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Available online at www.sciencedirect.com ScienceDirect Procedia Engineering 161 (2016 ) 1057 1063 World Multidisciplinary Civil Engineering-Architecture-Urban Planning Symposium 2016, WMCAUS 2016 Calibration of TDR Test Probes for Measuring Moisture Changes In The Construction Layers of the Railway Line Libor Ižvolt a, Peter Dobeš a, *, Martin Me ár a a University of Žilina, Faculty of Civil Engineering, Department of Railway Engineering and Track Management (DRETM), Univerzitná 8215/1, 010 26 Žilina, Slovakia Abstract In the introduction of the paper there is characterized a way of monitoring the moisture in the structure of the railway substructure and its subgrade in the Experimental stand DRETM II, which is a part of the experimental workplace of the Department of Railway Engineering and Track Management. The substantial part of the paper is devoted to the characteristics and calibration of TDR (Time domain reflectometry) test probes for selected rock materials, which are incorporated into the construction of Experimental stand DRETM II (crushed aggregate fr.0/31.5 mm, crushed aggregate fr.0/63 mm and clay blended with river gravel), as a basic prerequisite for determination of the actual moisture and its changes in the body of the railway substructure and subgrade during the year. Finally, this article outlines a comparison of individual TDR probes used in calibration and their suitability for monitoring moisture in various materials used in construction layers of the Experimental stand DRETM II. 2016 The Authors. Published by Elsevier by Elsevier Ltd. Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). Peer-review under responsibility of the organizing committee of WMCAUS 2016. Peer-review under responsibility of the organizing committee of WMCAUS 2016 Keywords: time domain reflectometry; calibration of TDR test probes; moisture changes; construction layers of railway line; protective layer. 1. Introduction Water occurring the in structural layers of the railway track has a major impact not only on the deformation, but also on thermo-technical features of inbuilt construction materials. The moisture content of the track substructure is not constant, but it varies in the course of the year, depending on the amount of downfall (water, snow), temperature and water regime of the body of the track substructure as well as its shape (embankment, cutting, cut) [1]. The experimental * Corresponding author. Tel.: +421 41 513 5849. E-mail address: dobes@fstav.uniza.sk 1877-7058 2016 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). Peer-review under responsibility of the organizing committee of WMCAUS 2016 doi:10.1016/j.proeng.2016.08.848

1058 Libor Ižvolt et al. / Procedia Engineering 161 ( 2016 ) 1057 1063 workplace of the Department of Railway Engineering and Track Management has been dealing with the influence of weather factors water, frost, snow cover (non-traffic load of the railway line) on the temperature regime of the railway line - subgrade for a long period. The mathematical modeling of the thermal regime of the construction layer of railway line (using Canadian software SoilVision) has brought the need to determine the relevant input parameters. For this reason, the Experimental stand DRETM II (Fig. 1) was built at the campus of the University of Žilina. Unlike the Experimental stand DRETM I, besides the temperature regime it also allows to monitor the moisture changes in the construction of railway substructure and its subgrade. Fig. 1. Experimental stand DRETM II. The arrangement of the Experimental stand DRETM II in cross-section is shown in the article entitled Monitoring of moisture changes in the construction layers of the railway substructure body and its subgrade, which is published in this proceedings. The Experimental stand DRETM II with its structural composition, in-built materials and dimensions represents the real railroad and therefore it allows to confront the real measured parameters with the parameters obtained by mathematical modeling of the regime of construction layers of railway line [2]. The mathematical model created on the basis of relevant inputs should serve for dimensioning of the protective layer of subgrade surface in the construction of railway substructure, possibly to assess the suitability of the new building materials design for construction of railway substructure. To monitor and identify moisture in the individual structural parts of the Experimental stand DRETM II, there have been inbuilt protective tubes of TDR (Time Domain Reflectometry), [5] allowing to continuously monitor moisture changes and identify the moisture of materials built in the experimental stand profile at any time. Since the moisture TDR probes are designed primarily for moisture determination of fine-grained materials (of bulk density up to 1700 kg/m 3 ), contain calibration curves for these materials, and the structural parts of the Experimental stand DRETM II (ballast bed, construction layers of the railway substructure body including earthwork structure) are made up of coarsegrained (inconsistent) material, it was necessary to establish calibration curves for these moisture probes for all materials built in the stand. For this purpose, there were used test methods and procedures specified below to implement calibration of moisture probes. 2. Calibration of TDR test probes for inhomogeneous (inbuilt) materials The dielectric constant indicates the ability of non-conducting material (in our case a rock material) to transmit electromagnetic waves, [3]. The dielectric constant of water is much greater than its value for solid particles and air. This means that even relatively small changes in the amount of water in the rock material, i.e. the change of rock material moisture, has a great effect on its dielectric constant. The water content in the rock material can be determined using the calibration model, depending on the dielectric constant of the rock material and the volume of water in the rock material.

