Product Information: COA: 20180199 Sample ID: D802027-01 Type: Concentrate/Extract Lot Number: 700mg Hemp oil Storage conditions: 4 C Customer: Sunshine Global Sample size: 15 ml 150 South Pine Island Rd, #300 Sampled by: Customer Plantation, FL 33324 Date Sampled: - License Number: - Sampling Location: - Date Accepted: 02/19/2017 Total CBD 150.14 mg THC 0.0% Microbial Pesticides Mycotoxins Total Terpenes 0.10% Residual Solvents Heavy Metals 1. Cannabinoid profile: Analysis Method: SOP.T.30.050 SOP.T.40.020 QA Testing mg/g CBDV 0.00 CBDA 0.00 CBGA 0.00 CBG 0.00 CBD 10.01 THCV 0.00 CBN 0.00 Total THC 0.00 -THC 0.00 -THCa 0.000 CBC 0.000 mg/g 12.00 10.00 8.00 6.00 4.00 2.00 0.00 www.eviolabsfl.com Page 1
2. Pesticides: Passed. Analysis Method: SOP.T.30.060, SOP.T.40.061 Pesticide ppb Pesticide ppb None detected None detected Abbreviations: ppb = Parts Per Billion 3. Residual Solvents: Passed Analysis Method: SOP.T.40.032 Analyte ppm Analyte ppm None detected Abbreviations: ppm = Parts Per Million 4. Contaminant Analysis: Passed. 4.1. Microbial Analysis Method: SOP.T.40.043 Escherichia Coli (Limit: Absent in 1g) Salmonella (Limit: Absent in 1g) Aspergillus fumigatus (Limit: Absent in 1g) Aspergillus flavus (Limit: Absent in 1g) Aspergillus niger (Limit: Absent in 1g) Aspergillus terreus (Limit: Absent in 1g) 5. Mycotoxins Analysis: Passed. Analysis Method: SOP.T.30.074, SOP.T.40.074 Aflatoxins Aflatoxins B1, B2, G1, G2 (Limit 20 µg/kg) 2.86 µg/kg Ochratoxins Ochratoxins A (Limit 20 µg/kg) 0.00 µg/kg 6. Heavy Metals: Passed. Analysis Method: SOP.T.30.052, SOP.T.40.050 Metal ppm Metal ppm Arsenic (As) 0.044 Lead (Pb) 0.336 Cadmium (Cd) 0.000 Mercury (Hg) 0.323 Abbreviations: ppm = Parts Per Million 7. Terpenes screening: Analysis Method: SOP.T.40.090 Analyte % Analyte % alpha-pinene (80-56-8) 0.01 Terpinolene (586-62-9)) 0.01 Camphene (79-92-5) 0.00 Linalool (78-70-6) 0.01 beta-myrcene (123-35-3) 0.02 (-)-Isopulegol (89-79-2) 0.00 (-)-beta-pinene (18172-67-3) 0.00 Geraniol (106-24-1) 0.00 delta-3-carene (13466-78-9) 0.00 trans-caryophellene 0.01 alpha-terpinene (99-86-5 0.00 alpha-humulene (6753-98-6) 0.00 www.eviolabsfl.com Page 2
Ocimene (13877-91-3) 0.02 cis-nerolidol 0.00 d-limonene (5989-27-5) 0.01 trans-nerolidol 0.00 Ocimene (mixture of isomers) 0.00 (-)-Guaiol (489-86-1) 0.00 1,8-Cineole (Eucalyptol) (470-82-6) 0.00 (-)-Caryophyllene oxide (1139-30-6) 0.00 gamma-terpinene (99-85-4) 0.01 (-)-alpha-bisabolol (23089-26-1) 0.00 8. Details of testing: 8.1. Cannabinoid Profile Test Results Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/l). 8.2. Pesticide Analysis Pesticide screening is performed using LC-MS (Non-Volatile Pesticides) and GC-MS (Volatile Pesticides) which can screen down to below single digit ppb concentrations for regulated pesticides. Currently we analyze for 66 pesticides. (Method: SOP.T.30.060 Sample Preparation for Pesticides Analysis via LCMSMS and GCMS, SOP.T40.060 Procedure for Pesticide Quantification Using LCMS, and SOP.T.40.061 Procedure for Volatile Pesticide Quantification Using GCMS) Pesticides Edible Products Dried Flowers All Other Processed Pesticides Edible Products Dried Flowers www.eviolabsfl.com Page 3 All Other Processed Abamectin B1a 0.02 0.02 0.02 Imazalil 0.02 0.02 0.02 Acephate 0.02 0.02 0.02 Imidacloprid 0.25 0.1 0.1 Acequinocyl 0.27 0.1 0.02 Kresoxim-methyl 0.01 0.01 0.01 Acetamiprid 0.01 0.01 0.01 Malathion 0.02 0.02 0.02 Aldicarb 0.01 0.01 0.01 Metalaxyl 3.6 0.1 0.02 Azoxystrobin 0.01 0.01 0.01 Methiocarb 0.01 0.01 0.01 Bifenazate 1.0 0.1 0.1 Methomyl 0.01 0.01 0.01 Bifenthrin 0.01 0.01 0.01 Methyl parathion 0.01 0.01 0.01 Boscalid 0.01 0.01 0.01 Myclobutanil 0.01 0.01 