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1 ROA-RI6 699 A SIMS STUDY OF THE INFLUENE OF LOW LEVELS OF SILION vi 1) R, AND ALIUN ON THE.. (U) TEXAS UNIY AT AUSTIN DEPT OF I HEMISTRY S AKHTER ET AL. 15 OT 85 TR-43 UNLASSIFIED N K-1582 F/G 7/4 NL 'SEOONERhhh I flllf m f

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3 I.5. OFFIE OF NAVAL RESEARH ontract No. N14-83-K-582 *Task No. NR TEHNIAL REPORT NO. 43 A SIMS Study of the Influence of Low Levels of Silicon and alcium * I on the Adsorption Properties of 2 on Pt(lll) S. Akhter,. M. Greenlief, H.-W. hen and J. M. White by Prepared for publication in Applied Surface Science Department of hemistry DTI e ELE OT %51 The University of Texas at Austin " Austin, Texas B Reproduction in whole or in part is permitted for any purpose of the United States Government. This document has been approved for public release and sale; its distribution is unlimited..j &J "." -* ". ". Q ","." q ". " - ' ".".". ". ". " ".,-. ',. -.,.., ' " " -.o. " '.' ''' " - " "":. "......

4 SEURITY LASSIFIATION OF THIS PAGE (When Data Entered) REPORT DOUMENTATION PAGE ROTBEFORE READ INSTRU7IONS OMPLETING FORM 1. REPORT NUMBER 12qO SO cyent's ATALOG NUMBER, 4. TITLE (end Subtitle) S. TVP1 OF REPORT & PEmOO OVERED Technical Report 43 A SIMS. Study of the Influence of Low Levels of January 1 - December 31, 1985 Silicon and alcium on the Adsorption Properties 6. PERFORMING ORG. REPORT NUMBER of 2 on Pt(111) 7. AUTNOR(@) s. ONTRAT OR GRANT NUBEa) S. Akhter,. M. Greenlief, H.-W. hen and J. M. White NO14-83-K PERFORMING ORGANIZATION NAME AND ADDRESS 1. PROGRAM ELEMENT. PROJET. TASK J. M. White, Department of hemistry AREA* WORK UNIT NUMBERS University of Texas Project No. NR Austin, TX ONTROLLING OFFIE NAME AND ADDRESS I". REPORT DATE Department of the Navy October 15, 1985 Office of Naval Research 13. NUMBEROF PAGES Arlin2ton. VA MONITORING AGENY NAME & ADORESS(If different from ontrolling Olfle) IS. SEURITY LASS. (.t tal report) 1S. DELASSIFIATION/DOWNGRADING SHEDULE 16. DISTRIBUTION STATEMENT (of tale SRoert) * Approved for public release; distribution unlimited. 17. DISTRIBUTION STATEMENT (of the abstract entered In Block I. different E,. Report) II. SUPPLEMENTA.Y NOTES Preprint: Appl. Surface. Sci. (in press) 13. KEY WOROS (ontinue on reere de It necessary and idendti by block ftombar) b. ABSTRAT (ontinue on rvoerae aide If neceeory and IdentIy by block number) -Surface impurity levels of a, Si and Al at or below the detectability limits of AES were followed in SIMS and correlated with oxygen adsorptiou u P (i1). il shown that oxidation of Si to SiOx, monitored by the rise in SIMS Si ion intensity, takes place above 5K during oxygen TPD. iox starts decomposing above 11K and can be reduced within 2 sec by 2xl torr of H 2 at 12K. The. 2 adsorbed/desorbed in a TPD cycle depends on the immediate history of the impur levels on the surface. SiOx presence correlates with an increase in the overall oxygen sticking coefficient. These results highlight the importance of impurity levels below AES detectability and suggest pretreatment methods for obtaining better reproducibility. 4. DD D I,JN, EDITION EY. Of NOV 6S IS OBSOLETE S/N 12-1'4-661 I SEURITY L.ASSIFIATION OF THIS PAGE (When Date Entered)

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