.6 6-14 Benzene 2.51 1. 2 13 85-125 Bromochloromethane 2.81 1. 2 14 75-13 Bromodichloromethane 2.49 1. 2 12 75-125 Bromoform 16.4 1. 2 8.2 6-125 Bromomethane 23.77 1. 2 119 3-185 Carbon disulfide 2.48 1. 2 12 6-165 Carbon tetrachloride 19.28 1. 2 96.4 65-14 Chlorobenzene 21.38 1. 2 17 8-12 Chloroethane 17.38 1. 2 86.9 5-14 Chloroform 19.58 1. 2 97.9 8-13 Chloromethane 19.42 1. 2 97.1 5-13 cis-1,2-dichloroethene 2.11 1. 2 11 75-134 cis-1,3-dichloropropene 18.96 1. 2 94.8 7-13 Dibromochloromethane 16.82 1. 2 84.1 6-115 Dibromomethane 2.77 1. 2 14 85-125 Dichlorodifluoromethane 18.28 1. 2 91.4 2-12 Ethylbenzene 22.59 1. 2 113 85-125 Hexachloroethane 15.37 1. 2 76.8 5-124 Isopropylbenzene 21.69 1. 2 18 8-127 m,p-xylene 46.1 2. 4 115 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Methyl iodide 34.3 1. 2 17 6-16 Methyl tert-butyl ether 16.14 1. 2 8.7 8-13 Methylene chloride 22.58 5. 2 113 75-14 Naphthalene 18.11 5. 2 9.6 55-16 n-propylbenzene 23.4 1. 2 115 78-12 o-xylene 22.43 1. 2 112 8-125 Styrene 21.5 1. 2 18 85-125 Tetrachloroethene 21.91 1. 2 11 77-138 Toluene 21.48 1. 2 17 85-125 trans-1,2-dichloroethene 19.45 1. 2 97.2 8-14 trans-1,3-dichloropropene 17.2 1. 2 86 81-123 trans-1,4-dichloro-2-butene 14.3 2. 2 71.5 46-118 Trichloroethene 2.6 1. 2 13 84-13 Trichlorofluoromethane 18.89 1. 2 94.4 6-14 Vinyl chloride 21.52 1. 2 18 5-136 Xylenes, Total 68.53 3. 6 114 8-126 Surr: 1,2-Dichloroethane-d4 19.12 2 95.6 75-12 Surr: 4-Bromofluorobenzene 2.33 2 12 8-11 Surr: Dibromofluoromethane 19.89 2 99.4 85-115 Surr: Toluene-d8 2.23 2 11 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B MS Sample ID: 166558-2A MS Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 3868779 Prep Date: Analysis Date: 6/9/216 8:55 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.91 1. 2 99.6 8-13 1,1,1-Trichloroethane 22.74 1. 2 114 75-13 1,1,2,2-Tetrachloroethane 2.1 1. 2 1 75-13 1,1,2-Trichloroethane 2.39 1. 2 12 75-125 1,1-Dichloroethane 2.78 1. 2 14 75-133 1,1-Dichloroethene 22.55 1. 2 113 7-145 1,2,3-Trichloropropane 19.76 1. 2 98.8 75-125 1,2,4-Trichlorobenzene 17.66 1. 2 88.3 7-135 1,2,4-Trimethylbenzene 2.34 1. 2 12 75-13 1,2-Dibromo-3-chloropropane 15.54 1. 2 77.7 6-13 1,2-Dibromoethane 21.99 1. 2 11 8-15 1,2-Dichlorobenzene 19.41 1. 2 97 7-13 1,2-Dichloroethane 19.69 1. 2 98.4 78-125 1,2-Dichloropropane 2.47 1. 2 12 75-125 1,3,5-Trimethylbenzene 2.95 1. 2 15 75-13 1,3-Dichlorobenzene 19.66 1. 2 98.3 75-13 1,4-Dichlorobenzene 19.42 1. 2 97.1 75-13 2-Butanone 17.13 5. 2 85.6 55-15 2-Hexanone 17.53 5. 2 87.6 6-135 4-Methyl-2-pentanone 23.94 1. 2 12 77-178 Acetone 15.73 1 2 78.6 6-16 Acrylonitrile 16.8 1. 2 8.4 6-14 Benzene 2.5 1. 2 12 85-125 Bromochloromethane 2.6 1. 2 1 75-13 Bromodichloromethane 2.33 1. 2 12 75-125 Bromoform 16.8 1. 2 8.4 6-125 Bromomethane 13.6 1. 2 65.3 3-185 Carbon disulfide 19.45 1. 2 97.2 6-165 Carbon tetrachloride 2.6 1. 2 13 65-14 Chlorobenzene 2.58 1. 2 13 8-12 Chloroethane 17.32 1. 2 86.6 5-14 Chloroform 19.49 1. 2 97.4 8-13 Chloromethane 15.54 1. 2 77.7 5-13 cis-1,2-dichloroethene 19.51 1. 2 97.6 75-134 cis-1,3-dichloropropene 17.65 1. 2 88.2 7-13 Dibromochloromethane 16.56 1. 2 82.8 6-115 Dibromomethane 21.4 1. 2 17 85-125 Dichlorodifluoromethane 2.4 1. 2 1 2-12 Ethylbenzene 21.47 1. 2 17 85-125 Hexachloroethane 14.27 1. 2 71.4 5-124 Isopropylbenzene 2.87 1. 2 14 8-127 m,p-xylene 44.4 2. 4 111 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Methyl iodide 23.54 1. 2 118 6-16 Methyl tert-butyl ether 14.86 1. 2 74.3 8-13 Methylene chloride 21.31 5. 2 17 75-14 Naphthalene 16.44 5. 2 82.2 55-16 n-propylbenzene 22.6 1. 2 11 78-12 o-xylene 21.17 1. 2 16 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 21.47 1. 2 17 77-138 Toluene 2.64 1. 2 13 85-125 trans-1,2-dichloroethene 18.86 1. 2 94.3 8-14 trans-1,3-dichloropropene 15.89 1. 2 79.4 81-123 trans-1,4-dichloro-2-butene 13.66 2. 2 68.3 46-118 Trichloroethene 2.83 1. 2 14 84-13 Trichlorofluoromethane 21.1 1. 2 15 6-14 Vinyl chloride 2.56 1. 2 13 5-136 Xylenes, Total 65.57 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 19.77 2 98.8 75-12 Surr: 4-Bromofluorobenzene 2.44 2 12 8-11 Surr: Dibromofluoromethane 2.89 2 14 85-115 Surr: Toluene-d8 2.2 2 11 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B MSD Sample ID: 166558-2A MSD Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 386878 Prep Date: Analysis Date: 6/9/216 9:2 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.11 1. 2 11 8-13 19.91 1 3 1,1,1-Trichloroethane 22.9 1. 2 114 75-13 22.74.71 3 1,1,2,2-Tetrachloroethane 2.56 1. 2 13 75-13 2.1 2.26 3 1,1,2-Trichloroethane 2.55 1. 2 13 75-125 2.39.782 3 1,1-Dichloroethane 2.95 1. 2 15 75-133 2.78.815 3 1,1-Dichloroethene 22.67 1. 