The Right Choice Merck Solvents for Analysis. Highest quality wide range of applications

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1 The Right Choice Merck Solvents for Analysis Highest quality wide range of applications

2 The right choice a suitable solvent for every application Throughout the world, solvents from Merck are synonymous with reliability and top quality. All our products undergo continuous development to meet increasing quality requirements. The extent and quality of our product range reflect the results of this work and the feedback received from our customers all over the world. We have solvents to suit every application. gaschromatography HPLC for analysis spectroscopy dried solvents preparative laboratory applications and production Great additional benefit Nowadays, the requirements made of a solvent are much higher than its actual product characteristics. In addition to analytical purity, factors such as handling, safety and documentation all play an increasingly important role. Solvents from Merck fulfil these requirements in full. Increased specifications We have developed a new and comprehensive set of specifications for solvents of analysis quality. For our customers, this means an extraordinarily wide range of applications, maximum reliability and proven safety. Comprehensive range With almost 70 solvents for analysis, (such as the multi talent for qualitative and quantitative analysis, for extraction, synthesis, as well as for sophisticated product applications) Merck offers a range to satisfy every need. That all-important added value An unparalleled range of packaging, withdrawal systems and services adds the finishing touch to what we have to offer: an all-inclusive package in which components are finely tuned down to the very last detail. You couldn t hope for a better partner than Merck for individual laboratory applications. Merck the partner for added value. 2

3 Highest quality throughout the work process Selected raw materials Our special quality claim starts as early as the careful selection of high-quality raw materials. We only use select source materials of known origin and have defined the requirements for raw materials in collaboration with our suppliers. We monitor compliance with these guidelines on an ongoing basis to ensure a safe basis for the production of high-quality solvents. Innovative manufacturing methods Subsequent treatment of the raw materials takes place in one of the world s most advanced production and filling plants for high-purity solvents. It was developed and constructed according to stringent requirements to ensure optimum production processes and outstanding product quality. Plant operation is largely fully automatic with product-specific filling lines. Our distillation and filling capacities are unique the world over and enable rapid, flexible handling. Experienced chemical analysis with comprehensive documentation A certificate of analysis issued for each individual solvent documents the high quality of our products. Highly efficient chemical analysis that works with reliable, validated methods and with state-of-the-art technology ensures strict compliance with all specification values. Diverse packing material and withdrawal systems Only high-quality packaging and withdrawal systems selected with meticulous care in accordance with the respective content can fully preserve the quality of the solvents. We thus offer a particularly extensive range of drums, withdrawal systems and accessories. Safe application results High batch consistency is crucial for your daily work in the laboratory. After all, the results of your chemical analysis depend on the quality of the materials used and must be reproducible at all times. Merck solvents offer you maximum reliability in this regard. 3

4 The right choice best specifications for highest quality For solvents for analysis, Merck has always offered an unrivalled range of comprehensive and extensive specifications. For our customers, this means top product quality and maximum analysis safety. In addition, the extensive product specification enables the use of solvents in a variety of complex applications. For example, the documented values for metals guarantee use for flame photometric measurements. The inclusion of organic parameters also enables the classification of unwanted side reactions. We also take great care to continue to improve our specifications and to adapt these to changing requirements. In this way, we harmonise our specifications with international standards or extend them to include new parameters. Using this method, we are able to offer our customers optimum safety for a wide variety of different applications. Specified in accordance with international standards International rules and regulations are becoming increasingly important. During this process, not only are inspection and manufacturing methods clearly regulated and comparable throughout the world, but the quality of the materials used is also defined. In addition to ISO regulations (International Organisation of Standardisation), the codes of the pharmaceutical industry (American and European Pharmacopoeia) in particular prescribe a high and defined purity for reagents, for example, for use in pharmaceutical quality control. Whenever a solvent is described in one of these standards, for example, the ACS (American Chemical Society), we meet the relevant requirements. Validated methods in accordance with the ACS and Reag. PhEur (new!) We declare our solvents to be in compliance with the ACS 9 th edition and now also the reagent part of the European Pharmacopoeia (Reag. PhEur) for analysis purposes. We exclusively use the latest and validated analysis methods for this purpose. However, with our extensive product specifications, we do more than just fulfil these requirements in many areas, we even exceed them by a substantial margin. Thus, for users in pharmaceutical quality control in particular, solvents for analysis from Merck are the safest choice also with regard to compliance with international audit requirements. 4

