A.C. Pronk & A.A.A. Molenaar Road & Railway Engineering, Delft University of Technology, Delft, The Netherlands

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The Modified Partial Healing Model used as a Prediction Tool for the Complex Stiffness Modulus Evolutions in Four Point Bending Fatigue Tests based on the Evolutions in Uni-Axial Push-Pull Tests. A.C. Pronk & A.A.A. Molenaar Road & Railway Engineering, Delft University of Technology, Delft, The Netherlands ABSTRACT: The Partial Healing (PH) model has proven to be a good tool in describing the evolution of the (weighted) complex stiffness modulus for a beam in a four point bending continuous fatigue test in controlled deflection mode. In principle the PH model is a material model which describes the change in the complex stiffness modulus for a unit volume due to loading. Taking into account the geometrical dimensions of the tested specimen the evolution of the weighted complex stiffness modulus for the specimen can be calculated when the parameters of the PH material model are known. The stress-strain field in uni-axial push-pull (UPP) tests ought to be homogenous over the length and the cross area of the cylinder. So, the evolution of the complex stiffness modulus in the UPP test can be used directly for the determination of the (material) parameters of the PH model. Therefore UPP tests can be used to predict the evolution of the complex stiffness modulus in two point bending (2PB) and four point bending (4PB) tests which can be compared with the measured evolution. This procedure is applied to 4PB test results of a RILEM project using a modified PH model. The modified PH model takes into account the possible existence of the so called low endurance limit. In the RILEM project several devices were used to investigate the fatigue properties of the same mix. The results for the UPP and 4PB tests are presented in this paper together with a new view on the definition and determination of the fatigue life. This might open a way for a comparison of the fatigue lives measured with different devices. KEY WORDS: Fatigue, endurance limit, healing, stiffness modulus evolution, fatigue life. 1 INTRODUCTION A major criterion in the design of asphalt pavements is the fatigue characteristics of an asphalt mix. The determinations of the fatigue characteristics are often carried out with dynamic cyclic bending tests with two, three or four point bending (2PB, 3PB, 4PB) devices applying constant sinusoidal deflections at a certain frequency and at a constant temperature. Force, deflection and the phase lag between force and deflection are measured during the test and are used for the calculation of the beam stiffness modulus. Normally the fatigue life is defined as the number of cycles at which the beam stiffness modulus has decreased to half its initial value. Mainly because the response of the specimen (beam) is measured and not the response of the material, the fatigue life determined with different devices will differ even between two similar devices but with different geometries for the specimens. This lack of agreement can be avoided if a material response model is the starting point of the back calculation. By taking into account the differences in configuration and stress/strain distributions in the specimen the response of the tested specimen can be determined.

Another issue is the phenomenon of healing. Rest periods during a fatigue test can increase the fatigue life (Bonnaure et al. 1982, Francken, 1978, Kim et al. 1989, Kim et al. 1994, Pronk, 1997). In these investigations the effect of healing was studied by applying real rest periods. However, if instead of a real rest period a pseudo rest period is applied with lower strain amplitude it has been shown that the stiffness also increases during these pseudo rest periods (Pronk, 1997). This implies that the phenomenon of reversible damage should be directly incorporated in the interpretation of fatigue tests with respect to the evolution of the stiffness modulus and phase lag. Therefore a material model should be used that implicitly includes the phenomenon of healing. Such a model is the Partial Healing (PH) model (Pronk, 21).The equations of the PH model are believed to describe the evolution of the complex stiffness modulus (modulus and phase lag) during the fatigue test satisfactorily. 2 THEORY The PH model is in principle a material model that describes the evolution of the properties for a unit volume. After integration over the dimensions of the specimen, taking into account the configuration (spatial strain/stress distribution) of the test device, a weighted complex stiffness modulus for the specimen is obtained. Given the complexity of the equations in the PH model this integration has to be carried out numerical. It is assumed that next to the viscous-elastic dissipated energy ΔW dis, which is completely transformed into heat, also energy is dissipated for the creation of micro cracks, dislocations and other defects. In strain controlled fatigue tests with sinusoidal loading the dissipated viscous-elastic dissipated energy per cycle is given by equation 1 in which ε is the constant strain, σ is the stress, S is the stiffness modulus, ϕ is the phase lag between σ and ε and F represents the loss modulus. ( ) 2 2 Δ W = sin( ) = Ssin = dis πεσ φ πε ϕ πε F (1) The assumption is that the damage Q is considered to have the same formulation as ΔW dis (Pronk, 199) which leads for strain controlled tests to equation 2 in which δ is a small parameter and T is the reciprocal value of the applied frequency f. d d ΔWdis 2 Q = δ. Wdis δ = δ fπε F (2) dt dt T The damage Q affects both the loss modulus F and the storage modulus G during loading according to equations 3 and 4. The first term in the integrals with the parameters α 1, 2 and β represents damage which heals in time (reversible damage) and the second term with the parameter γ 1,2 represents the irreversible damage which will just accumulate during the fatigue test. t dq {} τ ( ) {} β t τ Ft = F + α e γ 1 1 dτ o dτ t dq {} τ β( t τ) Gt {} = G α e γ 2 2 dτ o + dτ (3) (4)