2 113 7-145 22.55.531 3 1,2,3-Trichloropropane 2.16 1. 2 11 75-125 19.76 2 3 1,2,4-Trichlorobenzene 18.68 1. 2 93.4 7-135 17.66 5.61 3 1,2,4-Trimethylbenzene 2.5 1. 2 12 75-13 2.34.784 3 1,2-Dibromo-3-chloropropane 15.86 1. 2 79.3 6-13 15.54 2.4 3 1,2-Dibromoethane 22.75 1. 2 114 8-15 21.99 3.4 3 1,2-Dichlorobenzene 19.86 1. 2 99.3 7-13 19.41 2.29 3 1,2-Dichloroethane 19.98 1. 2 99.9 78-125 19.69 1.46 3 1,2-Dichloropropane 21.2 1. 2 15 75-125 2.47 2.65 3 1,3,5-Trimethylbenzene 21.29 1. 2 16 75-13 2.95 1.61 3 1,3-Dichlorobenzene 2.35 1. 2 12 75-13 19.66 3.45 3 1,4-Dichlorobenzene 2.2 1. 2 1 75-13 19.42 3.4 3 2-Butanone 17.28 5. 2 86.4 55-15 17.13.872 3 2-Hexanone 18.94 5. 2 94.7 6-135 17.53 7.73 3 4-Methyl-2-pentanone 24.55 1. 2 123 77-178 23.94 2.52 3 Acetone 18.66 1 2 93.3 6-16 15.73 17 3 Acrylonitrile 17.19 1. 2 86 6-14 16.8 6.67 3 Benzene 2.99 1. 2 15 85-125 2.5 2.36 3 Bromochloromethane 2.41 1. 2 12 75-13 2.6 1.73 3 Bromodichloromethane 2.96 1. 2 15 75-125 2.33 3.5 3 Bromoform 16.62 1. 2 83.1 6-125 16.8 3.3 3 Bromomethane 13.9 1. 2 69.5 3-185 13.6 6.23 3 Carbon disulfide 19.92 1. 2 99.6 6-165 19.45 2.39 3 Carbon tetrachloride 21.29 1. 2 16 65-14 2.6 3.29 3 Chlorobenzene 2.77 1. 2 14 8-12 2.58.919 3 Chloroethane 17.91 1. 2 89.6 5-14 17.32 3.35 3 Chloroform 19.79 1. 2 99 8-13 19.49 1.53 3 Chloromethane 16.15 1. 2 8.8 5-13 15.54 3.85 3 cis-1,2-dichloroethene 19.48 1. 2 97.4 75-134 19.51.154 3 cis-1,3-dichloropropene 18.32 1. 2 91.6 7-13 17.65 3.73 3 Dibromochloromethane 16.55 1. 2 82.8 6-115 16.56.64 3 Dibromomethane 21.6 1. 2 15 85-125 21.4 1.6 3 Dichlorodifluoromethane 2.32 1. 2 12 2-12 2.4 1.39 3 Ethylbenzene 22.3 1. 2 11 85-125 21.47 2.57 3 Hexachloroethane 14.86 1. 2 74.3 5-124 14.27 4.5 3 Isopropylbenzene 21.45 1. 2 17 8-127 2.87 2.74 3 m,p-xylene 45.43 2. 4 114 75-13 44.4 2.29 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 16648 Project: ECT (Hartland - 13223 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Methyl iodide 26.31 1. 2 132 6-16 23.54 11.1 3 Methyl tert-butyl ether 15.3 1. 2 76.5 8-13 14.86 2.92 3 Methylene chloride 21.12 5. 2 16 75-14 21.31.896 3 Naphthalene 17.63 5. 2 88.2 55-16 16.44 6.99 3 n-propylbenzene 22.37 1. 2 112 78-12 22.6 1.4 3 o-xylene 21.75 1. 2 19 8-125 21.17 2.7 3 Styrene 2.92 1. 2 15 85-125 2.41 2.47 3 Tetrachloroethene 22.11 1. 2 111 77-138 21.47 2.94 3 Toluene 21.1 1. 2 15 85-125 2.64 1.78 3 trans-1,2-dichloroethene 19.3 1. 2 96.5 8-14 18.86 2.31 3 trans-1,3-dichloropropene 16.14 1. 2 8.7 81-123 15.89 1.56 3 trans-1,4-dichloro-2-butene 14.4 2. 2 7.2 46-118 13.66 2.74 3 Trichloroethene 21.45 1. 2 17 84-13 2.83 2.93 3 Trichlorofluoromethane 2.7 1. 2 14 6-14 21.1 1.49 3 Vinyl chloride 21.1 1. 2 16 5-136 2.56 2.59 3 Xylenes, Total 67.18 3. 6 112 8-126 65.57 2.43 3 Surr: 1,2-Dichloroethane-d4 2.3 2 1 75-12 19.77 1.31 3 Surr: 4-Bromofluorobenzene 2.25 2 11 8-11 2.44.934 3 Surr: Dibromofluoromethane 2.68 2 13 85-115 2.89 1.1 3 Surr: Toluene-d8 2.9 2 1 85-11 2.2.546 3 S S The following samples were analyzed in this batch: 16648-1A QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 13223 Lone Tree Rd) WorkOrder: 16648 Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: 16648 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature 8-Jun-16 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.4/2.4 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:41:25 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: ECT (Hartland - 13247 Lone Tree Rd) Work Order: 166484 Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13247 Lone Tree Rd) Work Order: 166484 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received 166484-1 13247 Lone Tree Rd Water 6/7/216 7:54 6/8/216 9:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13247 Lone Tree Rd) Work Order: 166484 Sample ID: 13247 Lone Tree Rd Lab ID: 166484-1 Collection Date: 6/7/216 7:54 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 8:58 PM Sulfolane 1 µg/l 1 6/9/216 8:58 PM Surr: 2,4,6-Tribromophenol 56.7 38-115 %REC 1 6/9/216 8:58 PM Surr: 2-Fluorobiphenyl 5.6 32-1 %REC 1 6/9/216 8:58 PM Surr: 2-Fluorophenol 33.5 22-59 %REC 1 6/9/216 8:58 PM Surr: 4-Terphenyl-d14 76.3 23-112 %REC 1 6/9/216 8:58 PM Surr: Nitrobenzene-d5 58.6 31-93 %REC 1 6/9/216 8:58 PM Surr: Phenol-d6 17.1 13-36 %REC 1 6/9/216 8:58 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 3:15 PM 1,1-Dichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1-Dichloroethene 1. µg/l 1 6/9/216 3:15 PM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 3:15 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 3:15 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 3:15 PM 1,2-Dibromoethane 1. µg/l 1 6/9/216 3:15 PM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 