CHEMICAL ENGINEERING DEPARTMENT Equipments and List of Experiments in each Laboratory

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CHEMICAL ENGINEERING DEPARTMENT Equipments and List of Experiments in each Laboratory Name of Laboratory: Instrumentation and Process Control (1) Equipments/instruments List of Experiments: 1 Pressure Control Trainer 2 Temperature Control Trainer 3 Level Control Trainer 4 Flow Control Trainer 5 First order liquid level 6 Linearization 7 Tank in Series [Non-Interacting] 8 Tank in Series [Interacting] 9 Simulation Software for Binary Distillation Column for benzene and toluene 10 Simulation Software for Catalytic reformer 11 Simulation Software for Heat Exchanger 12 Anemometer 1. Dynamics of First Order Liquid Level System. 2. Study of Linearization 3. Dynamics of Non Interacting Tanks. 4. Dynamics of Interacting Tanks 5. Response of Manometer system 6. Simulation of Heat Exchanger 7. Simulation of Catalytic Reformer 8. Simulation of Binary Distillation 9. Study of Temperature Control Trainer 10. Study of Pressure Control Trainer 11. Study of Flow Control Trainer 12. Study of Level Control Trainer 13. Dissolved Oxygen Meter 14. Thermocouple Calibration

Name of Laboratory: Mass Transfer Operations List of Equipments/instruments MTO-I Lab: 1 Wetted wall column 2 Experimental cooling water tower 3 Fluid bed dryer 4 Liquid-liquid extraction unit 5 Gas absorption in sieve plate column 6 Packed bed distillation column 7 Gas Chromatograph 8 UV-Visible Spectrophotometer 9 Ultrasonic Probe 1. Diffusivity (Different constituents and Different temperatures) 2. Mass Transfer Coefficient (Different flow rates) 3. Latent Heat of Vaporization 4. Crystallization (Seeding and without seeding) 5. Humidification 6. Differential Distillation 7. Azeotropic Distillation 8. Steam Distillation 9. Hydro-distillation 10. Demo: Packed Bed Distillation MTO-II Lab: 1. Ternary Diagram (Two solvents) 2. Liquid-liquid Extraction (Single/Multiple stages) 3. Freundlich Isotherm (Adsorption isotherm in case of liquid solution) 4. Adsorption in Packed Bed Column (Different amount of adsorbent/ different concentrations of adsorbate) 5. Leaching (Conventional method, Microwave-assisted extraction, Ultrasound-assisted extraction, Soxhlet extraction) 6. Fluidized Bed Drying 7. Cooling Tower 8. Gas Chromatograph/ UV-Vis Spectrophotometer 9. Demo: Pilot scale unit of Liquid-liquid Extraction 10. Demo: Pilot Scale unit of Gas Absorption 11. Demo: Pervaporation Useful link for Virtual Lab: http://iitg.vlab.co.in/?sub=58

Name of Laboratory: Heat Transfer Operations 1 Conduction through Composite Wall 2 Thermal Conductivity of Insulating Powder 3 Heat Transfer in Laminar Flow 4 Heat Transfer in Turbulent Flow 5 Forced Convection Setup 6 Natural Convection 7 Plate Heat Exchanger 8 Shell and Tube Heat Exchanger 9 Heat Transfer by Radiation: Stefan- Boltzmann Law 10 Heat Transfer in Agitated Vessel 11 Thermal Conductivity of Metal Rod 1. Experiment on Heat transfer through composite wall at different temperature 2. Experiment on Thermal conductivity of insulating powder (Asbestos powder) 3. Experiment on Heat transfer in double pipe heat exchanger in laminar flow 4. Experiment on Heat transfer in turbulent flow 5. Experiment on Heat transfer by forced convection 6. Experiment on Heat transfer coefficient in natural convection 7. Experiment on Heat transfer in Plate Heat Exchanger 8. Experiment on Shell and tube heat exchanger 9. Experiment on Heat transfer by radiation: Stefan-Boltzmann Law 10. Experiment on Heat Transfer in Agitated Vessel 11. Experiment on Thermal conductivity of metal rod

Name of the Laboratory: Chemical Reaction Engineering Name of the Equipment 1. Gas Chromatograph (Thermo Scientific) 2. UV-Vis Spectrophotometer (Thermo Scientific) 3. UV-Vis Spectrophotometer (Hach) 4. S.S. Continuous Plug Flow Reactor with Furnace 5. Ultrasonic Processer 6. Automatic Film Applicator 7. Multi Vessel Dip Coating System 8. Incubator 9. Centrifuge 10. Deep Freezer 11. Microbial Fuel Cells (MFCs) Assembly 12. Solar Distillation Unit 1) Integral method of analysis of kinetic data 2) Differential method of analysis of kinetic data 3) Determination of activation energy and frequency factor 4) Half life method of analysis of kinetic data 5) Kinetics of pseudo first order reaction 6) Reaction kinetic studies using conductivity meter 7) Reaction kinetic studies in a batch reactor (virtual lab) 8) Reaction kinetic studies in a mixed flow reactor (virtual lab) 9) Reaction kinetic studies in a plug flow reactor (virtual lab)

Name of Laboratory: General Chemical Technology List of Experiments: 1. Preparation of Boric acid by acidified solution of borax (Na 2 B 4 O 7 ). 2. Preparation of Calcium chloride from HCl and lime stone (CaCO 3 ). 3. Preparation of detergent. 4. Preparation of nitro naphthalene from given chemicals. 5. Preparation of Potash alum from Aluminum Sulphate and Potassium sulphate. 6. Estimation of saponification value of coconut oil. 7. Determination of the kinematic viscosity of given oil sample using Redwood viscometer. 8. Determination of the aniline point of diesel. 9. Determination of the smoke point of kerosene and diesel. 10. Determination of the softening point of grease sample. 11. Determination of the penetration index using penetrometer. Name of Laboratory: Fluid Flow Operations Experiment on friction in annulus Experiment on venturi meter Experiment on equivalent length of pipe fittings Experiment on viscosity by Stokes law Experiment on Reynolds number Experiment on orifice meter Experiment on characteristics of centrifugal pump Experiment on friction in circular pipe Experiment on flow through triangular weir Experiment on flow through helical coil 1 Friction in annulus and orifice meter 2 Friction in Circular Pipe apparatus 3 Stokes law apparatus 4 Equivalent length of pipe fittings 5 Flow through venturi meter 6 Helical Coil Apparatus 7 V Notch and Rectangular Notch set up 8 Characteristics of Centrifugal pump Name of Laboratory: Computer Aided Design (CAD) 26 Nos. Dell Optiplex 990 computers with following specifications: Core i5-2400 CPU @ 3.10 GHz, 4 GB RAM, 64 bit OS-Windows 7 Professional, 500 GB HDD. COMSOL Multiphysics software (for CFD) Statistica Data Miner software (for statistical analyses) Origin software (for data analysis and publication-quality graphing)

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