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1 Supporting Information for Multilayer Hollow Spheres: Microwave-Assisted Metal-Organic-Framework Derivation and Highly Reversible Structure-Matched Stepwise Lithium Storage Wenxiang Guo, Weiwei Sun and Yong Wang* Department of Chemical Engineering, School of Environmental and Chemical Engineering, Shanghai University, Shangda Road 99, Shanghai, P. R. China,
2 Figure S1. XRD patterns of Cu-Ni-BTC and Ni-BTC. 2
3 Figure S2. Thermogravimetric curve of Cu-Ni-BTC in air. 3
4 Figure S3. Nitrogen adsorption isotherms of 4
5 Figure S4. (a-b) TEM images of the Cu-Ni-BTC MOF precursor. 5
6 Figure S5. SEM images of the CuO/NiO product synthesized by one-pot method, in which Ni(NO 3 ) 2 6H 2 O, Cu(NO 3 ) 2 3H 2 O and H 3 BTC are reacted under one-time microwave irradiation. 6
7 Figure S6. SEM images of (a) 120 (prepared at 120 o C) and (b) CuO@NiO 180 (prepared at 180 o C). (c)xrd patterns of various CuO@NiO composites. 7
8 Table S1 Electrochemical properties of multi-layer hollow of this work and previous NiO and CuO structures. These selected references represent the state-of-the-art properties of NiO/CuO nanostructures, therefore the outstanding electrochemical performances of the product in this work can be clearly demonstrated. Morphology Multilayer hollow sphere CuO sphere-nio nanosheet Electrochemical performances (charge capacity refers to lithium extraction capacity) Initial charge capacity of 856 mah g -1 and the retained capacity of 1086 mah g -1 after 200 cycles at 100 ma g -1. Initial charge capacity of 639 mah g -1, which decreases to 563 mah g -1 after 50 cycles at 80 ma g -1. References this work 1 Porous hexagonal Initial charge capacities of ~790 and 849 mah g -1 for CuO-NiO and CNT/CuO-NiO Hollow NiO microsphere Hollow NiO nanosphere Hollow NiO nanotube Mesoporous NiO nanosphere Urchin-like NiO microsphere Nanosheet-based NiO microsphere NiO nanoparticle NiO fiber CuO-NiO and CNT-supported composite, which decreases to ~320 and 566 mah g -1 after 50 cycles at 100 ma g -1. Initial charge capacity of 975 mah g -1, which decreases to 380 mah g -1 after 30 cycles at 200 ma g -1. Initial charge capacity of 889 mah g -1, which decreases to 393 mah g -1 after 50 cycles at ~215 ma g -1. Initial charge capacity of 620 mah g -1, which can be remained at 600 mah g -1 after 100 cycles at 200 ma g -1. Initial charge capacity of ~860 mah g -1, which decreases to ~447 mah g -1 after 80 cycles at 100 ma g -1. Initial charge capacity of ~600 mah g -1, which increases to ~650 mah g -1 after 50 cycles at 72 ma g -1. Initial charge capacity of ~1180 mah g -1, which decreases to nearly 0 mah g -1 after 30 cycles at 50 ma g -1. Initial charge capacity of 847 mah g -1, which decreases to ~600 mah g -1 after 50 cycles at 717 ma g -1. Initial charge capacity of 696 mah g -1, which can be retained at 638 mah g -1 after 50 cycles at 40 ma g
9 NiO nanofiber NiO nanorod array NiO nanocone array NiO nanoflake Mesoporous NiO nanosheet network 3D flower-like NiO CuO/Cu 2 O hollow polyhedron Hollow CuO octahedra Initial charge capacity of ~784 mah g -1, which decreases to ~550 mah g -1 after 100 cycles at 80 ma g -1. Initial charge capacity of 802 mah g -1, which decreases to 706 mah g -1 after 70 cycles at 1000 ma g -1. Initial charge capacity of 780 mah g -1, which increases to 1058 mah g -1 after 100 cycles at 144 ma g -1. Initial charge capacity of ~720 mah g -1, which can be maintained after 20 cycles at 100 ma