5 New specifications Continuous optimisation of the manufacturing processes and the selection of only the very best raw materials has enabled us to further improve the quality of our solvents. As a result of this process optimisation, we are now able to clearly tighten up the specifications for the most important solvents and to extend them to include additional analysis results. The new specifications take into account up to 60 parameters. In addition to improved values for purity, water content and evaporation residue, it is now additional metals and secondary components that make the scope of the new specifications unique and that highlight the high quality level compared with that of other suppliers: Acetone for analysis Purity in % Water in % Evaporation residue in % Number of parameters Merck Competitor Competitor Competitor Competitor Ethanol for analysis Purity in % Water in % Evaporation residue in % Number of parameters Merck Competitor Competitor Competitor Methanol for analysis Purity in % Water in % Evaporation residue in % Number of parameters Merck Competitor Competitor Competitor Competitor Acetone for analysis Purity Evaporation residue Number of parameters in % 100,0 99,9 99,8 99,7 99,6 99,5 99,4 99,3 99,2 99,1 99,0 Merck 99.8 % Competitors 99.5 % in % 0,001 0,0009 0,0008 0,0007 0,0006 0,0005 0,0004 0,0003 0,0002 0, Merck % Competitors % Merck Competitors

6 The right choice solvents for analysis with new product specifications 6 The new specifications or improved limit values are highlighted in colour Ethanol abs. GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99.9 % Appearance Solubility in water Acidity or alkalinity Titrable acid Titrable base Density (d 20 C / 20 C) UV absorption Aldehydes (as Acetaldehyde) % Fusel oils Substances reducing potassium permanganate (as O) % Carbonyl compounds (as CO) % Readily carbonizable substances Volatile impurities (GC) Acetaldehyde and acetal (GC) Acetone (GC) % Benzene (GC) % Ethylmethylketone (GC) 0.02 % Isoamyl alcohol (GC) 0.05 % Methanol (GC) 0.02 % 2-Propanol (GC) % Total of other impurities (GC) 0,03 % Higher alcohols (GC) 0.01 % Chloride (Cl) 0.3 ppm Nitrate (NO 3) 0.3 ppm Phosphate (PO 4) 0.3 ppm Sulphate (SO 4) 0.3 ppm Ag % As % Au % Be % Bi % Ga % In % Li % Mg % Mo % Pt % Sb % Ti % Tl % V % Zr % Evaporation residue % Water 0.1 % Methanol GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99.9 % Appearance clear Solubility in water Acidity Alkalinity Density (d 20 C/ 20 C) Boiling point C Ethanol (GC) 0.05 % Acetone % Acetaldehyde % Formaldehyde % Matter discoloured by H 2SO 4 Carbonyl compounds (as CO) % Chloride (Cl) 0.5 ppm Sulphate (SO 4) 1ppm Substances reducing potassium permanganate (as O) % Ag % As % Au % Be % Bi % Ga % In % Li % Mg % Mo % Pt % Ti % Tl % V % Zr % Evaporation residue % Water 0.05 %