1,2-Dichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,2-Dichloropropane 1. µg/l 1 6/9/216 3:15 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 3:15 PM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 2-Butanone 5. µg/l 1 6/9/216 3:15 PM 2-Hexanone 5. µg/l 1 6/9/216 3:15 PM 2-Methylnaphthalene 5. µg/l 1 6/9/216 3:15 PM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 3:15 PM Acetone 1 µg/l 1 6/9/216 3:15 PM Acrylonitrile 1. µg/l 1 6/9/216 3:15 PM Benzene 1. µg/l 1 6/9/216 3:15 PM Bromochloromethane 1. µg/l 1 6/9/216 3:15 PM Bromodichloromethane 1. µg/l 1 6/9/216 3:15 PM Bromoform 1. µg/l 1 6/9/216 3:15 PM Bromomethane 1. µg/l 1 6/9/216 3:15 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 13247 Lone Tree Rd) Work Order: 166484 Sample ID: 13247 Lone Tree Rd Lab ID: 166484-1 Collection Date: 6/7/216 7:54 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 13 9.5 1 97.6 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 13247 Lone Tree Rd) Work Order: 166484 Date: 1-Jun-16 Case Narrative Batch R189219 Sample VLCSW1-1669 The LCS recovery for volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were non-detect. No qualification is necessary for this analyte. Batch R189219 The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Date: 1-Jun-16 Batch ID: 8717 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8717-8717 Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 387197 Analysis Date: 6/9/216 3:25 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 21.75 5 43.5 38-115 Surr: 2-Fluorobiphenyl 21.56 5 43.1 32-1 Surr: 2-Fluorophenol 16.37 5 32.7 22-59 Surr: 4-Terphenyl-d14 35.69 5 71.4 23-112 Surr: Nitrobenzene-d5 28.3 5 56.1 31-93 Surr: Phenol-d6 7.63 5 15.3 13-36 LCS Sample ID: SLCSW1-8717-8717 Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 387198 Analysis Date: 6/9/216 3:45 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5.75 5 1 5.75 5-4 Sulfolane 54.53 1 1 54.5 3-1 Surr: 2,4,6-Tribromophenol 27.91 5 55.8 38-115 Surr: 2-Fluorobiphenyl 28.51 5 57 32-1 Surr: 2-Fluorophenol 19.32 5 38.6 22-59 Surr: 4-Terphenyl-d14 37.7 5 75.4 23-112 Surr: Nitrobenzene-d5 35.21 5 7.4 31-93 Surr: Phenol-d6 1.2 5 2 13-36 MS Sample ID: 166476-1B MS Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 387199 Analysis Date: 6/9/216 6:36 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 53 16.4 13.2 5-4 Sulfolane 65.27 11 16.4 61.4 3-1 Surr: 2,4,6-Tribromophenol 36.5 53.19 67.8 38-115 Surr: 2-Fluorobiphenyl 31.76 53.19 59.7 32-1 Surr: 2-Fluorophenol 2.45 53.19 38.4 22-59 Surr: 4-Terphenyl-d14 38.93 53.19 73.2 23-112 Surr: Nitrobenzene-d5 38.12 53.19 71.7 31-93 Surr: Phenol-d6 1.87 53.19 2.4 13-36 QC Page: 1 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: 8717 Instrument ID: SVMS8 Method: SW846 827D DUP Sample ID: 166478-1B DUP Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: 38721 Analysis Date: 6/9/216 7:16 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol 32.53 53.2 61.4 38-115 31.66 2.72 4 Surr: 2-Fluorobiphenyl 29.9 53.2 56.4 32-1 27.39 8.78 4 Surr: 2-Fluorophenol 18.87 53.2 35.6 22-59 16.97 1.6 4 Surr: 4-Terphenyl-d14 35.97 53.2 67.8 23-112 37.85 5.9 4 Surr: Nitrobenzene-d5 35.12 53.2 66.2 31-93 32.88 6.59 4 Surr: Phenol-d6 9.3 53.2 17.5 13-36 8.71 6.55 4 The following samples were analyzed in this batch: 166484-1B QC Page: 2 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B MBLK Sample ID: VBLKW1-1669-R189219 Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 3868762 Prep Date: Analysis Date: 6/9/216 1:38 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 2.49 2 12 75-12 Surr: 4-Bromofluorobenzene 18.47 2 92.4 8-11 Surr: Dibromofluoromethane 2 2 1 85-115 Surr: Toluene-d8 19.62 2 98.1 85-11 QC Page: 4 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B LCS Sample ID: VLCSW1-1669-R189219 Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 3868761 Prep Date: Analysis Date: 6/9/216 1:58 AM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.21 1. 2 11 8-13 1,1,1-Trichloroethane 21.58 1. 2 18 75-13 1,1,2,2-Tetrachloroethane 19.6 1. 2 98 75-13 1,1,2-Trichloroethane 2.68 1. 2 13 75-125 1,1-Dichloroethane 2.39 1. 2 12 75-133 1,1-Dichloroethene 21.68 1. 2 18 7-145 1,2,3-Trichloropropane 19.27 1. 2 96.4 75-125 1,2,4-Trichlorobenzene 21.3 1. 2 15 7-135 1,2,4-Trimethylbenzene 21.28 1. 2 16 75-13 1,2-Dibromo-3-chloropropane 15.2 1. 2 75.1 6-13 1,2-Dibromoethane 22.66 1. 2 113 8-15 1,2-Dichlorobenzene 2.98 1. 2 15 7-13 1,2-Dichloroethane 19.47 1. 2 97.4 78-125 1,2-Dichloropropane 2.58 1. 2 13 75-125 1,3,5-Trimethylbenzene 21.96 1. 2 11 75-13 1,3-Dichlorobenzene 21.37 1. 2 17 75-13 1,4-Dichlorobenzene 21.12 1. 2 16 75-13 2-Butanone 16.22 5. 2 81.1 55-15 2-Hexanone 16.77 5. 