0.01 Carbaryl 1.0 0.7 0.05 Naled 0.01 0.01 0.01 Carbofuran 0.01 0.01 0.01 Oxamyl 0.01 0.01 0.01 Chlorantraniliprole 0.01 0.01 0.01 Paclobutrazol 0.02 0.02 0.02 Chlorfenapyr 0.02 0.02 0.02 MGK-264 0.01 0.01 0.01 Chlorpyrifos 0.01 0.01 0.01 Permethrin 0.026 0.5 0.2 Clofentezine 0.01 0.01 0.01 Phosmet 0.01 0.01 0.01 Cyfluthrin 0.02 0.02 0.02 Piperonyl butoxide 0.03 0.1 0.1 Cypermethrin 1.3 0.1 0.04 Prallethrin 2.5 0.5 0.02 Daminozide 0.01 0.01 0.01 Propiconazole 0.12 0.1 0.02 DDVP (Dichlorvos) 0.01 0.01 0.01 Propoxur 63.0 3.0 3.0 Diazinon 1.0 1.0 0.5 Pyrethrins 0.5 0.1 0.02 Dimethoate 0.01 0.01 0.01 Pyridaben 0.02 0.02 0.02 Ethoprophos 0.02 0.02 0.02 Spinosad 0.02 0.02 0.02 Etofenprox 0.01 0.01 0.01 Spiromesifen 0.7 0.5 0.5 Etoxazole 0.01 0.01 0.01 Spirotetramat 4.4 0.1 0.02 Fenoxycarb 0.01 0.01 0.01 Spiroxamine 0.5 0.1 0.04 Fenpyroximate 0.01 0.01 0.01 Tebuconazole 0.29 0.1 0.02 Fipronil 0.01 0.01 0.01 Thiacloprid 20.0 0.1 0.1 Flonicamid 0.46 0.1 0.05 Thiamethoxam 10.0 0.1 0.1 Fludioxonil 1.7 0.1 0.08 Trifloxystrobin 0.01 0.01 0.01 Hexythiazox 0.01 0.01 0.01 0.01 0.01 0.01
8.3. Residual Solvents Analysis Residual solvent screening is performed using GC-MS which can detect below single digit ppm concentrations for residual solvents. Currently we analyze for 29 residual solvents. (Method: SOP.T.40.032 Residual Solvent Analysis vis GC/MS) Residual Solvents CAS No. Action Level for Medical Goods 1,2-Dichloroethane 107-06-2 2 1,1-Dichloroethene 75-35-4 8 1,1,1-Trichloroethane 71-55-6 1500 Acetone 67-64-1 750 Acetonitrile 75-05-8 60 Benzene 71-43-2 1 Butane 106-97-8 800 Carbon Tetrachloride 56-23-5 4 Chlorobenzene 108-90-7 360 Chloroform 67-66-3 2 Cyclohexane 110-82-7 3000 Ethanol 64-17-5 1000 Ethyl acetate 141-78-6 400 Ethyl ether 60-29-7 500 Ethylene glycol 107-21-1 620 Ethylene oxide 75-21-8 5 Formamide 75-12-7 220 Heptane 142-82-5 500 Hexane 110-54-3 50 Isopropyl alcohol 67-63-0 500 Methanol 67-56-1 250 Methylene chloride 75-09-2 125 Naphtha 8030-30-6 400 Pentane 109-66-0 750 Petroleum ether 8032-32-4 400 Propane 74-98-6 200 Trichloroethylene 79-01-6 25 Toluene 108-88-3 150 Total xylenes (ortho-, meta-, para-) 1330-20-7 150 8.4. Microbial Test Results Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails the microbiological-impurity testing. 8.5. Mycotoxins Analysis Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using VICAM AflaTest and OchraTest analysis. (Method: SOP.T.30.074 for sample prep and SOP.T.40.074 for analysis, LOQ for Aflatoxins 2 ppb and for Ochratoxins 3ppb). Total Aflatoxins (Aflotoxin B1, B2, G1, G2) must be <20µg/Kg of substance. Ochratoxins must be <20µg/Kg of substance. www.eviolabsfl.com Page 4
8.6. Heavy Metals Analysis Heavy Metals screen is performed using ICP-MS (Inductively Coupled Plasma Mass Spectroscopy) which can screen down to below single digit ppb concentrations for regulated heavy metals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS and SOP.T.40.050 Heavy Metals Analysis via ICP-MS. Heavy Metal Action Lavel for Medical Edible Products, Suppositories, Sublingual Products, and other Manufactured Products (µg/g) Action Level for All Inhaled Medical Goods (µg/g) Action Level for Topical and Transdermal Medical Goods (µg/g) Cadmium 0.5 0.2 5.0 Lead 0.5 0.5 10.0 Arsenic 1.5 0.2 3.0 Mercury 3.0 0.1 1.0 8.7. Terpenes screening Terpenoid profile screen is performed using GC-MS QP-2020 with Headspace Sampler (Gas Chromatography Mass Spectroscopy) which can screen down to below single digit ppb concentrations terpenes using Method SOP.T.40.090 Terpenoid Analysis Via GC-MS. Sample lot approved by: Jorge Segredo Date: 02/21/2018 Jorge Segredo Lab Director www.eviolabsfl.com Page 5