7 Toluene GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99.9 % Appearance clear Acidity Alkalinity Density (d 20 C / 20 C) Boiling Point C Chloride (Cl) 0.5 ppm Sulphate (SO 4) 1 ppm Thiophene % Sulfur compounds (as S) % Benzene (GC) % Readily carbonizable substances Ag % As % Au % B % Be % Bi % Ga % In % Li % Mg % Mo % Pt % Sb % Ti % Tl % V % Zr % Evaporation residue % Water = 0.03 % Improved specification parameter New specification parameter Subject to change Dichloromethane GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99,8 % Appearance clear Titrable acid 0,0002 meq/g Alkalinity 0,0002 meq/g Density (d 20 C / 4 C) 1,324 1,326 Boiling Point C Free chlorine (as Cl) 0,00002 % Chloride (Cl) 0,0001 % Matter discoloured by H 2SO Hazen Chloroform (GC) 0,005 % Ethanol (GC) 0,02 % Methanol (GC) 0,1 % Carbon tetrachloride (GC) 0,005 % Fluorescence (as chinine at 365 nm) 0,002 ppm Al 0,00005 % B 0, % Ba 0,00001 % Ca 0,00005 % Cd 0, % Co 0, % Cr 0, % Cu 0, % Fe 0,00001 % Mg 0,00001 % Mn 0, % Mo 0,00002 % Ni 0, % Pb 0,00001 % Sn 0,00001 % Zn 0,00001 % Evaporation residue 0,001 % Water 0,01 % Stabilized with about 50 ppm 2-Methyl-2- buten Acetone GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99.8 % Appearance of solution Solubility in Water Water-insoluble substances Density (d 20 C/20 C) Acidity or alkalinity Titrable acid Titrable base Cyclohexane (GC) 0.1 % Diacetone (GC) 0.02 % Ethanol (GC) 0.01 % Methanol (GC) 0.05 % 2-Propanol (GC) 0.05 % Related substances (GC) Aldehydes (as formaldehyde) % Substances reducing potassium permanganate (as O) % Reducing substances Chloride (Cl) 100 ppb Nitrate (NO 3) 100 ppb Phosphate (PO 4) 100 ppb Sulphate (SO 4) 100 ppb Ag % As % Au % B % Be % Bi % Ga % Ge % In % Li % Mg % Mo % Sb % Ti % Tl % V % Zr % Evaporation residue % Water 0.05 % 7

8 Propanol GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99.8 % Appearance clear Solubility in water Acidity meq/g Alkalinity Density (d 20 C / 20 C) Boiling point C Chloride (Cl) 300 ppb Nitrate (NO 3) 300 ppb Phosphate (PO 4) 500 ppb Sulphate (SO 4) 1000 ppb Substances reducing potassium permanganate (as O) 2 ppm Carbonyl compounds (as CO) % Matter discoloured by H 2SO 4 Acetone (GC) 0.01 % Ethanol (GC) 0.01 % Isopropylether (GC) 0.01 % Methanol (GC) 0.01 % 1-Propylalcohol (GC) 0.1 % Ag % As % Au % B % Be % Bi % Ga % In % Li % Mg % Mo % Pt % Sb % Ti % Tl % V % Zr % Evaporation residue % Water 0.05 % n-hexane GR for analysis ACS Purity (GC) 99.0 % Alkalinity Acidity Density (d 20 C / 4 C) Thiophene Aromatics (as benzene) 0.01 % Sulfur compounds (as S) % Matter discoloured by H 2SO 4 B % Mg % Evaporation residue % Water % Chloroform GR for analysis ACS, ISO, Reag. PhEur Purity (GC) % Assay according to ACS 99.8 % Appearance clear Free acid (as HCl) % Density (d 20 / 20 C) Boiling point C Acid and chloride Chloride (Cl) % Free chlorine % Carbonyl compounds (as CO) % Readily carbonizable substances Ethanol (GC) % Dichlormethane (GC) 0.01 % Carbon tetrachloride (GC) 0.01 % Tetrachloroethylene (GC) 0.01 % Trichloroethylene (GC) 0.01 % Related substances (GC) 0.7 % Aldehydes and ketones (C 3H 6O) % Suitability for determination with dithizone B % Mg % Mo % Evaporation residue % Water 0.01 % 8

9 Tetrahydrofuran GR for analysis ACS, Reag. PhEur Purity (GC) 99.8 % Appearance clear Density (d 20 /20 C) Acidity meq/g Alkalinity Peroxide (as H 2O 2) % B % Mg % Evaporation residue % Water 0.03 % Diethyl ether GR for analysis ACS, ISO, Reag. PhEur Purity (GC) 99.7 % Appearance clear Titrable acid Alkalinity Density (d 20 /20 C) Boiling point C Chloride (Cl) % Sulphate (SO 4) % Acetone (GC) % Ethanol (GC) 0.02 % Methanol (GC) 0.02 % Peroxide (as H 2O 2) % Carbonyl compounds as HCHO 0,001 % as CO % Matter discoloured by H 2SO 4 B % Mg % Evaporation residue % Water 0.03 % Improved specification parameter New specification parameter Subject to change 9