2 83.8 6-135 4-Methyl-2-pentanone 22.16 1. 2 111 77-178 Acetone 14.1 1 2 7.5 6-16 Acrylonitrile 15.91 1. 2 79.6 6-14 Benzene 2.51 1. 2 13 85-125 Bromochloromethane 2.81 1. 2 14 75-13 Bromodichloromethane 2.49 1. 2 12 75-125 Bromoform 16.4 1. 2 8.2 6-125 Bromomethane 23.77 1. 2 119 3-185 Carbon disulfide 2.48 1. 2 12 6-165 Carbon tetrachloride 19.28 1. 2 96.4 65-14 Chlorobenzene 21.38 1. 2 17 8-12 Chloroethane 17.38 1. 2 86.9 5-14 Chloroform 19.58 1. 2 97.9 8-13 Chloromethane 19.42 1. 2 97.1 5-13 cis-1,2-dichloroethene 2.11 1. 2 11 75-134 cis-1,3-dichloropropene 18.96 1. 2 94.8 7-13 Dibromochloromethane 16.82 1. 2 84.1 6-115 Dibromomethane 2.77 1. 2 14 85-125 Dichlorodifluoromethane 18.28 1. 2 91.4 2-12 Ethylbenzene 22.59 1. 2 113 85-125 Hexachloroethane 15.37 1. 2 76.8 5-124 Isopropylbenzene 21.69 1. 2 18 8-127 m,p-xylene 46.1 2. 4 115 75-13 QC Page: 5 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Methyl iodide 34.3 1. 2 17 6-16 Methyl tert-butyl ether 16.14 1. 2 8.7 8-13 Methylene chloride 22.58 5. 2 113 75-14 Naphthalene 18.11 5. 2 9.6 55-16 n-propylbenzene 23.4 1. 2 115 78-12 o-xylene 22.43 1. 2 112 8-125 Styrene 21.5 1. 2 18 85-125 Tetrachloroethene 21.91 1. 2 11 77-138 Toluene 21.48 1. 2 17 85-125 trans-1,2-dichloroethene 19.45 1. 2 97.2 8-14 trans-1,3-dichloropropene 17.2 1. 2 86 81-123 trans-1,4-dichloro-2-butene 14.3 2. 2 71.5 46-118 Trichloroethene 2.6 1. 2 13 84-13 Trichlorofluoromethane 18.89 1. 2 94.4 6-14 Vinyl chloride 21.52 1. 2 18 5-136 Xylenes, Total 68.53 3. 6 114 8-126 Surr: 1,2-Dichloroethane-d4 19.12 2 95.6 75-12 Surr: 4-Bromofluorobenzene 2.33 2 12 8-11 Surr: Dibromofluoromethane 19.89 2 99.4 85-115 Surr: Toluene-d8 2.23 2 11 85-11 S QC Page: 6 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B MS Sample ID: 166558-2A MS Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 3868779 Prep Date: Analysis Date: 6/9/216 8:55 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 19.91 1. 2 99.6 8-13 1,1,1-Trichloroethane 22.74 1. 2 114 75-13 1,1,2,2-Tetrachloroethane 2.1 1. 2 1 75-13 1,1,2-Trichloroethane 2.39 1. 2 12 75-125 1,1-Dichloroethane 2.78 1. 2 14 75-133 1,1-Dichloroethene 22.55 1. 2 113 7-145 1,2,3-Trichloropropane 19.76 1. 2 98.8 75-125 1,2,4-Trichlorobenzene 17.66 1. 2 88.3 7-135 1,2,4-Trimethylbenzene 2.34 1. 2 12 75-13 1,2-Dibromo-3-chloropropane 15.54 1. 2 77.7 6-13 1,2-Dibromoethane 21.99 1. 2 11 8-15 1,2-Dichlorobenzene 19.41 1. 2 97 7-13 1,2-Dichloroethane 19.69 1. 2 98.4 78-125 1,2-Dichloropropane 2.47 1. 2 12 75-125 1,3,5-Trimethylbenzene 2.95 1. 2 15 75-13 1,3-Dichlorobenzene 19.66 1. 2 98.3 75-13 1,4-Dichlorobenzene 19.42 1. 2 97.1 75-13 2-Butanone 17.13 5. 2 85.6 55-15 2-Hexanone 17.53 5. 2 87.6 6-135 4-Methyl-2-pentanone 23.94 1. 2 12 77-178 Acetone 15.73 1 2 78.6 6-16 Acrylonitrile 16.8 1. 2 8.4 6-14 Benzene 2.5 1. 2 12 85-125 Bromochloromethane 2.6 1. 2 1 75-13 Bromodichloromethane 2.33 1. 2 12 75-125 Bromoform 16.8 1. 2 8.4 6-125 Bromomethane 13.6 1. 2 65.3 3-185 Carbon disulfide 19.45 1. 2 97.2 6-165 Carbon tetrachloride 2.6 1. 2 13 65-14 Chlorobenzene 2.58 1. 2 13 8-12 Chloroethane 17.32 1. 2 86.6 5-14 Chloroform 19.49 1. 2 97.4 8-13 Chloromethane 15.54 1. 2 77.7 5-13 cis-1,2-dichloroethene 19.51 1. 2 97.6 75-134 cis-1,3-dichloropropene 17.65 1. 2 88.2 7-13 Dibromochloromethane 16.56 1. 2 82.8 6-115 Dibromomethane 21.4 1. 2 17 85-125 Dichlorodifluoromethane 2.4 1. 2 1 2-12 Ethylbenzene 21.47 1. 2 17 85-125 Hexachloroethane 14.27 1. 2 71.4 5-124 Isopropylbenzene 2.87 1. 2 14 8-127 m,p-xylene 44.4 2. 4 111 75-13 QC Page: 7 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Methyl iodide 23.54 1. 2 118 6-16 Methyl tert-butyl ether 14.86 1. 2 74.3 8-13 Methylene chloride 21.31 5. 2 17 75-14 Naphthalene 16.44 5. 2 82.2 55-16 n-propylbenzene 22.6 1. 2 11 78-12 o-xylene 21.17 1. 2 16 8-125 Styrene 2.41 1. 2 12 85-125 Tetrachloroethene 21.47 1. 2 17 77-138 Toluene 2.64 1. 2 13 85-125 trans-1,2-dichloroethene 18.86 1. 2 94.3 8-14 trans-1,3-dichloropropene 15.89 1. 2 79.4 81-123 trans-1,4-dichloro-2-butene 13.66 2. 2 68.3 46-118 Trichloroethene 2.83 1. 2 14 84-13 Trichlorofluoromethane 21.1 1. 2 15 6-14 Vinyl chloride 2.56 1. 2 13 5-136 Xylenes, Total 65.57 3. 6 19 8-126 Surr: 1,2-Dichloroethane-d4 19.77 2 98.8 75-12 Surr: 4-Bromofluorobenzene 2.44 2 12 8-11 Surr: Dibromofluoromethane 2.89 2 14 85-115 Surr: Toluene-d8 2.2 2 11 85-11 S S QC Page: 8 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B MSD Sample ID: 166558-2A MSD Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: 386878 Prep Date: Analysis Date: 6/9/216 9:2 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 2.11 1. 2 11 8-13 19.91 1 3 1,1,1-Trichloroethane 22.9 1. 2 114 75-13 22.74.71 3 1,1,2,2-Tetrachloroethane 2.56 1. 