1. GENERAL INFORMATION IUPAC

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1 AM-0 O N H C N. GENERAL INFORMATION IUPAC Name: {-[(-methylpiperidin--yl)methyl]-h-indol--yl}(naphthalen--yl) methanone CFR: Not Scheduled (0/0) CAS#: Synonyms: Source: Appearance: Kovat's Index: None DEA Reference Material Collection Yellow powder Pending UV max (nm): Not Determined. CHEMICAL AND PHYSICAL DATA. CHEMICAL DATA Form Chemical Formula Molecular Weight Melting Point ( o C) Base C 6 H 6 N O 8 6. Latest Revision: 0/5/0 Page of 6

2 AM-0. QUALITATIVE DATA. NUCLEAR MAGNETIC RESONANCE Sample Preparation: Dilute analyte to ~5 mg/ml in deuterochloroform (CDCl ) containing TMS for 0 ppm reference and dimethylfumarate as quantitative internal standard. Instrument: Parameters: 00 MHz NMR spectrometer Spectral width: at least containing - ppm through ppm Pulse angle: 90 o Delay between pulses: 5 seconds H NMR: AM-0; Lot 0698-; CDCl ; 00 MHz Dimethylfumarate (ISTD) Dimethylfumarate (ISTD) 0 TMS 9 8 CHCl Impurity Water Chemical 5 Shift (ppm) 0 Latest Revision: 0/5/0 Page of 6

3 AM-0 H NMR: AM-0; Lot 0698-; CDCl ; 00 MHz Chemical Shift (ppm). Gas Chromatography/Mass Spectrometry Sample Preparation: Dilute analyte ~ mg/ml in chloroform Instrument: Agilent gas chromatograph operated in split mode with MS detector Column: DB- MS (or equivalent); 0m x 0.5 mm x 0.5 µm Carrier Gas: Helium at ml/min Temperatures: Injector: 80 o C Injection Parameters: MS Parameters: Retention Time: MSD transfer line: 80 o C MS Source: 0 o C MS Quad: 50 o C Oven program: ) 00 o C initial temperature for.0 min ) Ramp to 00 o C at o C/min ) Hold final temperature for 9.0 min Split Ratio = 5:, µl injected Mass scan range: -550 amu Threshold: 00 Tune file: stune.u Acquisition mode: scan 5.9 min Latest Revision: 0/5/0 Page of 6

4 AM-0 EI Mass Spectrum: AM-0; Lot Intensity [x 0 6 ] EI m/z Intensity [x 0 ] EI Latest Revision: 0/5/0 Page of m/z

5 AM-0. INFRARED SPECTROSCOPY (FTIR) Insrument: FTIR with diamond ATR attachment ( bounce) Scan Parameters: Number of scans: Number of background scans: Resolution: cm - Sample gain: 8 Aperture: 50 FTIR ATR (Diamond, Bounce): AM-0; Lot %Transmittance Wavenumber (cm-) %Transmittance Wavenumber (cm-) Latest Revision: 0/5/0 Page 5 of 6

6 AM-0. ADDITIONAL RESOURCES Kneisel, S.; Bisel, P.; Brecht, V.; Broecker, S.; Müller, M.; Auwärter, V. Identification of the cannabimimetic AM-0 and its azepane isomer (N-methylazepan--yl)--(-naphthoyl)indole in a research chemical and several herbal mixtures. Forensic Toxicol. 0, 0 (), 6-. Uchiyama, N.; Kawamura, M.; Kikura-Hanajiri, R.; Goda, Y. Identification of two new-type synthetic cannabinoids, N-(-adamantyl)--pentyl-H-indole--carboxamide (APICA) and N-(-adamantyl)-- pentyl-h-indazole--carboxamide (APINACA), and detection of five synthetic cannabinoids, AM-0, AM-, AM-, CB- (CRA-), and AM-8, as designer drugs in illegal products. Forensic Toxicol. 0, 0 () -5. Kneisel, S.; Westphal, F.; Moosmann, B.; Brecht, V.; Bisel, P.; Vidal, C.; Jacobsen-Bauer, A.; Bork, W.; Auwärter, V. Trends auf dem Gebiet der synthetischen Cannabinoidmimetika: Massenspektren und ATR-IR-Spektren neuer Verbindungen aus dem Zeitraum Ende 00 bis Ende 0. Toxichem Krimtech, 0; 78 (); Forendex Wikipedia Latest Revision: 0/5/0 Page 6 of 6

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