Libor Ižvolt et al. / Procedia Engineering 161 ( 2016 ) 1057 1063 1059 The first step that needs to be done to determine the water content in the material is the calibration of dielectric constant for each material in general. The approaches using the method of dielectric constant provide relatively quick measurements and accurate results if the calibration is properly implemented. 2.1. Methodology of calibration curve construction for TDR test probes The protection of TDR probe Trim Pico-Profile against mechanical damage is provided by its insertion into the protective PVC access tube. The sensitivity of measurement is the highest around the tube and decreases exponentially with distance to the medium as shown in Fig. 2. Fig. 2. Distribution of electromagnetic field around the probe [3]. The TDR probes were especially developed for fine-grained materials and therefore they contain basic calibration curves appropriate for these materials. Since not all the building materials applied in the body of the Experimental stand DRETM II met the conditions for this curve, it was necessary to carry out test measurements of inbuilt materials and create the appropriate calibration curves. The TDR test probes Trim Pico-Profile allow us to carry out the calibration and then to create a linear or non-linear dependence (to the polygon of 5th order) of the tested building materials. In order to create the calibration curve, there is used a probe connected to module SM-Bus (Fig. 3) and then the entire calibration is performed using the software product PICO-CONFIG. Fig. 3. Calibration of the TDR test probe for clay blended with river gravel.

1060 Libor Ižvolt et al. / Procedia Engineering 161 ( 2016 ) 1057 1063 The calibration curve is established on the basis of two measurement points. The first measurement point is obtained from the measurement of the dry sample (or a sample of low moisture), and the second measurement point is obtained from the sample of maximum possible moisture w m (maximum moisture). The time interval t p for the known, laboratory-determined moisture is measured according to the standard [5] and subsequently there are calculated coefficients m 0 and m 1 using the relation: m w w m 2 m1 1 (1) t p 2 t p1 m w m t (2) 0 m 2 1 p 2 where is: w m1(2) moisture of dry (saturated) material, (%), t p1(2) time interval obtained on a dry (saturated) sample, (ps). In order to achieve the highest possible accuracy of the moisture values of rock material there was used a combination of linear and non-linear method of calibration coefficient determination (determination of at least four time intervals according to at least four different moistures). 2.2. Calibration curves of inhomogeneous (inbuilt) materials Within the calibration of the TDR test probes, there were used three different materials taken from the Experimental stand DRETM II, where the crushed aggregate fr. 0/31.5 mm has the protective layer function, crushed aggregate fr. 0/63 mm forms the embankment of railway line and clay blended with river gravel is located in the subgrade of embankment [4]. The calibration coefficients and curves were created for 6 various TDR test probes with serial numbers 34315-34320. The measured time intervals t p for the moisture of calibrated materials determined by laboratory are shown in Tab. 1. Table 1. Time intervals measured for calibrated materials corresponding to certain moisture content w m. Crushed aggregate fr. 0/31.5 mm Crushed aggregate fr. 0/63 mm Clay blended with river gravel 34315 34316 34317 0.00 136 0.00 153 0.00 154 2.38 299 2.56 356 5.26 365 3.96 369 4.22 394 10.83 553 6.00 438 5.74 467 16.10 652 6.69 451 6.66 526 20.88 660 0.00 349 0.00 363 0.00 395 2.38 395 2.56 420 5.26 450 3.96 425 4.22 437 10.83 485 6.00 439 5.74 456 16.10 544 6.69 458 6.66 466 20.88 550 0.00 144 0.00 173 0.00 228 2.38 276 2.56 297 5.26 460 3.96 312 4.22 346 10.83 546 6.00 391 5.74 443 16.10 690 6.69 419 6.66 521 20.88 711 Table 1. Time intervals measured for calibrated materials corresponding to certain moisture content w m. continue

Libor Ižvolt et al. / Procedia Engineering 161 ( 2016 ) 1057 1063 1061 Crushed aggregate fr. 0/31.5 mm Crushed aggregate fr. 0/63 mm Clay blended with river gravel 34318 34319 34320 0.00 368 0.00 372 0.00 404 2.38 401 2.56 439 5.26 480 3.96 441 4.22 454 10.83 505 6.00 459 5.74 496 16.10 548 6.69 477 6.66 499 20.88 567 0.00 124 0.00 203 0.00 339 2.38 293 2.56 346 5.26 502 3.96 363 4.22 393 10.83 571 6.00 432 5.74 492 16.10 675 6.69 455 6.66 529 20.88 681 0.00 147 0.00 188 0.00 318 2.38 290 2.56 331 5.26 475 3.96 351 4.22 368 10.83 549 6.00 406 5.74 471 16.10 708 6.69 444 6.66 527 20.88 737 The range of time intervals t p was determined from at least 6 measurements, where the probe was placed in the protective tube in different positions in relation to the surrounding material, while for each position 10-time interval measurements were determined. From the measured values there were subsequently created calibration curves for the individual TDR probes that are shown in Fig. 4 to Fig. 6. Fig. 4. The dependence of moisture w m on the time interval t p for crushed aggregate fr. 0/31.5 mm. From the endpoints of the presented calibration curves there were subsequently calculated coefficients m 0 a m 1, which are shown in Tab. 2. The coefficients m 0 and m 1 were subsequently attributed by the program Pico Config to the appropriate TDR test probes and the check measurement was also done.

