Detoxification of wastewater containing As and Sb by hydrothermal mineralization

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1 P l Sp ETp S 2007, SETS Dx ww Sb b hhl lz Tkh k, R S, 2 Hk h 2 ETp S, N Uv, N, Jp 2 Dp ppl h, G Shl E, N Uv, N, Jp b: W h x ww x b hhl lz Th wh OH 2 w h l ww 2000 p Th w v h pp l l 5 O 4 OH 2 Sb 2 O 7, pvl llq p hhl w l h h l, h vl l pv ll p wh h h b bhp pp Th l h w 002 whh w lw h h h w Jp w p h l pll 2000 Th, h hhl lz h v h x h pll w Sb p Kw: Hhl Mlz,,, Ww NTRODUTON h p w l h p v l l hl p l h ww pl pl hl pw pl Hwv, h hv xl hh x h b h lv h pll h vl O O h h h, l wh v h hlh x, lhh ll, h h v l 4 Th, h l l Jp NESJ p w 0 h p w 002 vl ppp q ql l ww h Fh, vl pbl b pll w hv, h Blh, h 57 O h, h p Jp, h h xp b l Th, h blh h vl l ww lbl Svl hq v q hv b vlp, xpl, b p, ll 8, b p 9 bll h 0 Epll, h p h hx zvl hv b vl v Hwv, h hv h llw pbl Rvl l lw, pll O 2 Th pplbl w q b, bh h b ll b ppl hz w Th h pbl h l pp wh lw lbl w b hh bl x q Sll, h v hq v p q, b h l pp Th, h xp vlp w hq v p bl l pp q l, x p p h hh lbl w, ql l l, xpl, l Pb, 2 Sb 2 O 7 hl O OH H 2 O Jhb 5 O 4 OH Th h h bl p lbl Sbb l W p h pv h b l b v q l b, l lb b l h lbl l hhl, ll hhl lz hq 46 h p, w v h v hq l ww O, V SbVO 4 b hhl lz 2 EXPERMENTL DETLS Hhl Ml ww wh 2000 w pp b lv 2 O, 2 O 5 05 N NOH l, lz b Hl ll z w Wk P hl, L Ml ww 80 SbO 4 w pp b lv Sb 2 O 5 h ll z w Th l ww 0 L w l p vl l wh lb h wh lz p h: H K, 902

2 P l Sp ETp S 2007, SETS OH 2, v, wh H 2 O 2 xz Hhl w b lv h vl v 296 h v p h 0020 Th p h vl w ll ll,, p h vp p w h p Th, w kp h 05 MP 50 0 MP 20 h hhl, h vl w l w ph h Pp b b h hhl w l ll Hhl lz b h plp pp, whh hw F, w h,, pv l h l pp hhl D h hhl, h v p l h pl b b w vp p, h pp p p b 05 µ l l h, h pl w l l w p b l ll l h hhl b plh b h p plp pp Spk l H P vl Fl 05 µ Spl b S b F Sh plp hhl lv l Th pp w b X XRD: RGKU R2500 Kα Th l bv qlv l l h pp w p b l p SEM: JEOL JSMT20 qpp wh pv X p EDS: JED240 Th l h pp w b hv l hl lz TGDT: RGKU Th pl, TG820 Qv l h h lv b h hhl w b h lb bl h h l h lv, x b hhl lv wh HNO 02 L0 L w w h Th l w l b PMS RESRLTS ND DSUSSON Hhl lz ww wh OH 2 lz T p h h l ww : wh OH 2 hw F Th l b OH 2 lz h l ww, w w 4 v b h hhl lz Th h l p b l Hwv, h NESJ 0 B p h hhl lz h l ww wh OH 2, w v v,, pp x Th l h b b h p h h pl, h w 04, whh h b h hhl, b ll hh h h NESJ T T h F 2 Dp h h w h Ⅲ: 2000, 00 OH 2 w : 06, : 08 F hw h XRD p h pp b h 00 Ubl pk w bv h p b h h wh h pk OH 2 h l XPS, TGDT SEMEDS l, h hl l h bl p w 5 O OH 4H 2 O Sh hw pbl h hhl lz Th 5 O OH 4H 2 O wl b plh b h Sh Slbl h p lvl lw, b h b h l b OH F 4 hw h XRD p h pp b h 200 Eh pp F 4 w pp h llw F 4: h pp b h F 4b: 5 O OH 90

