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1 APPLIED SCIENCE PRIVATE UNIVERSITY (A.S.U) AMMAN - JORDAN جامعة العلوم التطبيقية الخاصة ( ج.ع.ت( عمان األردن فلنجعل من أردن العرب جامعة للعرب Faculty : Pharmacy Department: Pharmaceutics and Pharmaceutical Sciences Academic Year: 2017/2018 Semester : First ( Course Syllabus ) Subject Name Credit Hours Course No. Prerequisite Physical pharmacy Concurrent course Coordinator Name Lecturer/s Room No. Dr.Areen Khattabi Dr.Areen Khattabi And Faten Odah 120 Course website Office Hours a_khtabi@ asu.edu.jo u.jo/bio/index.jsp 1-2(S, T,Th) (M and W) (S) Course Description: This course investigates the application of physico-chemical principles to problems in the pharmaceutical sciences. The impact of physicochemical and biopharmaceutical properties of drugs on the safety, effectiveness, stability and formulation of various pharmaceutical dosage forms is discussed thoroughly during the course. This will be achieved via understanding the following topics: states of matter, the subphases that solids can exist, properties of drugs in solution and colligative properties, equilibrium phenomena, solubility, chemical kinetics, drug stability and interfacial phenomena. Course Objectives: This course intends to make the students understand: 1. The physicochemical and biopharmaceutical properties of the drug substances as well as drug products. 2. The impact of such properties on the formulation, processing and performance of final dosage forms in terms of bioavailability, safety and stability. Intended Learning Outcomes: Following the successful completion of this course, the student should be able to: A. Knowledge and understanding: Student is expected to A1. Recognize the various subphases that solids can exist in such as, polymorphs, solvates, hydrates, amorphous etc. A2. Understand the physical properties of the solid state of drugs and their relevance to the production and performance of finished pharmaceutical products. A3. Know the various factors (ph, Temperature, salt) that affect the solubility of a drug in pharmaceutical solutions. 1
2 A4. Understand the fundamentals of chemical reaction kinetics of simple and complex reactions. B. Subject specific skills: Student is expected to B1. Establish methodologies for differentiating the various orders of Chemical Reactions as well as how to compute various kinetics parameters associated with each order. B2. Develop a theoretical and mathematical foundation for surface tension and its rule in wetting as well as adsorption at liquid or solid interfaces B3. Apply the knowledge, which the student had learnt, to be able to prepare different buffers C. Cognetive and Intellectual skills: Student is expected to C1. Build up knowledge and scientific skills regarding factors that affect reaction rate and drug stability and the overall stability of pharmaceuticals C2. Understand the rule of partition coefficient during preformulation studies in the development of pharmaceutical dosage forms D. Transferable Skills: Student is expected to be able to D1. Recognize the concept of colligative properties and their pharmaceutical applications such as the preparation of isotonic solutions D2. Acquire knowledge about the concept of solubility and the various ways for improving it for medicinal substances with poor water solubility Development of ILOs is promoted through the following teaching and learning methods: ILOs Learning Methods Evaluation Methods The introduction Lectures and Reading Exams A1, A2, A3, A4, B2, Lectures, which is accompanied with oral Exams C1 and C2 questions and discussions about the topic B1, B3, D1, A3 and A4 based on thinking Problem solving and oral discussions with the students Exams Course Content: Week Date Lecture number / hours 1. 3 hours Topic s Details Introduction (Molecular expressions and electrolyte properties of drug molecules) 2 Exams/ /quizes/holidays Main Reference (chapter) Basic Physical Pharmacy, Joseph K.H.Ma, Boka W.Hadzija (2013), part 1( physical pharmacy in solutions ILOs achieved Lectures 2. 3 hours States of Matter Lectures
