Fused silica suspension for the Virgo optics: status and perspectives

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Fused silica suspension for the Virgo optics: status and perspectives Helios Vocca for the Virgo Perugia Group

The expected Virgo Sensitivity 10-15 Total sensitivity h(f) [1/sqrt(Hz)] 10-16 10-17 10-18 10-19 10-0 10-1 10 - Total thermal noise Thermal noise: Mirror Thermal noise: Pendulum Shot noise Radiation Pressure Seismic Creep Magnetic Laser Power Acoustic Quantum Limit Newtonian (Cella) Newtonian (Thorne) 10-3 10-4 10-5 10 0 10 1 10 10 3 10 4 Frequency [Hz]

Pendulum Thermal Noise X g ( ω) 4kBT 5 ω 1 L w E g + θ 4π nm g E ml w φ T C wire b S Wire loss angle: φwire 0 th = φ + φ + φe T b : Breaking strength C S : Confidence factor φ 0 φ th φ e : Material loss angle : Thermoelastic loss angle : Excess loss angle Thermoelastic loss angle ωτ φth = 1+ ωτ Eα T = c τ = π d w D ( ) Excess loss angle Frictional processes in the marionetta-wire clamps Frictional losses in the wiremirror contact point

Present solution The Virgo present solution for the suspension last stage uses four 00 µm diameter C85 steel wires. In these conditions: - φ 0 10 4 - φ th (max) 10 3 (at 680 Hz) - C S = 0.6 - T b.9 GPa

Excess loss angle Frictional losses in the upper clamps High pressure clamping system Frictional losses in the wire mirror contact point Fused Silica spacers

What can we do best? Find a wire material with smaller loss angle and larger breaking strength!

φ w (f) 10-3 10-4 10-5 10-6 Measured losses of materials C85 steel Niobium Invar Sapphire SiC Aluchrom Chromalloy Marval φ 10-4 φ 10-6 Fused Silica SQ Suprasil New Fused Silica New F.S. with bob CuBe Titanium Tungsten A factor 10 on h sensitivity 10-7 Fused Silica Synthetic FS with bob 1 10 100 1000 frequency (Hz) Virgo Perugia group: G.Cagnoli et al., Phys. Lett. A 55 (1999) 30-35

Production facility Pure O -H flame No fibersupport contact Direct measurement of the fiber diameter Directly tested the fiber breaking strength

FS Breaking strength (1) 7 The breaking strength of FS fibers depends on material purity, production and handling procedure. 6 5 4 3 T T SiO b C 85 b = 4.05 ± 0.55 =.90 ± 0.0 GPa GPa 7000 6000 5000 Breaking Strength [MPa] 4000 3000 000 1000 Acid Alcohol 1 0 Dirty φw/t b is a factor 00 lower for FS fibers, but C s is lowered by the large T b fluctuation. H.Vocca et al., Proc. of the3th Lisa symposium (000, sub. to Class. Quant. Grav) M.Punturo et al, talk to the GREX meeting (Grasse, 000) P.Amico et al, Nuclear Inst. and Methods in Physics Research A, pp 97-99 Apr.001

FS Breaking strength () Very strong under elongation (and compression) Very fragile for shocks The Breaking strength is dramatically reduced by: Cracks on the fiber surface contact with metals or other hard surfaces Humidity some worry for ageing caused by humidity no statistical evidence for this effect in our labs, but some alarms this effect is reported by optical fiber producers (closest to the theoretical FS breaking strength) good news from Glasgow for fibers under vacuum more tests needed O O Si O O O Si O O H O H + OH - O O Si O OH OH O Si O O

Coating of the wire surface Surface coating could prevent FS ageing Effect of a Carbon coating (with Nitrogen contaminations) on loss angle has been tested An evident increase of the wire loss angle has been measured More tests are needed with different coatings and better thickness control. φ w (f) 10-4 F.S. with C coating F.S. with C plus N=30% F.S. with C plus N=60% F.S. without coating 10-5 10-6 100 1000 frequency (Hz)

Monolithic solution With FS fibers we can gain in φ 0 thermoelastic damping because of α SiO clamping losses breaking strength 6 1 6 1 0.5 10 K < αc 17 10 K SiO < C On the other hand we lose in C S due to the dispersion of the breaking strength 85 85

Clamping losses: Wire-marionetta clamp friction Wire-mirror lateral side friction Clamp with FS fibers The upper head can be welded to a larger head (a FS ring) that can be easily clamped to the marionetta (see later): few tests made in Perugia some problems with stresses accumulated in the head annealing procedure to be implemented (well known by the FS component producers) For the lower clamping we cannot hot-weld the wire to the mirror large thermal stress We cannot use glue Vacuum compatibility and substrate pollution We need to chemically bond the wire to the mirror without any pollution or thermal stress

Potassium silicate bonding Silicate bonding is a Hydroxide-Catalysis chemical process. Test are made in a class 10000 clean room, under a class 100 laminar flux. It is important a: control of the purity of H O and KOH accurate cleaning of the SiO samples In this conditions the breaking strength vs time of samples with different flatness quality has been investigated (λ/4, λ/7 and λ/10). For λ/10 samples we are dominated by the clamping Mean λ/4 =.5±0.6 MPa Mean λ/7 =3.3±0.8 MPa Mean λ/10 =3.9±0.5 MPa Breaking Stress [M p a ] 6 4 0 1 3 4 5 6 7 8 9 1 0 1 0 1 0 0 7 1 4 1 8 3 5 4 4 9 5 6 6 3 7 0 λ=xxx nm 1 0 T im e [ w e e k ] 1 0 74 4 1 0 T im e [ D a y ] 7 1 0 4 6. 9 3 1. 3 1 5. 6 B r e a k i n g l o a d [ k g ]

Possible Implementation KOH KOH FS λ/10 polished ear Marionetta clamp flat strips 4 40 40mm λ/10 polished region Transportation of the payload is an (almost) easy task Hanging procedure will be very crucial (and difficult)

Virgo sensitivity with FS suspension 10-18 h [1/sqrt(Hz)] 10-19 10-0 10-1 C85 steel wire (total) Fused Silica wire (total) FS pendulum thermal noise Mirror thermal noise 10-10 -3 1 10 100 1000 Frequency [Hz]

Conclusions FS suspension can improve our sensitivity in the low frequency range up to a factor 10 Strength of FS fibers satisfy our requirements but more experience needed in: ageing of FS fibres storage conditions, handling and mounting procedures welding strength Silicate bonding is the right solution to attach the wires to the mirror, but we need to define the bonding area and ear shape A full scale test is foreseen in autumn at the Virgo site