S1: The. in wet. materials. S2: The. exothermic. materials
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1 Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2014 Supporting Information S1: The corrected mass loss at 400 C (Δm 400 C ) is plotted against the adsorbed VOC in wet impregnation experiments. The compounds are listed in order of increasing boiling point. All tested materials (except CeO 2 ) were milled in waterr and calcined (1 h/500 CC in air) prior to testing. S2: The exothermic peaks in DTA analysis (T exo ) is plotted against the adsorbed VOC in wet impregnation experiments. The compounds are listed in order of increasing boiling point. All tested materials (except CeO 2 ) were milled in waterr and calcined (1 h/500 CC in air). 1
2 S3: Relative mass loss (top left) ) and differential thermo analysis signal (bottomm left) of diethylether adsorption on five different support materials. Ion current of reaction products (m/ m/z = 18, 44, 2 and 31) evolving during sample heating (right( block).. All data were collected simultaneously. 2
3 S4: Relative mass loss (top left) and differential thermo analysis signal (bottom left) off linalool adsorption on used support materials. Ion current of reaction products (m/z = 18, 44, 2 and 41) evolving during sample heating (right( block).. All data were collected simultaneously. 3
4 S5: Relative mass loss (top left) and differential thermo analysiss signal (topp right) of limonene adsorption on used support materials. Ion current of reaction products (m/z = 18, 44, 2 and 68) evolving during sample heating (right( block).. All data were collected simultaneously. 4
5 S6: Relative mass loss (top left) and differential thermo analysis signal (bottom left) of hexanoic acid adsorption on used support materials. Ion current of reaction products (m/z = 18, 44, 2 and 60) evolving during sample heating (right( block).. All data were collected simultaneously. 5
6 S7: Relative mass loss (left) and differential thermo analysis signal ( right) of triethylamine adsorption on used support materials. Ion current of reaction products (m/z = 18, 44, 2 andd 58) evolving during sample heating (right block). All data were collected simultaneously. 6
7 S8: Relative mass loss (left) and differentiall thermo analysis signal (right) of blanks of five different support materials. S Table 1 Relative mass loss at 400 C wet impregnation (raw data) Blank Diethylether Linalool Limonene Hexanoic acid Triethylamine - Δm total [%] 400 C CeO CeO 2 /H-ZSM H-ZSM CeO 2 /13X calc X calc
8 S9: Left Relative mass loss of wet impregnated adsorber materials with different compounds dissolvedd in diethylether. Right: Exothermic event temperature off adsorbates on different support materials from exothermic peak (DTA) was taken as an indicatorr for reaction. Additionally CO 2 evolution is plotted. Contributions originating from dietylether (solvent)( in samples containing linalool, limonene, hexanoic acid and triethylamine were neglected. 8
9 S Table 2 Wet impregnation adsorption data - Δm total [%] 400 C a T exo [ C] Diethylether CeO CeO 2 /H-ZSM-5calc H-ZSM-5calc CeO 2 /13X calc X calc Triethylamine CeO CeO 2 /H-ZSM-5calc /380 H-ZSM-5calc CeO 2 /13X calc X calc Limonene CeO CeO 2 /H-ZSM-5calc H-ZSM-5calc CeO 2 /13X calc X calc Linalool CeO CeO 2 /H-ZSM-5calc H-ZSM-5calc CeO 2 /13X calc X calc Hexanoic acid CeO CeO 2 /H-ZSM-5calc H-ZSM-5calc CeO 2 /13X calc X calc a blank and diethylether subtracted 9
10 S Table 3 Gas phase adsorption data - Δm total [%] 400 C a T exo [ C] Limonene CeO CeO 2 /H-ZSM-5calc H-ZSM-5calc CeO 2 /13X calc X calc Linalool CeO CeO 2 /H-ZSM-5calc H-ZSM-5calc CeO 2 /13X calc /255 13X calc Triethylamine CeO /230 CeO 2 /H-ZSM-5calc /240 H-ZSM-5calc CeO 2 /13X calc X calc /340 a blank subtracted 10
11 S10: STEM micrographs of CeO 2 /H-ZSM-5 (a) and H-ZSM-5 (b) after milling and calcination. EDX mapping region (c) and elemental analysis for cerium (e), oxygen (d) and aluminum (f) of cerium oxide dispersion on H-ZSM-5. S11: STEM micrographs of CeO 2 /13X (a) and 13X ( b). EDX mapping region of CeO 2 /13X/ (c), oxygen (d) and aluminum (f) dispersion on 13X. 11
12 S12: TEM micrographs of CeO 2 /H-ZSM-5 (left) and CeOC 2 /13X (right). S13: EDX mapping of CeO 2 /13X calcined (cyan = Ce, magentaa = Si, yelloww = aluminum) 12
13 S14: XRD pattern of here used materials S15: Comparison of gas phase adsorption, external surface and pore volume 13
14 Cost estimation A detailed economic study was not performed. However, assuming an average concentration of indoors VOC of 0.5 ppm (equals 2.6 mg/m 3 for an average molecular weight of 130 g/mol) (Huey-Jen Su, Atmospheric Environment 41 (2007) ) and an adsorption capacity of 3 wt. %, this would correspond to 30 g VOC/kg adsorber. For an average room volume of 50 m 3 (total VOC about 130 mg) this would correspond to about 230 room volumes (230 r. V. /kg adsorber). At this point the adsorber needs to be regenerated. Systems based on activated carbon can adsorb about 10 wt. % (100 g VOC) corresponding to about 770 r. V. /kg adsorber. However, at this point the activated carbon must be replaced or regenerated separately, as regeneration on place would simply release the captured VOC in the environment. This will increment significantly the maintenance costs and the carbon emissions as small amounts of AC are not reactivated but incinerated. Compared to HVAC systems where the indoor air is replaced typically tree times per hour large air volumes must be filtered, cooled or heated in order to assure good indoor air quality. This will further increment the running costs. Additionally, an HVAC system is a complex construction and periodical maintenance is required. Table 4 Cost estimate for weekly regeneration (2.2 kg adsorber) Material price Adsorber material costs Material [$/kg] [$/Adsorber] Time to exhaustion [d] c Cost for one year of operation [$] CeO 2 /zeolite a Activated carbon b a assuming 2 service/maintenance b assuming 15 service/exchange plus material c air exchange is 3 room volumes per hour Service/maintenance costs: 50$/service From the table above is visible, that after about 3 cycles (exhaustion/regeneration for CeO 2 /zeolite) the acquisition costs are equalized. 14
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