The source of the reversible damage is not really known. In the author s view it could be a kind of pseudo plasticity like thixotropy or a thin liquid behavior. Nevertheless, equations 3 and 4 describe the measured evolutions very well. Fitting the PH model on 4PB fatigue tests at different strain levels showed that the parameter β is dependent on the squared value of the applied strain (β=β ε 2 ). Due to the transformation of the dissipated viscous-elastic energy per cycle (equation 1) into heat the temperature of the tested specimen will increase and as a consequence the modulus of the complex stiffness modulus will decrease and the phase lag will increase. This phenomenon is not taken into account in the PH model. But if forced convection temperature control is used, the temperature increase is limited in 4PB and UPP tests (Pronk, 1996). It should be marked that for the asphalt mix at issue the coefficient α 1 for the reversible damage of the loss modulus F turned out to be nil. This simplifies the equations considerable. 3 UNI-AXIAL PUSH-PULL TESTS As mentioned above the PH model is a material model. Therefore a direct application of the PH model is only possible for the UPP tests. In a RILEM project (Di Benedetto et al. 24) fatigue tests were carried out on the same mix using different fatigue devices. The results for the UPP and 4PB tests are used in this paper. In the UPP test the evolution of the complex stiffness modulus for any unit volume should be equal to the evolution for the whole cylinder. However, a constant uniform strain field throughout the whole UPP cylinder is difficult to maintain. Normally three strain gages or LVDT s, which are equally located around the specimen (12 degrees), are used for the process control. In practice only in 2% of the tests the strains measured by the three sensors can be considered equal to each other (mean differences less than 5 µm/m). Here only two UPP tests can be considered as real constant strain tests (E13D8-14 and E13D18-17; table 1). Nevertheless taking the mean strain value it appears that the evolution of the complex stiffness modulus in the other tests could also be fitted very well with the PH model. The fit is carried out starting with cycle 1 in order to eliminate partly the relatively large temperature effect in the initial phase of the test. The end of the regression interval was taken equal to the fatigue life N1 (Hopman et al. 1989). In total five UPP tests were available. In table 1 the mean values of the strains in this interval are given together with the range and if the strains decreased or increased on this interval. Table 1: Strain amplitudes on the interval from 1 cycles to N1 and the variation in strain amplitudes ( random, increase or decrease) on this interval. Beam Average Minimum Maximum Change [μm/m] [μm/m] [μm/m] E13D 8 14 81.9 79.3 83.4 random E13D 18 17 173.6 17 176 E13D 1 1 115 19 126 E13D 1 1 159.4 151 179 E13D 1 13 111.2 17 12 The values for the regression coefficients are given in table 2 if a mean strain value is adopted. Even for an increase of 28 µm/m on the regression interval (E13D1-1) the fit is good as indicated in figure 1. Reversible damage in the loss modulus was taken into account in the PH model, but it appeared that at least for this asphalt mix this term is nil (δα 1 = ).