2 13 75-13 2.1 2.26 3 1,1,2-Trichloroethane 2.55 1. 2 13 75-125 2.39.782 3 1,1-Dichloroethane 2.95 1. 2 15 75-133 2.78.815 3 1,1-Dichloroethene 22.67 1. 2 113 7-145 22.55.531 3 1,2,3-Trichloropropane 2.16 1. 2 11 75-125 19.76 2 3 1,2,4-Trichlorobenzene 18.68 1. 2 93.4 7-135 17.66 5.61 3 1,2,4-Trimethylbenzene 2.5 1. 2 12 75-13 2.34.784 3 1,2-Dibromo-3-chloropropane 15.86 1. 2 79.3 6-13 15.54 2.4 3 1,2-Dibromoethane 22.75 1. 2 114 8-15 21.99 3.4 3 1,2-Dichlorobenzene 19.86 1. 2 99.3 7-13 19.41 2.29 3 1,2-Dichloroethane 19.98 1. 2 99.9 78-125 19.69 1.46 3 1,2-Dichloropropane 21.2 1. 2 15 75-125 2.47 2.65 3 1,3,5-Trimethylbenzene 21.29 1. 2 16 75-13 2.95 1.61 3 1,3-Dichlorobenzene 2.35 1. 2 12 75-13 19.66 3.45 3 1,4-Dichlorobenzene 2.2 1. 2 1 75-13 19.42 3.4 3 2-Butanone 17.28 5. 2 86.4 55-15 17.13.872 3 2-Hexanone 18.94 5. 2 94.7 6-135 17.53 7.73 3 4-Methyl-2-pentanone 24.55 1. 2 123 77-178 23.94 2.52 3 Acetone 18.66 1 2 93.3 6-16 15.73 17 3 Acrylonitrile 17.19 1. 2 86 6-14 16.8 6.67 3 Benzene 2.99 1. 2 15 85-125 2.5 2.36 3 Bromochloromethane 2.41 1. 2 12 75-13 2.6 1.73 3 Bromodichloromethane 2.96 1. 2 15 75-125 2.33 3.5 3 Bromoform 16.62 1. 2 83.1 6-125 16.8 3.3 3 Bromomethane 13.9 1. 2 69.5 3-185 13.6 6.23 3 Carbon disulfide 19.92 1. 2 99.6 6-165 19.45 2.39 3 Carbon tetrachloride 21.29 1. 2 16 65-14 2.6 3.29 3 Chlorobenzene 2.77 1. 2 14 8-12 2.58.919 3 Chloroethane 17.91 1. 2 89.6 5-14 17.32 3.35 3 Chloroform 19.79 1. 2 99 8-13 19.49 1.53 3 Chloromethane 16.15 1. 2 8.8 5-13 15.54 3.85 3 cis-1,2-dichloroethene 19.48 1. 2 97.4 75-134 19.51.154 3 cis-1,3-dichloropropene 18.32 1. 2 91.6 7-13 17.65 3.73 3 Dibromochloromethane 16.55 1. 2 82.8 6-115 16.56.64 3 Dibromomethane 21.6 1. 2 15 85-125 21.4 1.6 3 Dichlorodifluoromethane 2.32 1. 2 12 2-12 2.4 1.39 3 Ethylbenzene 22.3 1. 2 11 85-125 21.47 2.57 3 Hexachloroethane 14.86 1. 2 74.3 5-124 14.27 4.5 3 Isopropylbenzene 21.45 1. 2 17 8-127 2.87 2.74 3 m,p-xylene 45.43 2. 4 114 75-13 44.4 2.29 3 QC Page: 9 of 1

Client: Merit Energy Work Order: 166484 Project: ECT (Hartland - 13247 Lone Tree Rd) Batch ID: R189219 Instrument ID: VMS1 Method: SW826B Methyl iodide 26.31 1. 2 132 6-16 23.54 11.1 3 Methyl tert-butyl ether 15.3 1. 2 76.5 8-13 14.86 2.92 3 Methylene chloride 21.12 5. 2 16 75-14 21.31.896 3 Naphthalene 17.63 5. 2 88.2 55-16 16.44 6.99 3 n-propylbenzene 22.37 1. 2 112 78-12 22.6 1.4 3 o-xylene 21.75 1. 2 19 8-125 21.17 2.7 3 Styrene 2.92 1. 2 15 85-125 2.41 2.47 3 Tetrachloroethene 22.11 1. 2 111 77-138 21.47 2.94 3 Toluene 21.1 1. 2 15 85-125 2.64 1.78 3 trans-1,2-dichloroethene 19.3 1. 2 96.5 8-14 18.86 2.31 3 trans-1,3-dichloropropene 16.14 1. 2 8.7 81-123 15.89 1.56 3 trans-1,4-dichloro-2-butene 14.4 2. 2 7.2 46-118 13.66 2.74 3 Trichloroethene 21.45 1. 2 17 84-13 2.83 2.93 3 Trichlorofluoromethane 2.7 1. 2 14 6-14 21.1 1.49 3 Vinyl chloride 21.1 1. 2 16 5-136 2.56 2.59 3 Xylenes, Total 67.18 3. 6 112 8-126 65.57 2.43 3 Surr: 1,2-Dichloroethane-d4 2.3 2 1 75-12 19.77 1.31 3 Surr: 4-Bromofluorobenzene 2.25 2 11 8-11 2.44.934 3 Surr: Dibromofluoromethane 2.68 2 13 85-115 2.89 1.1 3 Surr: Toluene-d8 2.9 2 1 85-11 2.2.546 3 S S The following samples were analyzed in this batch: 166484-1A QC Page: 1 of 1

ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 13247 Lone Tree Rd) WorkOrder: 166484 Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: 166484 Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature 8-Jun-16 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.4/2.4 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:55:5 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

13-Jul-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI 49646 Re: Merit (13955 Cherry Blossom Ln) Work Order: 16739 Dear Sean, ALS Environmental received 1 sample on 8-Jul-216 1:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 18. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS 3352 128th Avenue Holland, Michigan 49424-9263 PHONE (616) 399-67 FAX (616) 399-6185 ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

ALS Group USA, Corp Date: 13-Jul-16 Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: 16739 Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date 16739-1 13955 Cherry Blossom Ln (Water Well) Date Received Water 7/7/216 14:3 7/8/216 1:3 Hold Sample Summary Page 1 of 1