g -1. Initial charge capacity of ~689 mah g -1, which increases to ~1000 mah g -1 after 80 cycles at 144 ma g -1. Initial charge capacity of 1186 mah g -1, which decreases to 713 mah g -1 after 40 cycles at 100 ma g -1. Initial charge capacity of 513 mah g -1, which increases to ~740 mah g -1 after 250 cycles at 100 ma g -1. Initial charge capacity of ~480 mah g -1, which can be retained at ~470 mah g -1 after 100 cycles at 100 ma g Initial charge capacity of 614 mah g -1 for hollow cube, Hollow Cu 2 O cube and uichin CuO nanorod Porous CuO nanorod CuO nanowire CuO Nanofiber which decreases to 79 mah g -1 after 50 cycles at 150 ma g -1. Initial charge capacity of ~500 mah g -1 for hollow urchin, which increases to 560 mah g -1 after 50 cycles at 150 ma g -1. Initial charge capacity of 580 mah g -1, which increases to 650 mah g -1 after 100 cycles at 337 ma g -1. Initial charge capacity of ~550 mah g -1, which increases to ~634 mah g -1 after 200 cycles at 337 ma g -1. Initial charge capacity of 867 mah g -1, which decreases to 581 mah g -1 after 50 cycles at 100 ma g -1. Initial charge capacity of 452 mah g -1, which can be retained at ~400 mah g -1 after 100 cycles at 100 ma g
10 Pine-needle-like CuO array Mesoporous CuO nanosheet CuO nanoflower Dandelion-like CuO Bundle-like CuO CuO nanowalnut Initial charge capacity of ~630 mah g -1, which can be retained as 626 mah g -1 after 100 cycles at 674 ma g -1. Initial charge capacity of 533 mah g -1, which increases to 640 mah g -1 after 100 cycles at 674 ma g -1. Initial charge capacity of ~620 mah g -1, which can be retained at 530 mah g -1 after 50 cycles at 16.7 ma g -1. Initial charge capacity of 576 mah g -1, which decreases to 400 mah g -1 after 50 cycles at 67 ma g -1. Initial charge capacity of ~750 mah g -1, which decreases to 666 mah g -1 after 70 cycles at 180 ma g -1. Initial charge capacity of ~600 mah g -1, which decreases to ~420 mah g -1 after 30 cycles at 67 ma g References 1. Chen, H.; Li, C. L.; Li, N.; Xiang, X. K.; Hu, Z. L. Facile Synthesis of CuO-NiO Nanocomposites with High Surface Areas and Their Application for Lithium-Ion Batteries. Micro Nano Lett. 2013, 8, Abbas, S. M.; Hussain, S. T.; Ali, S.; Ahmad, N.; Ali, N.; Abbas, S.; Ali, Z. Modification of Carbon Nanotubes by CuO-Doped NiO Nanocomposite for Use as An Anode Material for Lithium-Ion Batteries. J. Solid State Chem. 2013, 202, Xie, D.; Yuan, W. W.; Dong, Z. M.; Su, Q. M.; Zhang, J.; Du, G. H. Facile Synthesis of Porous NiO Hollow Microspheres and Its Electrochemical Lithium-Storage Performance. Electrochim. Acta 2013, 92, Sasidharan, M.; Gunawardhana, N.; Senthil, C.; Yoshio, M. Micelle Templated NiO Hollow Nanospheres as Anode Materials in Lithium Ion Batteries. J. Mater. Chem. A 2014, 2, Liu, L. X.; Guo, Y. Y.; Wang, Y. P.; Yang, X. J.; Wang, S. X.; Guo, H. Hollow NiO Nanotubes Synthesized by Bio-Templates as The High Performance Anode Materials of Lithium-Ion Batteries. Electrochim. Acta 2013, 114, Zhang, G. H.; Chen, Y. J.; Qu, B. H.; Hu, L. L.; Mei, L.; Lei, D. N.; Li, Q.; Chen, L. B.; Li, Q. H.; Wang, T. H. Synthesis of Mesoporous NiO Nanospheres as Anode Materials for Lithium Ion Batteries. Electrochim. Acta 2012, 80, Zhang, C. M.; Chen, J.; Zeng, Y.; Rui, X. H.; Zhu, J. X.; Zhang, W. Y.; Xu, C.; Lim, T. M.; Hng, H. H.; Yan, Q. Y. A Facile Approach toward Transition Metal Oxide Hierarchical Structures and Their Lithium Storage Properties. Nanoscale 2012, 4,
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