3 P l Sp ETp S 2007, SETS b Kα 2θ F 4 XRD p h pp : b h 5 O OH 4H 2 O, b: 5 O OH, : 5 O 4 OH, : 200 wh 08 OH 2 8 h : Kα 2θ F XRD p h pp b b h 00 wh 08 OH 2 Ⅲ: 2000, : b h, b: 4 h, : 2 h, : 6 h, : OH 2 Oh pk w bl b pp b h h pp b h h l l w F 4: p 5 V O 4 OH b hhl lz V O 4 wh OH 2 lz h F 4: Pp h hhl h l ww O h Th l h h pp h x 5 O OH 5 V O 4 OH Th, l w 5 O OH 4H 2 O wl b v h hhl lz Sh h, h pp w xz 5 O 4 OH XPS p h pp b h p 200 hw h x b G l b GTD h h xz w H 2 O, b h w Th, h x w plh b h bw O H 2 O hw Sh j h, h 5 V O 4 OH wl b h bw O 4 pp OH 2 Sh k ll, h lbl 5 O OH 4H 2 O 5 O OH w, whh w b pl lbl, w H 2 O H 2 O, pvl Th, h v F wl b b h vl l w 5 O OH 4H 2 O h 5 O OH, whh h hh lbl w wh Th l l h h lbl h pp h 5 O OH 4H 2 O hv v lbl v h p, h lbl 5 V O 4 OH w l h h w v lw p wh h bv vl p xp, h, h l x 5 O 4 OH wl b v pp p OH 2 + H 2 O 2 O 2 + 2H 2 O b 2O 2 + 2H 2 O 2OH 2 + O 2 2 H 2 O 2 2 H 2 O + O 2 O + H 2 O OH 2 O + 5 OH H 2 O 5 O OH 4 H 2 O + 9OH 5 O OH 4 H 2 O 5 O OH + 4 H 2 O h O + O 2 O 4 + O O + H 2 O 2 O 4 + H 2 O j O + H 2 O O 4 + H 2 k O 4 + 5OH 2 5 O 4 OH + 9OH Sh Pbl h hhl lz L T h F 5 Dp wh 08 OH 2 % H 2 O 2 Ⅲ : 2000 : 00, : 50 E H 2 O 2 904

4 P l Sp ETp S 2007, SETS Th H 2 O 2 x pp 5 V O 4 OH w x F 5 hw h p h hhl 06 h wh h 08 OH 2 % H 2 O 2 b h l b OH 2 H 2 O 2 w ppxl 50 whh w hh h h h wh OH 2 l D b h hw F w v h 5 O OH 4H 2 O Th H 2 O 2 hb h 5 O OH 4H 2 O O 2 O h h h, l 05 h p 2 h F 6 hw h XRD p h pp h bv hhl D pk O 2 bv h 0 h 8 h h h pk OH 2 pp wh h O 2 pk Th l hw h h x OH 2 h b Sh, whh ll wh H 2 O OH 2 Shb Hh vl b h p wh h H 2 O 2 F wl b b p 5 O OH 4H 2 O Sh O 2 O h h h, l h pk 5 V O 4 OH w bv h hhl Th, h vl h p b h l x V b H 2 O 2 O 2, 5 O 4 OH Shh,, j, k Hwv, v v ll bv F 5 h h NESJ l b v Ox wl b, b ll x l h w b l l hh hw h Kα 2θ F 6 XRD p h pp b b hhl lz wh 08 OH 2 % H 2 O 2 00, : b h, b: 4 h, : 8 h, : 6 h : OH 2, : 5 O 4 OH, : O 2 b 200 L T T h F 7 Dp h h w h wh 08 OH 2 5 % H 2 O 2 Ⅲ: 2000 : 00, : 50 F 7 hw l v v 5% H 2 O , whh h l x h w Hwv, h w l h h vl NESJ, 0 h p 5% H 2 O h Th l hw h h x 2000 h 5 V O 4 OH w l pl b h hhl wh H 2 O 2 Obvl, h p H 2 O 2 p h l, whh l 5% H 2 O 2 h xz 2000 Th l h h hhl lz v v v v vl p h Th, l h h hhl lz v hq h v b ww 2 Hhl lz ww b plp pp Tp Splp Bh p T h l v h p T F 8 Dp h h 50 b : bh p pp : plp pp O 4 : 2000, : Tp vl h 905