3 3. 3 hours 4. 3 hours solid 5. 3 hours solids 6. 3 hours 7. 3 hours 8. 3 hours 9. 3 hours hours (Intermolecular forces, The gaseous state, The liquid state) part of solids Solids (Crystal structure, Crystal form, Polymorphism, Crystal hydrates, Dissolution of solid drugs, Biopharmaceutical importance of particle size, Wetting of powders, Solid dispersions) FIRST EXAM Physicochemical properties of drugs in solution Physicochemical properties of drugs in solution Ionic Equilibria & buffered solutions SECOND EXAM Ionic Equilibria & buffered solutions Drug stability (The chemical decomposition of drugs, Kinetics of chemical decomposition in solution, Solid dosage forms, Factors influencing drug stability, Stability testing and prediction of shelflife) hours Drug stability hours The solubility of drugs (Definitions, Factors influencing 3 Chapter 1 Chapter 1 Chapter 1 Chapter 2 Chapter 2 Part of chapter 2 and part of chapter 3 Part of chapter 2 and part of chapter 3 Chapter 3 Chapter 3 Chapter 4 A1 and A2 A1 and A2 A1 and A2 A3 and D1 A3 and D1 B3 B3 A4, B1 and C1 A4, B1 and C1 C2 and D2
4 13. 3 hours hours solubility, Measurement of solubility, The solubility parameter, Solubility in mixed solvents, Solubility problems in formulation, Partitioning, Biological consequences of log P) The solubility of drugs Surfactants and interfacial phenomenon FINAL EXAM Chapter 4 Martin s Physical Pharmacy and Pharmaceuti cal Sciences C2 and D2 B2 Grade Distribution: Your course grade will be determined by the following: Assessment Method % of Final Grade Due Date First Exam 25 % To be announced Second Exam 25 % To be announced Third Exam 50 % To be announced * Provisional dates are scheduled in the course schedule. Distribution of examination material (may vary depending on material included): 45 % - questions based on critical thinking, connecting the topics and successful conclusions. 25% - questions based on memorizing (if available) 30% - calculations and questions based on using laws presented in the course 23. Course Policies: A- Attendance policies: Attendance: Mandatory. First warning with 4 absences Last warning with 5 absences Failing in the subject with 6 absences B- Absences from exams : Will result in zero achievement unless health report or other significant excuse is documented. C- Health and safety procedures: NA 4
5 D- Honesty policy regarding cheating, plagiarism, misbehavior: The participation, the commitment of cheating will lead to applying all following penalties together 1. Failing the subject he/she cheated at 2. Failing the other subjects taken in the same course 3. Not allowed to register for the next semester. The summer semester is not considered as a semester E- Grading policy: Exams and Quizzes. First Exam: Second exam: Assignments/quizzes: Final Exam: Total: 25 points 25 points NA 50 points 100 points F- Available university services that support achievement in the course: Classrooms, internet classes 24. Required equipment: Data show, internet connection and board. Make-up Exam Policy: Make-up exams will be offered for valid reasons. They may be different from regular exams, both in content and format. Textbooks information: Main Reference: Physicochemical Principles of Pharmacy, Sixth Edition, Alexander T Florence, David Attwood Other References: Martin s Physical Pharmacy and Pharmaceutical Sciences. Patrick J. Sinko. 6th Edition, Additional information: No side talks during lecture No mobile phones during lecture Entering the lecture theatre after the instructor is not permitted. Homework should be done by students independently and will be asked at the exams Course Material and Announcements Students need to use the e-learning page at the ASU website in order to get all lecture handouts and guidelines which will be uploaded there. 5
6 In addition, course related announcements and exam results will be posted on the ASU online AND/OR course website and is the responsibility of each student to check the sites regularly. Name of Course Coordinator: Dr. Areen Khattabi 15/10/2017 Signature: Date: Head of curriculum committee: Signature: Head of Department: Signature: Dean: Signature: Copy to: Head of Department Head of curriculum committee Course File C 26 / version 3 Date: رقم اجراء الخطة الدراسية 19 UF) QP 29) 6
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