12 Fitted Smix Fitted Loss Modulus Fitted Phase Measured Smix Measured Loss Modulus Measured Phase 3 Modulus [MPa] 8 4 25 2 Phase [degree] 2 4 6 8 1 12 Cycles 15 Figure 1: Measured and fitted evolution of the complex stiffness modulus for cylinder E13D1-1 in the UPP test while using a mean strain value of 159.4 μm/m. Table 2: PH parameter values from regressions adopting mean strain values on the interval. S mix ϕ Beam δα 1 = δα 2 = δγ 1 = δγ 2 = β = α 1 /(πfε 2 ) α 2 (πfε 2 ) γ 1 /(πfε 2 ) γ 1 /(πfε 2 ) β/ε 2 [-] [-] [-] [-] [s -1 ] [GPa] [ o ] E13D 8-14 242.8 3.4 15. 222 1.5 18.5 E13D1-1 731.6 7.5 52.5 512 12.3 17.9 E13D1-1 856. 25. 121.8 56 1.9 19.4 E13D1-13 74.7 7.5 45.1 515 11.4 17.9 E13D18-17 1111.1 47.9 136,3 547 11.2 2.9 The individual fits are good as shown in figure 1, but the fitted values for the PH parameters in table 2, especially the parameters δγ 1 and δγ 2, are quite different from each other, which is not in accordance with the starting point in the theory. In the theory it is adopted that the parameters δα 1, δα 2, δγ 1, δγ 2 and β are constants. However, it s not unlikely that both the reversible and irreversible damage will increase with a higher strain level. In view of the results given in table 2 and the good comparison between regression and measured evolution, the time decay constant β can be taken equal to 52, [s -1 ] without introducing large deviations. Table 3: PH parameter values if the parameter α 1 is taken equal to and β equal to 5, s -1. Beam Average ε δα 2 = α 2 /(πfε 2 ) δγ 1 = γ 1 /(πfε 2 ) δγ 2 = γ 1 /(πfε 2 ) [µm/m] [-] [-] [-] E13D8-14 81.9 579.3 3.4 16.4 E13D1-13 111.2 748.5 7.5 45.2 E13D1-1 115 742.9 7.5 52.6 E13D1-1 159.4 875.4 25. 123. E13D18-17 173.6 16.1 47.9 133.8

A regression with these adoptions leads to the PH parameter values given in table 3. The renewed regression did not lead to larger deviations between the fitted and the measured evolutions as indicated by figure 2 for beam E13D8-14. The obtained coefficients seem to depend on the applied strain level (table 3). 12 Fitted Smix Measured Loss Modulus Fitted Phase Measured Smix Fitted Loss Modulus Measured Phase 25 Modulus [MPa] 8 4 2 Phase [degree] 1 2 3 Cycles Figure 2: Measured and fitted evolutions of the complex stiffness modus for cylinder E13D8-14 using the PH parameters values of table 3 (δα 1 = and β = 52, s -1 ). 15 4 MODIFIED PH MODEL In figures 3 and 4 the values of table 3 are plotted as a function of the strain amplitude. The trends of the values for the permanent damage regression coefficients δγ 1 and δγ 2 in figure 3 indicate the existence of the so called endurance limit (equation 8). Here the endurance limit is taken equal to 74 μm/m. The best relation for γ 1 δ is than:.24 1 6 (ε 74 1 6 ). ( ) δγ = γ ε ε for ε > ε and nil for ε < ε (8) 1,2 1,2 limit endurance endurance Below the endurance limit the stiffness modulus will still decrease in the start of a fatigue test but will also restore completely. The decrease is more than can be expected of the small increase in temperature (less than 1.5 degrees Celsius in a temperature cabinet with forced convection temperature control). The intercept of the trend line in figure 4 is taken equal to nil because for ε = the PH parameters should be nil as well. Based on these calculations the parameters for the modified PH model which are used for the prediction of the evolution of the complex stiffness modulus in 4PB tests are presented in table 4. The only parameters which will be fitted for the comparison with the measured evolution in the 4PB tests are the initial loss modulus and storage modulus. Asphalt is not a very homogenous material and due to the natural variability the parameters might vary per specimen. Therefore in a second step some of the parameters mentioned in table 4 will also be varied in order to investigate whether another combination of parameters yields a better fit.

PH parameters δγ1 & δγ2 14 12 1 8 δγ 2 = 1.365 1 6 (ε - 74 1-6 ) δγ 1 δγ 2 R 2 =.998 δγ 1 =.46 1 6 (ε - 88 1-6 ) 6 R 2 =.85 4 2 5 7 9 11 13 15 17 19 Strain amplitude [μm/m] Figure 3: The PH parameters δγ 1 and δγ 2 as a function of the strain amplitude ε (table 3). PH parameter δα2 12 1 8 6 4 δα 2 = 6,15 1-6 ε R 2 =,83 5 7 9 11 13 15 17 19 Strain amplitude [μm/m] Figure 4: The PH parameter δα 2 as a function of the strain amplitude ε (table 3). Table 4: PH parameter values used for the prediction of stiffness evolution in 4PB tests. δα 1 = α 1 /(πfε 2 ) [-/-] δα 2 = α 2 (πfε 2 ) [-/-] = δα 2 ε = 6.15 1 6 ε δγ 1 = γ 1 /(πfε 2 ) [-/-] = δγ 1 (ε ε lim ) =.24 1 6 (ε ε lim ) δγ 2 = γ 1 /(πfε 2 ) [-/-] = δγ 2 (ε ε lim ) = 1.365 1 6 (ε ε lim ) β = β/ε 2 [s -1 ] = 52, ε lim [μm/μm] = 74 1-6 5 FOUR POINT BENDING DATA In the same RILEM project 12 prismatic beams (4555 mm 3 ) were tested in a 4PB device of which the outer span was 4 mm and the mid span was 13 mm. The beams were sawn from 4 slabs. Three strain levels were used in the tests at a frequency of 9.8 Hz and at a temperature of 2 C. An overview is given in table 5 together with the fatigue life N1 (based on a change in the dissipated energy ratio; Hopman, 1989) and the traditional fatigue life N f,5 (based on a 5% reduction of the initial stiffness modulus).