ALS Group USA, Corp Date: 13-Jul-16 Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: 16739 Sample ID: 13955 Cherry Blossom Ln (Water Well) Lab ID: 16739-1 Collection Date: 7/7/216 2:3 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW846 827D Prep: SW351 / 7/11/16 Analyst: RM Diisopropanolamine 5 µg/l 1 7/12/216 1:36 PM Sulfolane 1 µg/l 1 7/12/216 1:36 PM Surr: 2,4,6-Tribromophenol 79. 38-115 %REC 1 7/12/216 1:36 PM Surr: 2-Fluorobiphenyl 64.7 32-1 %REC 1 7/12/216 1:36 PM Surr: 2-Fluorophenol 37.1 22-59 %REC 1 7/12/216 1:36 PM Surr: 4-Terphenyl-d14 65.9 23-112 %REC 1 7/12/216 1:36 PM Surr: Nitrobenzene-d5 68. 31-93 %REC 1 7/12/216 1:36 PM Surr: Phenol-d6 2.2 13-36 %REC 1 7/12/216 1:36 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,1-Trichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,2-Trichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 7/12/216 5:44 PM 1,1-Dichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1-Dichloroethene 1. µg/l 1 7/12/216 5:44 PM 1,2,3-Trichloropropane 1. µg/l 1 7/12/216 5:44 PM 1,2,4-Trichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 1,2,4-Trimethylbenzene 1. µg/l 1 7/12/216 5:44 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 7/12/216 5:44 PM 1,2-Dibromoethane 1. µg/l 1 7/12/216 5:44 PM 1,2-Dichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 1,2-Dichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,2-Dichloropropane 1. µg/l 1 7/12/216 5:44 PM 1,3,5-Trimethylbenzene 1. µg/l 1 7/12/216 5:44 PM 1,3-Dichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 1,4-Dichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 2-Butanone 5. µg/l 1 7/12/216 5:44 PM 2-Hexanone 5. µg/l 1 7/12/216 5:44 PM 2-Methylnaphthalene 5. µg/l 1 7/12/216 5:44 PM 4-Methyl-2-pentanone 1. µg/l 1 7/12/216 5:44 PM Acetone 1 µg/l 1 7/12/216 5:44 PM Acrylonitrile 1. µg/l 1 7/12/216 5:44 PM Benzene 1. µg/l 1 7/12/216 5:44 PM Bromochloromethane 1. µg/l 1 7/12/216 5:44 PM Bromodichloromethane 1. µg/l 1 7/12/216 5:44 PM Bromoform 1. µg/l 1 7/12/216 5:44 PM Bromomethane 1. µg/l 1 7/12/216 5:44 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

ALS Group USA, Corp Date: 13-Jul-16 Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: 16739 Sample ID: 13955 Cherry Blossom Ln (Water Well) Lab ID: 16739-1 Collection Date: 7/7/216 2:3 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17 92.4 13 95.7 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l 1 75-12 %REC 1 8-11 %REC 1 85-115 %REC 1 85-11 %REC 1 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

ALS Group USA, Corp Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: 16739 Date: 13-Jul-16 Case Narrative Batch R191319 The MS/MSD data for volatiles is not related to this project's sample. No data requires qualification. Batch R191319 The LCS recovery for volatile compounds 1,2 Dibromoethane and Methyl iodide was above the upper control limit. Sample results were non-detect for these compounds therefore no data requires qualification. Case Narrative Page 1 of 1

ALS Group USA, Corp Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Date: 13-Jul-16 Batch ID: 8841 Instrument ID: SVMS8 Method: SW846 827D MBLK Sample ID: SBLKW1-8841-8841 Units: µg/l Client ID: Run ID: SVMS8_16712A SeqNo: 3918355 Analysis Date: 7/12/216 12:32 PM Prep Date: 7/11/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol 41.77 5 83.5 38-115 Surr: 2-Fluorobiphenyl 35.4 5 7.1 32-1 Surr: 2-Fluorophenol 21.55 5 43.1 22-59 Surr: 4-Terphenyl-d14 41.3 5 82.6 23-112 Surr: Nitrobenzene-d5 35.82 5 71.6 31-93 Surr: Phenol-d6 13.26 5 26.5 13-36 LCS Sample ID: SLCSW1-8841-8841 Units: µg/l Client ID: Run ID: SVMS8_16712A SeqNo: 3918356 Analysis Date: 7/12/216 12:53 PM Prep Date: 7/11/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 16.54 5 1 16.5 1-5 Sulfolane 53.44 1 1 53.4 3-1 Surr: 2,4,6-Tribromophenol 38.13 5 76.3 38-115 Surr: 2-Fluorobiphenyl 31.66 5 63.3 32-1 Surr: 2-Fluorophenol 21.2 5 42.4 22-59 Surr: 4-Terphenyl-d14 37.49 5 75 23-112 Surr: Nitrobenzene-d5 33.79 5 67.6 31-93 Surr: Phenol-d6 13.11 5 26.2 13-36 LCSD Sample ID: SLCSDW1-8841-8841 Units: µg/l Client ID: Run ID: SVMS8_16712A SeqNo: 3918357 Analysis Date: 7/12/216 1:14 PM Prep Date: 7/11/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 14.1 5 1 14 1-5 16.54 3 Sulfolane 53.3 1 1 53 3-1 53.44.77 3 Surr: 2,4,6-Tribromophenol 4.35 5 8.7 38-115 38.13 5.66 3 Surr: 2-Fluorobiphenyl 33.3 5 66.1 32-1 31.66 4.24 3 Surr: 2-Fluorophenol 2.85 5 41.7 22-59 21.2 1.66 3 Surr: 4-Terphenyl-d14 38.26 5 76.5 23-112 37.49 2.3 3 Surr: Nitrobenzene-d5 34.93 5 69.9 31-93 33.79 3.32 3 Surr: Phenol-d6 11.79 5 23.6 13-36 13.11 1.6 3 The following samples were analyzed in this batch: 16739-1B QC Page: 1 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B MBLK Sample ID: VBLKW1-16712-R191319 Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: 3918579 Prep Date: Analysis Date: 7/12/216 1:21 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 2 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d4 2.94 2 15 75-12 Surr: 4-Bromofluorobenzene 18.79 2 94 8-11 Surr: Dibromofluoromethane 19.85 2 99.2 85-115 Surr: Toluene-d8 19.61 2 98 85-11 QC Page: 3 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B LCS Sample ID: VLCSW1-16712-R191319 Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: 3918578 Prep Date: Analysis Date: 7/12/216 12:6 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 22.13 1. 