1062 Libor Ižvolt et al. / Procedia Engineering 161 ( 2016 ) 1057 1063 Fig. 5. The dependence of moisture w m on the time interval t p for crushed aggregate fr. 0/63 mm. Fig. 6. The dependence of moisture w m on the time interval t p for clay blended with river gravel. Table 2. Coefficients m 0 and m 1 calculated for individual TDR test probes and test materials. Crushed aggregate fr. 0/31.5 mm Crushed aggregate fr. 0/63 mm Clay blended with river gravel m 0 m 1 m 0 m 1 m 0 m 1 34315-9.258 0.0344-7.480 0.0274-1.226 50.402 34316-27.577 0.0752-37.893 0.0955-0.166 11.153 34317-5.554 0.0289-3.460 0.0201-0.884 41.291 34318-25.497 0.0675-22.587 0.0575-0.228 12.274 34319-6.351 0.0281-4.757 0.0214-0.676 30.470 34320-5.998 0.0287-3.830 0.0201-0.377 28.256

Libor Ižvolt et al. / Procedia Engineering 161 ( 2016 ) 1057 1063 1063 3. Conclusion Using the TDR probes, the applied method of dielectric constant measurement (which was the input parameter for determination of the moisture content), and high-quality calibration we can achieve high precision of measured values of moisture provided some conditions are met (sufficient consolidation to avoid air gaps, maximum moisture not exceeded, sufficient engagement of the probe in soil). The comparison of moisture values determined on the basis of calibration curves and the moisture of the samples determined in accordance with the procedure referred to in standard [6] are shown in Tab. 3. Table 3. Comparison of the measured moisture with the moisture of the samples determined according to the procedure referred to in standard [6] for individual TDR test probes. Crushed aggregate fr. 0/31.5 mm Crushed aggregate fr. 0/63 mm Clay blended with river gravel w m (TDR) w m [6] w m (TDR) w m [6] w m (TDR) w m [6] 34315 4.42-4.83 4.39-4.60 4.37-4.67 4.41-4.96 15.60-16.32 15.98-16.38 34316 3.47-4.02 4.39-4.60 4.41-4.94 4.41-4.96 16.40-17.20 15.98-16.38 34317 4.26-4.34 4.39-4.60 4.34-4.48 4.41-4.96 15.61-16.60 15.98-16.38 34318 3.48-3.86 4.39-4.60 3.00-4.17 4.41-4.96 16.27-17.30 15.98-16.38 34319 4.33-4.68 4.39-4.60 4.11-4.33 4.41-4.96 15.75-16.43 15.98-16.38 34320 4.19-4.49 4.39-4.60 3.94-4.77 4.41-4.96 15.84-16.16 15.98-16.38 As it is evident from Tab. 3, the measurement accuracy of the TDR test probes is within ± 0.5% (major differences were recorded only for the probe no. 34316 and no. 34318) and the value corresponds to the deviation stated by the manufacturer. Even thicker grading of the test material does not affect the accuracy of the measurement, (sometimes it is necessary to apply multiple measurements), in spite of the fact that the moisture probe is designed for fine-grained materials. It is thus clear that the measured moisture values are objective and can be used for detection of fluctuations in moisture of material built in the body of the railway substructure in the course of the year and the simulation of the thermal regime using the software SoilVision and the software product SV HEAT. Acknowledgements The presented results are the results of solving the VEGA grant project 1/0275/16 Structure optimization of sleeper subgrade due to non-traffic load aspect, which allows the realization of experimental measurements and consequently obtaining the relevant results that are presented in this paper. References [1] Ižvolt, L.: Railway substructure stress, diagnostics, design and implementation of body construction layers of railway subgrade. (Scientific monograph). University of Žilina, 2008, ISBN 978-80-8070-802-3. [2] Ižvolt, L., Hodas, S.: Software support for temperature regime modelling of railway track construction, in: Systemy transportowe, IX. konferencja naukowo-techniczna, Katowice, 2013, ISBN 978-83-926923-5-5. [3] Trime Pico-profile manual (http://www.imko.de/en/products/soilmoisture/soil-moisture-sensors/trimepicoipht3). [4] Dobeš, P.: Calibration of TDR test probe for measuring moisture in the body of the railway substructure and its subgrade, in: Civil and environmental engineering : scientific technical journal. - ISSN 1336-5835. - Vol. 11, no. 2 (2015), pp. 84-94. [5] Drusa M., Chenbe V. - Implementation of TDR Technology for Monitoring of Negative Factors of Slope Deformations, Proceedings of SGEM 2012 Vol II., ISSN 1314-2704 p.143-150, DOI: 10.5593/sgem2012 [6] STN 721012 Laboratory determination of soil moisture, 09/1980.