Table 5: 4PB beams used in the RILEM project. Beam code Strain ε [μm/m] N1 [k cycles] N f,5 [k cycles] 51 137 51 12 53 218 48 11 54 177 17 34 A51 137 4 1 A53 178 13 27 A54 217 42 9 A61 138 2 43 A62 219 9 2 A64 179 16 27 B61 218 12 2 B62 137 27 46 B63 177 12 215 6 NUMERICAL INTEGRATION OF THE PH MODEL In contrast with the UPP test the 4PB test is not a homogenous test with respect to the strain distribution. The strain is maximal at the surface in the mid span and decreases linearly to nil at the neutral zone halfway through the beam. In the outer sections the strain decreases to nil at the outer supports. At this location the material will in principle not be damaged in the fatigue test. Therefore an integration of the PH model over the whole specimen has to be performed. This is done in a numerical way using Simpson s rule. One half of the outer section of the beam is divided in 11 = 1 unit volumes. For the mid span the stiffness modulus distribution is equal to the one at the inner support. The weighted loss modulus F and weighted storage modulus G for the beam are calculated according to equation 9 because in the bending of the beam the product of the stiffness modulus and the bending moment is the relevant parameter. 15. 1 15. 1 2 2 F{ x, y,} t y dy dx G{ x, y,} t y dy dx F{} t = & G{} t = 15. 1 15. 1 2 2 y dy dx y dy dx (9) 7 APPLICATION OF THE MODIFIED PH MODEL ON THE RILEM 4PB DATA The PH parameters in table 4 are used for a comparison of the evolutions according to the modified PH model with the measured evolutions. Only the initial loss modulus and storage modulus are fitted. The comparisons between the measured evolutions and the evolutions according to the modified PH model were surprisingly fair to good for all beams as shown in figure 5 for beam 51. Probably due to the integration over the beam and the possible existence of an endurance limit, the information in the evolution of the complex stiffness modulus for the beam is sometimes not enough for determining a unique solution. The fitting is carried out by first varying Fo and Go alone, next adding δα 2 and β and at last δγ 1, δγ 2 and the endurance limit ε lim are added in the fit. The result of the fitting for beam 54 is presented in figure 6.

Beam Stiffness [MPa] 1 8 6 4 2 Stiffness Beam Model Stiffness Beam Data Loss Modulus Data Loss Modulus Model Phase Beam Model Phase Beam Data N1 Beam 51 ε limit = 74 μm/m N f,5 3 25 2 Phase [degree] 5 Cycles 1 15 15 Figure 5: Comparison of the evolution for the complex stiffness of beam 51 and the fitted evolution using the modified PH model with the parameter values of table 4. 12 Beam Stiffness Data Beam Stiffness Model Loss Modulus Data Loss Modulus Model Beam Phase Data Beam Phase Model 25 Beam Stiffness [MPa]] 1 8 6 4 2 Beam 54 ε = 177 μm/m N1 N f,5 2 15 1 Phase [degree] 1 2 3 4 Cycles 5 Figure 6: Comparison of the evolution for the complex stiffness of beam 54 and the fitted evolution using the modified PH model varying all parameters of table 4. The results for all beams following this protocol are given in table 6. To clarify the lack of information in the evolution of the complex beam stiffness for a good iteration a fit for beam A54 with complete other values for the parameters is given in figure 7. It is quite clear that this fit is also very good.