2 111 8-13 1,1,1-Trichloroethane 21.9 1. 2 15 75-13 1,1,2,2-Tetrachloroethane 2.44 1. 2 12 75-13 1,1,2-Trichloroethane 22.54 1. 2 113 75-125 1,1-Dichloroethane 17.93 1. 2 89.6 75-133 1,1-Dichloroethene 19.36 1. 2 96.8 7-145 1,2,3-Trichloropropane 22.54 1. 2 113 75-125 1,2,4-Trichlorobenzene 22.41 1. 2 112 7-135 1,2,4-Trimethylbenzene 23.47 1. 2 117 75-13 1,2-Dibromo-3-chloropropane 23.8 1. 2 115 6-13 1,2-Dibromoethane 32.84 1. 2 164 8-15 1,2-Dichlorobenzene 2.77 1. 2 14 7-13 1,2-Dichloroethane 19.3 1. 2 96.5 78-125 1,2-Dichloropropane 17.92 1. 2 89.6 75-125 1,3,5-Trimethylbenzene 24.48 1. 2 122 75-13 1,3-Dichlorobenzene 21.37 1. 2 17 75-13 1,4-Dichlorobenzene 2.85 1. 2 14 75-13 2-Butanone 15.79 5. 2 79 55-15 2-Hexanone 17.92 5. 2 89.6 6-135 4-Methyl-2-pentanone 21 1. 2 15 77-178 Acetone 15.72 1 2 78.6 6-16 Acrylonitrile 15.69 1. 2 78.4 6-14 Benzene 19.98 1. 2 99.9 85-125 Bromochloromethane 15.87 1. 2 79.4 75-13 Bromodichloromethane 2.79 1. 2 14 75-125 Bromoform 18.59 1. 2 93 6-125 Bromomethane 17 1. 2 85 3-185 Carbon disulfide 18.42 1. 2 92.1 6-165 Carbon tetrachloride 2.24 1. 2 11 65-14 Chlorobenzene 21.76 1. 2 19 8-12 Chloroethane 15.65 1. 2 78.2 5-14 Chloroform 16.63 1. 2 83.2 8-13 Chloromethane 14.3 1. 2 7.2 5-13 cis-1,2-dichloroethene 17.49 1. 2 87.4 75-134 cis-1,3-dichloropropene 17.31 1. 2 86.6 7-13 Dibromochloromethane 17.41 1. 2 87 6-115 Dibromomethane 22.5 1. 2 112 85-125 Dichlorodifluoromethane 15.55 1. 2 77.8 2-12 Ethylbenzene 21.7 1. 2 15 85-125 Hexachloroethane 14.93 1. 2 74.6 5-124 Isopropylbenzene 23.79 1. 2 119 8-127 m,p-xylene 43.28 2. 4 18 75-13 S QC Page: 4 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B Methyl iodide 42.46 1. 2 212 6-16 Methyl tert-butyl ether 17.56 1. 2 87.8 8-13 Methylene chloride 16.24 5. 2 81.2 75-14 Naphthalene 21.43 5. 2 17 55-16 n-propylbenzene 22.81 1. 2 114 78-12 o-xylene 2.78 1. 2 14 8-125 Styrene 23.61 1. 2 118 85-125 Tetrachloroethene 24.83 1. 2 124 77-138 Toluene 21.5 1. 2 15 85-125 trans-1,2-dichloroethene 18.12 1. 2 9.6 8-14 trans-1,3-dichloropropene 17.7 1. 2 85.4 81-123 trans-1,4-dichloro-2-butene 16.44 2. 2 82.2 46-118 Trichloroethene 22.58 1. 2 113 84-13 Trichlorofluoromethane 17.87 1. 2 89.4 6-14 Vinyl chloride 15.81 1. 2 79 5-136 Xylenes, Total 64.6 3. 6 17 8-126 Surr: 1,2-Dichloroethane-d4 2.2 2 1 75-12 Surr: 4-Bromofluorobenzene 2.29 2 11 8-11 Surr: Dibromofluoromethane 2.33 2 12 85-115 Surr: Toluene-d8 2.27 2 11 85-11 S QC Page: 5 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B MS Sample ID: 16754-11A MS Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: 3919521 Prep Date: Analysis Date: 7/12/216 9:2 PM DF: 5 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 132 5 1 13 8-13 1,1,1-Trichloroethane 13 5 1 13 75-13 1,1,2,2-Tetrachloroethane 114 5 1 11 75-13 1,1,2-Trichloroethane 146 5 1 15 75-125 1,1-Dichloroethane 92 5 1 92 75-133 1,1-Dichloroethene 9945 5 1 99.4 7-145 1,2,3-Trichloropropane 161 5 1 16 75-125 1,2,4-Trichlorobenzene 114 5 1 11 7-135 1,2,4-Trimethylbenzene 118 5 1 111 75-13 1,2-Dibromo-3-chloropropane 11 5 1 11 6-13 1,2-Dibromoethane 1582 5 1 158 8-15 1,2-Dichlorobenzene 147 5 1 15 7-13 1,2-Dichloroethane 982 5 1 98.2 78-125 1,2-Dichloropropane 916 5 1 91.6 75-125 1,3,5-Trimethylbenzene 1182 5 1 118 75-13 1,3-Dichlorobenzene 146 5 1 15 75-13 1,4-Dichlorobenzene 13 5 1 1 75-13 2-Butanone 73 2,5 1 73 55-15 2-Hexanone 7775 2,5 1 77.8 6-135 4-Methyl-2-pentanone 947 5 1 94.7 77-178 Acetone 778 5, 1 77.8 6-16 Acrylonitrile 794 5 1 79.4 6-14 Benzene 138 5 1 14 85-125 Bromochloromethane 8315 5 1 83.2 75-13 Bromodichloromethane 988 5 1 98.8 75-125 Bromoform 8355 5 1 83.6 6-125 Bromomethane 8485 5 1 84.8 3-185 Carbon disulfide 865 5 1 86.5 6-165 Carbon tetrachloride 963 5 1 96.3 65-14 Chlorobenzene 171 5 1 17 8-12 Chloroethane 81 5 1 8.1 5-14 Chloroform 8435 5 1 84.4 8-13 Chloromethane 775 5 1 7.8 5-13 cis-1,2-dichloroethene 2223 5 1 1346 87.8 75-134 cis-1,3-dichloropropene 837 5 1 83.7 7-13 Dibromochloromethane 823 5 1 82.3 6-115 Dibromomethane 1112 5 1 111 85-125 Dichlorodifluoromethane 747 5 1 74.7 2-12 Ethylbenzene 132 5 1 13 85-125 Hexachloroethane 673 5 1 67.3 5-124 Isopropylbenzene 1149 5 1 115 8-127 m,p-xylene 2148 1, 2 17 75-13 S QC Page: 6 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B Methyl iodide 2262 5 1 226 6-16 Methyl tert-butyl ether 875 5 1 87 8-13 Methylene chloride 8415 2,5 1 84.2 75-14 Naphthalene 