J. Am. Chem. Soc., 1996, 118(9), , DOI: /ja953497z
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1 J. Am. Chem. Soc., 1996, 118(9), , DOI:1.121/ja953497z Terms & Conditions Electronic Supporting Information files are available without a subscription to ACS Web Editions. The American Chemical Society holds a copyright ownership interest in any copyrightable Supporting Information. Files available from the ACS website may be downloaded for personal use only. Users are not otherwise permitted to reproduce, republish, redistribute, or sell any Supporting Information from the ACS website, either in whole or in part, in either machinereadable form or any other form without permission from the American Chemical Society. For permission to reproduce, republish and redistribute this material, requesters must process their own requests via the RightsLink permission system. Information about how to use the RightsLink permission system can be found at Copyright 1996 American Chemical Society
2 H NMIR (C. 3 MHz) CHC? I I I I I i I I-J l Ppm
3 CH CE I I I I I I I I 7 6 ili p I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I PPM il/ Tm8
4 Tfg-fPRINT DOCUMENT ' TMS Ph 'HNMR Cl 3, 3 MHz 'I I - HCQ 3 r~~~~ w D *wm I I I I I I I I I I I I I I I I I I j p p j i 17.: I I I...~ 3 2 I, *i**'* y1.2 ± I C- ru LJ I I I I' PPt4 & ~ PPM
5 TGifT PRINT DOCUMENT H 'H NMR (Cs, 3 MHz) I- a., Et - II I I I I I I I I I I I I I I I I I I I I I ,,,,I3 4 3 Il I i ui I I I j I 11 iii 2 1 PPM
6 H CO 2 Et LIGHT PRINT DOCUm,'--4T C 'H NMR (ODd MHz) fzf -~ cc -7W 1 ~1fJ 7' 6~ 51 4 p 1
7 LIGHT PRINT DUiv1.N[ H NMR Cl 3, 3 MHz O ckcc m F-1e 7 I I a l"wal' PPM C.-
8 UGHT PRINT DOCUMNT N H TMSK\ 1 H NMR (Cis 3 MHz) cc g liiii~ii I I 1-7-T 1 I A -- T--l DPI I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I b * I '~jj 9-) I j P~
9 H O 1 H NMR (Cls, 3 MHz) CHC3 I I I I l I I I I I I 4 I r -r PPm
10 H CO 2 Et Z Me 3 Si> OH H NMR (C1 3, 3 MHz) O -OfO Tmg ' -99 I I I I I r I I i li I l 7 i l III I I si I OPPM
11 LIGHT PRINT DOCUMENT 1H NMR (C 3. 3 MHz) r I Ii I Ijil ii jill II A I ~I.4 I 3 III I II 2 PPM Q9
12 LIGHT PRINT DOCUUii IH NMR (coc 3, 3 MHz) c)c=cct et e/e ( 6~ -- ti L,~J. S 7.5 4,i I I I I I I opn L.3
13 1H NMR (Ci. 3 MHz) cc It E4oAc. I I li I l l 9 I II R i A -I I lil i a i s i l s 1 1 l a u PPM
14 1 H NMR (Ci 3, 3 MHz) P-ME. 3 q~) PPM
15 LIGHT PRINT DOCUMENt ' -e z C ick -e i 1 I I I I.... I a I I I I I r I I I I ppm
16 LIGHT PRINT DOGUMWNT h.' 1 H NMR (Ci 3, 3 MHz) ) I. CHCE, I I Ii II ii I I I I I I I I I I I I I I i II I I I I I I I I I I lrt I i 9 III III a PPM L.
17 E4oho CH CE 3. 8 / 6 5 I ~~ I3 -T - -r - r I PPM 9-
18 'H NMR (Cis, 3 MHz) ZD It ZD CL PP II
19 IH-1T PRINT DOCUMENT HO TMS Ph 1 H NMR (Cis. 3 MHz) I I ri I- I III I I F A I I I I I I I I I I I I I I K~ ~OPPt4 Q-) L PPM r-
20 LIGHT PRINT DOCUMENT HO Me TMS Ph 'H NMR (Ci 3, 3 MHz) / P17 -e Tx - ' FiEz t " I " " "I 6,5 3 2 Ppm l-
21 1 HT PRINT DOCUMENI C atc-4 4PPM., I 2.. I43. L.J
22 * ' - LIGHT PRINT DCCUMW; LIQ111 uu 'H NMR CI 3, 3 MHz Ci) -e z CJRC* -e ,. a OPpI4