5 P l Sp ETp S 2007, SETS Hhl lz b h plp pp F w h l ww 2000 V O 4 pv l h l l p h F 8 hw h l hhl lz b bh p plp pp h h l pp h w 006 Th l hw h h p l h pp hhl bl l pv l v, b l h pl Sh h pl b l wh l Th l h l wl b b ll l Th l xp bh p hhl pp F, whh ll plh b l wh 5 O 4 OH L l z lw l 5 O 4 OH pp h l p Hwv, wh h l p pp hhl, l wh h w, b h pll pv l h l l l wh Th, h pl w h b h plp hhl pp Hhl lz Sb ww F 9 hw h p Sb h w 5020 wh OH 2 lz Sb l b OH 2, b h hhl Hwv, ll b ppl h hhl lz Rl Sb w wh p, w h wh 0 OH 2 Th, h hhl lz l v Sb q F 0 hw h XRD p h pp b b h wh 005 OH h Th pp b h w 2 Sb 2 O 7, whh h h l l Ml Pb, 2 Sb 2 O 7 Th v 2 Sb 2 O 7 wl b l b h vl p lhh l Sb v ll b h h OH 2 h 00, w ll 2+ l p l h lbl OH 2 w v hhl, v wh h OH 2 Hwv, h wh 005 OH 2 hw lw v Sb F 9b Th lw v pbl h h OH 2 pp Rl SEMEDS l hw h h 2 Sb 2 O 7 w l h b S b S b S T Th T Th T Th F 9 Dp Sb h wh ; 005, ; 0, ; 02, ; 0 OH 2 lz ; 50, b; 200, ; 20 ; pl l w b w 5 hxl OH 2 Th, xp h 2 Sb 2 O 7 wl b b h SbO wh hxl p h OH 2 pp Th h l h hhl lz q b pv l v Sb wl b b h OH 2 pp h 2 Sb 2 O 7 Fh, l Sb wh p l w h vl F 9b whh lw h h Sb wh 0 OH 2 20 Th l h h lbl 2 Sb 2 O 7 hhl lw h h p p h, bh p p vl w l w p h h D h p, l 2 Sb 2 O 7 wl Sb O h h h, p b 906

6 P l Sp ETp S 2007, SETS Kα 2θ F 0 XRD p h pp b b hhl h wh 005 OH 2 : 2 Sb 2 O 7, : OH 2 l h vl pv h l 2 Sb 2 O 7 h l p pll 0 D Sb w hv hh h p lv h pp b lv l 2 Sb 2 O 7 w Th l h Sb h h b bhp wl b hh h h b h plp hhl Th, h p l h pp hhl wl pv h v v Sb b hhl lz 4 ONLUSONS W hv h pp v, b hhl lz hq, whh h l h lbl l h Eh Sl x lz b OH 2 lz H 2 O 2 xz w v h pp jhb wh hh l Th hhl lz h l ww, whh 2000, p l lw h h NESJ, 0 Th p q l pp hhl l pll pv l h l bl x ww v wh hh O h h h, h hhl lz wh OH 2 l pp q Th v l w 2 Sb 2 O 7, whh h l Ml Th, h pp wl b pbl b p h p h l p Rp l hw h h lbl 2 Sb 2 O 7 hhl w lw h h p p xp h h p l pp hhl bl h pv l v Sb Th, w l h h hhl lz v hq pp v, ww v w REFERENES M B F H Fl, Hh E Hbl,,, 200, pp 98 2 M B F H Fl, Hh E Hbl,, 2, 200, pp 9707 P L Sl D G Kbh, ppl Gh, 7, 5, 2002, pp N Khl, S h, Th J h, ppl R, 52,, 2000, pp 8 5 J k, K z, H Fkh, H M, S Nk, T Yh, H Ohj, H M w K k, ppl Gh, 9, 2, 2004, pp M H, M K Sp, S h, M M Rh, D Ml, D Lh, B D, B Nk, B K R, Mkhj D hkb, Ev S Thl, 9,, 2005, pp J R P, D L k, J L Vlzl, J G, M Kz, G w, H M M W, J Hz M, 24,, 2005, pp P R K, S hh, K Khl S P Mhj, hph, 55, 9, 2004, pp Y S, M K, T K Y M, W Rh, 6,, 2002, pp K Zbl, W Rh, 8,, 2004, pp 726 S B, M D Jh, G P K X G M, W Rh, 9, 5, 2005, pp O X Lp S J H, W Rh, 9, 9, 2005, pp M L P B M, W Rh, 6, 7, 982, pp T k, R S H h, W Rh, 9, 2, 2005, pp T k, R S H h, Bll h hl S Jp, 79, 8, 2006, pp D M Sh S R Rll, Gh E h, 67, 22, 200, pp

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