Table 6: Parameter values for the modified PH model in fitting the 4PB tests. Beam δα 2 [1 6 ] δγ 1 [1 6 ] δγ 2 [1 6 ] β [s -1 ] ε lim [μm/m] 51 6.15.24 1.36 52 59 53 7.88.361 1.55 824 54 6.15.24 1.36 417 5 A51 6.15.327 1.35 4925 3 A53 6.15.24 1.36 493 43 A54 6.15.56 2.22 767 12 A61 6.15.291 1.36 585 9 A62 6.15.318 1.35 1412 67 A64 6.15.316 1.35 544 26 B61 6.15.314 1.35 1147 47 B62 6.15.39 1.35 635 4 B63 6.15.297 1.35 72 18 Beam Stiffness [MPa]] 1 8 6 4 2 Beam Stiffness Data Beam Stiffness Model Beam Phase Data Beam Phase Model δα 2 δγ 1 ε lim = 8.55 1 6 ; β = 69, [s -1 ] =.81 1 6 ; δγ 2 = 3.26 1 6 = 59 [μm/m] 25 2 Phase [degree] 2 4 6 8 1 Cycles Figure 7: Comparison of measured data and the fitted modified PH model for beam A54 using different parameter values than given in table 4. 15 1 4PB data UPP data N = 8.36 1 13 ε - 3.9 R 2 =.75 (UPP + 4PB) Strain [μm/m] 1 1 1.E+4 1.E+5 Cycles 1.E+6 1.E+7 Figure 8: Comparison of fatigue lives N PH determined in UPP and 4PB tests.

8 PROPOSED NEW FATIGUE LIFE DEFINITION Next to the traditional definition N f, 5 for the fatigue life, the definition N1 based on a change in the dissipated energy per cycle is used in the interpretation of fatigue tests. However, both definitions fail when fatigue lives measured with different devices are compared. Given the very good fits using the modified PH model for the UPP and 4PB tests it is worthwhile to investigate if another definition might overcome this aspect. This fatigue life N PH is defined as the moment when the measured data for the complex stiffness modulus starts to deviate from the evolution fitted with the modified PH model. Clearly the determination of this moment is not really objective but as shown in figure 8 the values of N PH for the UPP and 4PB tests follow the same Wohler curve. Although the UPP fatigue lives are located at one side of the trend line this raises the confidence in the application of the PH model. 9 CONCLUSIONS The modified PH model describes the evolution of the complex stiffness modulus in a UPP test very well including the possible existence of an endurance limit. The material parameters of the modified PH model established in a UPP test can be used for describing the evolution of the weighted beam stiffness in a 4PB test. But good fits for the 4PB tests are also possible with different sets of material PH parameters. The numbers of cycles at which the comparable fits start to deviate from the measured data do not differ much. This number can be used as a fatigue life definition. The proposed fatigue life definition N PH has potential to align results from UPP and 4PB tests. For this project it turns out that the value for N PH is only a bit higher than N1. REFERENCES Bonnaure, F.P. et al., 1982. A laboratory investigation of the influence of rest periods on the fatigue characteristics of bituminous mixes. Proceedings of the Association of the Asphalt Pavement Technologists, Kansas, USA. Di Benedetto, H. et al., 24. Fatigue of bituminous mixtures. Materials and Structures, Volume 37, Issue 267. Francken, L., 1979. Fatigue of a bituminous mix under realistic loading conditions. De wegentechniek, Vol, XXIV, no. 4. (in Dutch and French). Hopman, P.C. et al., 1989. A renewed interpretation method for fatigue measurements - Verification of Miner s rule. Proceedings of the 4 th Eurobitume Symposium, Madrid, Spain. Kim, Y.R. and Little, D.N., 1989. Evaluation of Healing in Asphalt Concrete by means of the Theory of Non Linear Visco-Elasticity. Transportation Research Board, Washington, USA. Kim, Y.R. et al., 1994. Healing in asphalt concrete pavements: Is it real?. Transportation Research Board, Washington, USA. Pronk, A.C. et al., 199. Energy dissipation: The leading factor of fatigue. Proceedings Strategic Highway Research Program: Sharing the Benefits, London, UK. Pronk, A.C. et al., 1996. Temperature increase in an asphalt beam during fatigue; theory and practice. Proceedings Wegbouwkundige Werkdagen, ISBN 9-6628-221-5, CROW, Ede, The Netherlands. Pronk, A.C., 1997. Healing during fatigue in 4 point dynamic bending tests. Report: W-DWW-97-95, DWW, Delft, The Netherlands. Pronk, A.C., 21. Partial healing in fatigue tests on asphalt specimens. International Journal Road Materials and Pavement Design, Volume 4, Issue 4.