23 IrHT PRINT DOCUMLNT 'HNMR Ph Cl 3, 3 MHz ' I,- I I I I I I I I I I I PPM. I -. 4,--I- *~ I i..s u.o 148. L.Z C-
24 LIGHT PRINT DOCUvik.Nf O 'HNMR I Cl 3, 3 MHz C C cc I-lrT7T Ic~g I a 7 6 s lr1i - I 2 Ipp -4 i 5 1. ;. - ok v.
25 LMHT-4 PRINT DOCUMENT ' ' -e z c~&ca 3 lii II I ii I Ii I II, I I ; 7 34 I I I I t - I I ~ I I I I I I I I I I I I a I 3 -~ 2 IPPN -e '1.~ -~ -.~-.'-
26 LIGHT PRINT cocumnie /CO 2 Et N OH Z ZD O 'HNMR Cl 3, 3 MHz cc O It cc uco O O) I.1*~ 8 il l i l l 6 i I I I I S I 5 4 j I I I I j I 3 2 1Pf~ a d n e e s s r I i l f i l i i l l j a3 I ass C- si I 9
27 pot o HO Ph i4~~ I"' Ph IH NMR CI 3 MHz (4) (b) () P7 LI? -e I I liii II 9,,.... I.... B 7 ~.3 6 I1 1 1 A I I I I I I I I I I l j I l I I I ji I I I I I I I I I I I I I I II I I I f Ij PPM C 6. l17
28 1 1W-HT Pnl,',T DOCU-WEN. 'H NMR C1 3, 3 MI-z L- T I j1hi1~ liij liii liii I I I liii liii lilililililli III Iii 1 9a I 6 5 I 4. ;.- j. 3.7av I I I I
29 I IGHT PlINT DOUMENLI'l O. 'H NMR Cl 3, 3 MHz -e 5 CVA M3 -e cc 1 I i I ~ I I I I I I I I I I I 9 liii I I l I l l li i li i 2 1 PPM t...a
30 LIGHT PRINT DOCUMENY O TMS & 'H NMR Cl 3, 3 MHz cc o r r ' /ccc 1111 I~ I ii1111 II III 1111 a pll II l~ ii ciii lii I I I 1 I QPpm L t T-
31 I-IC-HT Pr!!\'T DOCUJMPHIE 'H NMR C1 3, 3 MHz PPH C..1I.5 :4.:~~~~ li i. PPM
32 LIGHT PRINT DOCUMENT O 'H NMR Cl 3, 3 MHz o cc F cc O) Oe I3i2s i a ( P
33 IY!HT PRINT DOCUMLNT O 'HNMR Cl 3, 3 MHz 21i cc KcS 8.3 ** rl OPN? 21.7
34 O ' rtlght PYNT DOCUM[ENT TMS H NMR C1 3, 3 MHz w F.. I j~i~j I II i l i til I i 44 -J I S I I l I I I I I ii.1.1 l Il I ji I I II ljilli Ilij I l l'' J- 1 1 PM 123.1
35 LIGH-T PRINT DOCIUMIWF' TMS TBSO C 2 -i-pr 'H NMR CI 3, 3 MHz (Suw-ktf,-) cc It *j j 2 L~3 / ii) I Ii ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ -- TrrrTi I I lii I I I I I I II Ij I I II I itli i I III I I I I I I I I I I I I I I i. I I m IeY, --QQs
36 LIGHT PRINT DOCUMENT --- e 7. / -J 6.( / I : ;j~ii -~ ~JLJ - ma / I (-. ( ~ II cc O. O) AI~O /. ~Jr' da. I I I I I I I I I I I Ii Ia I l I (A) ril ( ( (b) 6 I 5 4 I 3 I N' I'J A -4.6 :68. Oe O) C>TtC
37 LIGHT PRINT DOCUMENT o Tus 'HNMR Cl 3, 3 MHz OO "I nly ll 11 *i I a p OPP a
38 cc 14 C atc I ll i i I li t i g l i i AL st lii lalissil estpal III I I I lilil...-ral-. fli- I ~ a I I a l T T PPM
39 LIGHT PRINT DOCUMENT TMS Ph )o 'H NMR Cl 3, 3 MHz / I i1 IIIII i I IIIIII 9 8 hal I I i I1II11III116I1 II VI U1 F FT-r-ryTFrr- rrri I I k a ?
40 LIGHT PRINT DOCUMEPLNil- TMS OH H NMR Cl 3, 3 MHz JL c1c~5 1' 1f I l~lilli li I II l it I I II li s1 1 ti ll I & li e : A I. PPM LoJ
41 LIGHT PRINT DOCUMENT cc cc ) C ck4ct3 V -ati I 9g Ijilil jilt Bill LII [I1117IT I I I I a i a I I I I I I I I I I II I I I I I I I I I I A I I I I I. I I I I I I I I I I I I I I - I 1 ' l i l l I I I I 1 7,3 a.? ~ M 22.1 T7.- l/- a O/- O
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J. Med. Chem., 1997, 40(14), , DOI: /jm970199z
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