974 2,5 1 97.4 55-16 n-propylbenzene 182 5 1 18 78-12 o-xylene 136 5 1 14 8-125 Styrene 1174 5 1 117 85-125 Tetrachloroethene 1246 5 1 125 77-138 Toluene 143 5 1 14 85-125 trans-1,2-dichloroethene 943 5 1 94.3 8-14 trans-1,3-dichloropropene 787 5 1 78.7 81-123 trans-1,4-dichloro-2-butene 758 1, 1 75.8 46-118 Trichloroethene 3613 5 1 254 17 84-13 Trichlorofluoromethane 94 5 1 94 6-14 Vinyl chloride 122 5 1 421 78.1 5-136 Xylenes, Total 3184 1,5 3 16 8-126 Surr: 1,2-Dichloroethane-d4 14 1 14 75-12 Surr: 4-Bromofluorobenzene 118 1 12 8-11 Surr: Dibromofluoromethane 9955 1 99.6 85-115 Surr: Toluene-d8 992 1 99.2 85-11 S S QC Page: 7 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B MSD Sample ID: 16754-11A MSD Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: 3919522 Prep Date: Analysis Date: 7/12/216 9:27 PM DF: 5 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane 188 5 1 19 8-13 132 5.24 3 1,1,1-Trichloroethane 158 5 1 16 75-13 13 2.59 3 1,1,2,2-Tetrachloroethane 124 5 1 12 75-13 114.981 3 1,1,2-Trichloroethane 182 5 1 18 75-125 146 3.39 3 1,1-Dichloroethane 972 5 1 97.2 75-133 92 5.5 3 1,1-Dichloroethene 132 5 1 13 7-145 9945 3.65 3 1,2,3-Trichloropropane 171 5 1 17 75-125 161.938 3 1,2,4-Trichlorobenzene 143 5 1 14 7-135 114 2.87 3 1,2,4-Trimethylbenzene 116 5 1 116 75-13 118 4.54 3 1,2-Dibromo-3-chloropropane 119 5 1 12 6-13 11.838 3 1,2-Dibromoethane 1591 5 1 159 8-15 1582.567 3 1,2-Dichlorobenzene 147 5 1 15 7-13 147 3 1,2-Dichloroethane 9975 5 1 99.8 78-125 982 1.57 3 1,2-Dichloropropane 934 5 1 93.4 75-125 916 1.95 3 1,3,5-Trimethylbenzene 1189 5 1 119 75-13 1182.548 3 1,3-Dichlorobenzene 187 5 1 19 75-13 146 3.8 3 1,4-Dichlorobenzene 132 5 1 13 75-13 13 2.9 3 2-Butanone 767 2,5 1 76.7 55-15 73 4.94 3 2-Hexanone 83 2,5 1 8.3 6-135 7775 3.23 3 4-Methyl-2-pentanone 7465 5 1 74.6 77-178 947 23.7 3 Acetone 87 5, 1 8.7 6-16 778 3.66 3 Acrylonitrile 85 5 1 8 6-14 794.815 3 Benzene 149 5 1 15 85-125 138 1.1 3 Bromochloromethane 8775 5 1 87.8 75-13 8315 5.38 3 Bromodichloromethane 166 5 1 17 75-125 988 7.64 3 Bromoform 857 5 1 85.7 6-125 8355 2.54 3 Bromomethane 8815 5 1 88.2 3-185 8485 3.82 3 Carbon disulfide 9435 5 1 94.4 6-165 865 8.68 3 Carbon tetrachloride 118 5 1 12 65-14 963 5.6 3 Chlorobenzene 184 5 1 18 8-12 171 1.16 3 Chloroethane 847 5 1 84.7 5-14 81 5.58 3 Chloroform 895 5 1 89.5 8-13 8435 5.92 3 Chloromethane 7135 5 1 71.4 5-13 775.844 3 cis-1,2-dichloroethene 231 5 1 1346 96.5 75-134 2223 3.86 3 cis-1,3-dichloropropene 8725 5 1 87.2 7-13 837 4.15 3 Dibromochloromethane 839 5 1 83.9 6-115 823 1.93 3 Dibromomethane 1132 5 1 113 85-125 1112 1.78 3 Dichlorodifluoromethane 7435 5 1 74.4 2-12 747.47 3 Ethylbenzene 166 5 1 17 85-125 132 3.29 3 Hexachloroethane 6565 5 1 65.6 5-124 673 2.48 3 Isopropylbenzene 1177 5 1 118 8-127 1149 2.41 3 m,p-xylene 2178 1, 2 19 75-13 2148 1.36 3 S S QC Page: 8 of 9

Client: Merit Energy Work Order: 16739 Project: Merit (13955 Cherry Blossom Ln) Batch ID: R191319 Instrument ID: VMS9 Method: SW826B Methyl iodide 236 5 1 231 6-16 2262 1.93 3 Methyl tert-butyl ether 995 5 1 91 8-13 875 4.38 3 Methylene chloride 881 2,5 1 88.1 75-14 8415 4.59 3 Naphthalene 9845 2,5 1 98.4 55-16 974 1.7 3 n-propylbenzene 112 5 1 11 78-12 182 1.83 3 o-xylene 148 5 1 15 8-125 136 1.2 3 Styrene 1214 5 1 121 85-125 1174 3.39 3 Tetrachloroethene 1262 5 1 126 77-138 1246 1.2 3 Toluene 168 5 1 17 85-125 143 2.42 3 trans-1,2-dichloroethene 9695 5 1 97 8-14 943 2.77 3 trans-1,3-dichloropropene 812 5 1 81.2 81-123 787 3.13 3 trans-1,4-dichloro-2-butene 77 1, 1 77 46-118 758 1.57 3 Trichloroethene 368 5 1 254 114 84-13 3613 1.84 3 Trichlorofluoromethane 957 5 1 95.7 6-14 94 1.79 3 Vinyl chloride 124 5 1 421 81.8 5-136 122 3.7 3 Xylenes, Total 3226 1,5 3 18 8-126 3184 1.31 3 Surr: 1,2-Dichloroethane-d4 12 1 12 75-12 14 1.94 3 Surr: 4-Bromofluorobenzene 19 1 11 8-11 118.937 3 Surr: Dibromofluoromethane 9835 1 98.4 85-115 9955 1.21 3 Surr: Toluene-d8 987 1 98.7 85-11 992.55 3 S The following samples were analyzed in this batch: 16739-1A QC Page: 9 of 9

ALS Group USA, Corp Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) WorkOrder: 16739 Date: 13-Jul-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit backgro or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jul-16 1:3 Work Order: 16739 Received by: DS Checklist completed by Diane Shaw Gary Byar 8-Jul-16 Reviewed by: esignature Date esignature 8-Jul-16 Date Matrices: Carrier name: Water UPS Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 4.6/4.6 c SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 7/8/216 1:35:5 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

2024 © sciencedocbox.com Privacy Policy | Terms of Service | Feedback