10 The right choice optimum packaging and withdrawal systems Unique packaging diversity We are fully aware of the need for high quality packaging in order to maintain the high quality of our solvents until practical application. In addition to quality assurance, the economic aspect also plays a key role: we always develop packaging in accordance with the needs of our customers since only when packaging sizes are suitable for the respective applications and requirements is it possible to make economical use of the solvents. We offer a unique variety of different packaging sizes and types for our solvents. The following criteria are central to Merck s development and selection of packaging materials: Use of high-quality materials Safe handling Avoidance of interactions between solvents and packaging material Ecological and economical benefit (e.g. re-useable packaging) Avoidance of packaging and chemical waste 10

11 1-l-, 2,5-l- and 4-l-glass bottles Optimum characteristics for handling, storage and transport. Safe footprint, low centre of gravity, optimum emptying, safety screw cap S40. 1-l-, 2,5-l- and 5-l-PE-bottles Outstanding handling characteristics due to integrated carrying handle for 2.5-l- and 5-l-bottles. Made from HDPE, tested for blisters and particles, pressure-resistant to 2.5 bar. No risk of fracture, small footprint (optimum for storage), low weight (easy to transport and low transport costs). UN certification (to be sent without polystyrene outer packaging). Innovative packaging material In addition to conventional packaging, such as bottles, drums and barrels, we also implement quite specific solutions: intermediate bulk containers (IBCs), road tankers or tank containers. If technically possible, we also fill other packaging containers that you provide. 5-l-aluminium bottle, 10-l-, 25-l- and 190-l-stainless-steel drums Optimum material characteristics (no interaction), use as reusable container, can be combined with a variety of different withdrawal systems For many years, Merck has been developing new practically-orientated packaging concepts and chemical packaging, which are used exclusively by Merck. In addition, we have been authorised as an official inspection authority by the Federal Institute for Materials Research and Testing (BAM). 25-l- and 180-l-steel drums Ideal packaging for safe and low-cost use, especially in the production process. 11

12 Withdrawal system with threaded adapter, flexible stainless steel-coated teflon tube and self-closing filling nozzle System compounds: 2"-thread adapter with two rapidaction connections, spiral gas feed tube for pressurizing, stainless steel-coated teflon tube with rapid-action connector and threaded connector, self-closing stainless steel nozzle with large handle. Advantages: flexible tubing (gas: 180 cm usable length, product: 80 cm length), enables simple and safe filling of smaller bottles or containers, central storage and supply possible. Safe and flexible withdrawal system For the safe extraction of high-purity solvents, we have developed withdrawal systems that are optimally matched to the different laboratory applications. Due to the diverse range of individual components and possible combinations, customised solutions present no problem whatsoever: ranging from the simple extraction tap made of polyethylene, threaded adapters, barrel keys and complete withdrawal systems with manual pressure build-up to high-tech systems with quick-fit connections and self-closing nozzles everything is possible. Withdrawal system for manual pressure build-up for stainless steel returnable drums System compounds: exchangeable dip tube for 10 and 20 L stainless steel drums, clamp for outlet tube, ball valve, pump ball, three-way stopcock. Advantages: independent from gas supply, enables simple and safe filling of smaller bottles or containers, can be used in the laboratory, central storage possible. 12

13 The right choice comprehensive service Customised solutions Our high quality claim also includes meeting individual customer requirements our extraordinary service offers you additional value: Manufacture of special qualities or solvent mixes Adoption of customer s own specifications Use of customer s own or special packaging Development of individual logistics concepts Support with regulatory questions High availability We set great store by the continuous provision and punctual delivery of our solvents. On the basis of our large distillation and filling capacities, we are flexible when reacting to individual customer requirements. You can rely on the unique combination of all benefits: Solutions High product quality Best batch consistency Safe analysis Comprehensive documentation Specifications Best specifications Very wide range of applications Great packaging diversity Accessories Flexible withdrawal systems Customised service 13

14 The right choice our complete range Ordering information and product range overview of solvents GR for analysis The complete item number is made up of the material and packaging number. For a 2.5-litre glass bottle for acetone, this is e.g Are you interested in other innovative products by Merck? Then visit us on the Internet at We provide information and advise our clients to the best of our ability and knowledge, however without any obligation and without any assumption of liability on our part. Existing legislation and other regulations shall in all instances be observed by our clients. This shall also apply to industrial property rights of third parties as may exist. Our information and advice shall not absolve our clients from the obligation of inspecting our products at their own responsibility for the suitability thereof for the purposes intended. Name Purity % Acetone ACS, ISO, Reag PhEur 99.8 Acetonitrile ACS, Reag PhEur 99.5 Acetylacetone 99 n-amyl alcohol 98.5 Aniline 99.5 Benzene ACS, ISO, Reag PhEur 99.7 Benzyl alcohol Butanol ACS, ISO, Reag PhEur Butanol 99 tert-butanol ACS, Reag PhEur 99.5 n-butyl acetate 99.5 tert-butyl methyl ether 99.5 Carbon disulfide ACS, Reag PhEur 99.9 Crabon tetrachloride 99.8 Carbon tetrachloride for determinations with dithizone ISO 99.9 Chloroform stab. ACS, ISO, Reag PhEur Chloroform for determinations with dithizone Cyclohexan ACS, ISO, Reag. PhEur ,2-Dichlorbenzene for extraction analysis 99.0 Dichloromethane ACS. ISO, Reag PhEur 99.8 Diethanolamine 99.5 Diethyl ether ACS, ISO, Reag PhEur 99.7 Diisopropyl ether ACS, Reag PhEur 99.0 Diisopropyl ketone 98.0 n,n-dimethylfomamide ACS, ISO, Reag PhEur 99.8 n,n-dimethylformamide LAB 99.5 Dimethyl sulfoxide Reag PhEur ,4-Dioxane ACS, ISO 99.5 Ethanol absolute ACS, ISO, Reag PhEur 99.9 Ethanol denatured with about 1 % MEK 99.5 Ethanolamine 99.5 Ethyl acetate ACS, ISO, Reag PhEur 99.5 Ethylene glycol Reag PhEur 99.5 Ethylene glycol monomethyl ether ACS, Reag PhEur 99.5 Ethyl methyl ketone ACS, Reag PhEur 99.5 Formamide ACS, Reag PhEur 99.5 Glycerol about 87 % Glycerol ACS, Reag PhEur 99.5 n-heptane Reag PhEur 99 n-hexane ACS 99.0 n-hexane ACS, Reag PhEur 96.0 Isoamyl alcohol ACS, Reag PhEur 99 Isoamyl alcohol (mixture of isomers) for determination of fat acc. to Gerber 98.0 Isobutanol ACS, Reag PhEur 99 Isobutyl methyl ketone for extraction analysis ACS, Reag PhEur 99.0 Isohexane 95.0 Isooctane ACS, Reag PhEur 99.5 Methanol ACS, ISO, Reag PhEur 99.9 n-pentane 99.0 Petroleum Petroleum benzine boiling range C Petroleum benzine boiling range C ACS, ISO Petroleum benzine boiling range C Petroleum benzine boiling range C Piperidine 99 1-Propanol ACS. Reag PhEur Propanol ACS, ISO, Reag PhEur 99.8 Pyridine ACS, Reag PhEur 99.5 Tetrahydrofuran ACS, Reag PhEur 99.8 Toluene ACS, ISO, Reag PhEur ,1,1-Trichloroethane 99.5 Trichloroethylene ACS, Reag PhEur ,1,2-Trichlorotrifluoroethane ACS, Reag PhEur 99.8 n-undecane 99 Water Xylene ACS, ISO, Reag PhEur

15 Packaging-number Packaging Content 100 ml Glass x ml Glass x ml Glass x.0500 Evaporation residue % Water % Pruduct-number x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x 500 ml Polyethylene x I Glass x.1000 Polyethylene x I Polyethylene x I Glass x.2500 Polyethylene x I Polyethylene x I Polyethylene x l Aluminium x l Titripac x I Stainless steel x.6010 drum 25 l Steel drum x I Steel drum x I Stainless steel x.6025 drum 180 I Steel drum x I Steel drum x I Stainless steel x.6190 drum x x x x x x x x x x x x x x x x x x x x x x x x 15

16 Further information on Merck and our products: Merck KGaA Darmstadt, Germany Fax: W

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