Reagents - Install/Replace. Select method/sequence. KF Reagent calibration Running KF titration methods. Running SAC sequences

Transcription

1 Short-For t-form Reminders Reagents - Install/Replace Select method/sequence KF Reagent calibration Running KF titration methods Running SAC sequences Maintenance recommendations Storage recommendations Spare parts & accessories Electrodes and solutions DT080 Printed by Radiometer Analytical SAS B Short-Form Reminders

2 Short-Form Reminders

3 To replace empty reagent bottles, use the bottle exchange procedure Reagents - Install/Replace Form no. Select method or sequence and For a and 3 method XYZ For a sequence Install reagent system. Enter Reagent window. then 3. Press to enter batch no., expiry date then confirm 4. If required, rinse burette Remove a reagent 5. Install reagent bottle and press to flush Run the Rinse procedure in the Burette functions screen. This procedure is required when you no longer wish to use the reagent or replace it by another one.. Enter Reagent window. 3 XYZ then 4 JKL

4 Bottle exchange: with one of same type and ID. Enter Reagent window 4. Confirm. then 5. Enter batch no. and expiry date of new reagent and confirm 6. Remove bottle 3. Press to select reagent 7. Install new bottle and press to flush and fill Replace reagent: with different type and ID. Enter Reagent window 4. Confirm replace. then Enter batch no. and expiry date 6. Remove old, install new reagent bottle, press to flush DT080 Printed by Radiometer Analytical SAS France B

5 Straightforward method selection Select method/sequence Form no. Select method. Enter main menu. Select method from list 3. Confirm

6 Select sequence. Enter main menu. 3 XYZ then 3. Enter sequence name and confirm 4. Esc Check icons You can run the method You can run the method. However a calibration and/or a reagent bottle exchange must be performed soon Check the reagents for installation or calibration purposes Programming error due to missing parameters DT080 Printed by Radiometer Analytical SAS France B

7 Calibrate your reagent KF Reagent calibration Form no. 3 Select reagent. Enter Reagent window. then to select reagent from list 3. Confirm Run. To run the calibration. Enter User ID, if required, and confirm

8 3. Enter Standard batch number then confirm 4. Rinse electrode(s) and dip in beaker. Check solvent level. Confirm 5. After cell equilibration, inject Standard advised amount into the cell. Confirm 6. Enter Standard amount. Confirm Automatic result display Press to save result View statistics Stop then More tests/end of analysis Resume analysis Emergency stop DT080 Printed by Radiometer Analytical SAS France B

9 Run your analyses Running KF titration methods Form no. 4 Run. To run your selected method (*). Enter User ID, if required, and confirm 3(*). Enter Sample ID and confirm 4(*). Rinse electrode(s) and dip in beaker. Check solvent level and confirm 5. After drift determination, inject Sample advised amount into the cell. Confirm 6. Enter Sample amount. Confirm (*) In Run sample start = Shortcut mode, steps, 3 and 4 and are chained automatically:. Rinse and dip electrodes in beaker.. To start drift determination.

10 Automatic result display (*) Press to save results (*) In Run sample end = Shortcut mode, this window does not appear and the results are displayed. View statistics (*) then (*) In Run sample end = Shortcut mode, this window does not appear. More tests/end of analysis (*) Running new tests/samples in Run Sample start = Shortcut mode: Rinse and dip electrode in beaker then or (*) In Run sample end = Shortcut mode, this window only appears if several sample replicates have been edited for the method. Stop Del Emergency stop Resume analysis. To resume analysis. Calculations are not performed To end an analysis before the maximum titration time or the maximum volume have been reached. Calculations are performed, if result found DT080 Printed by Radiometer Analytical SAS France B

11 Use your Sample stack for daily analyses Running SAC sequences Form no. 5 Preparing the sample stack. 3 XYZ + 5. Locate beaker no. and place it on the sample changer turntable/tray. 6. Enter a new sample ID and confirm Repeat steps to 5 for each beaker in the sequence Check the sample test quantity or enter the sample test quantity to place in beaker no. Confirm + 7. Esc then Esc

12 Run. (*). Enter User ID, if required, Enter drift and confirm (*) In Run sample start = Shortcut mode, step is skipped. Emergency stop Stop Resume analysis. To repeat titration in the same beaker. Stop Next analysis. To start sequence in the next beaker. Stop Del End of analysis. To stop the sequence. To end an analysis before the maximum titration time or the maximum volume have been reached. Calculations are performed, if result found. DT080 Printed by Radiometer Analytical SAS France B

13 For burette air bubble removal, run the Flush procedure Maintenance recommendations Form no. 6 Daily Check and maintain electrodes according to manufacturer recommendations. Check that there is no crystallisation at piston level, if so rinse the burette using appropriate solvent to remove crystals. If not sufficient, dismount burette to remove crystals. Check that there is no crystallisation at addition tip end that may block the reagent to pour freely, if so use appropriate solvent to remove crystals. Check the level of reagent in the reagent bottle Empty waste bottle if installed. Remove air bubbles from the burette and tubing by running a Flush procedure from the burette menu. Weekly Reagent glass cylinder piston Reagent Flush the burette with appropriate solvent to ensure complete cleaning of burette and stopcock. Change burette stand Check the piston for leakages. The burette stand must be changed when at least mm of liquid can be seen between the two sealing lips. Refer to diagram. Having mm or less liquid between the two sealing lips does not require to change the burette stand.

14 Annualy Replace burette stand,, 5, 0, 5, 50 ml and the anti-diffusion tip, part. no Frequent use or use with aggressive or concentrated reagents occurring crystallisation risks may severely reduce the burette and anti-diffusion tip lifetime and may consequently require to replace them more frequently. Replace burette stand set of 3 tubing, (stands 5, 0, 5, 50 ml, part number X3T5 and stand ml, part number X3T6). Replace damaged burette accessories: bottle stopper, desiccant tubing. Contact your Radiometer Analytical representative for instrument revision and cleaning. Recommendations of use After installing new burette and/or tubing, before use, check that all tubing fittings are sufficiently tightened to prevent leakage, and that no tubings are crimped (do not over tight fittings) The reagent should be at room temperature before use in the burette. If you do not use your titration system during several days, always rinse the burette with a suitable solvent (example: ethanol for a KF titrant burette). This makes it possible to lengthen the lifetime of the stopcock and the burette. Organic solvents: the organic solvents given as reacting with and/or destroying the VITON (Fluorinated polymer) should not be used with our burette stands (example: TetraHydroFurane). The solvents given as simply making inflate the VITON are allowed. Please contact us if you wish to work with solvents destroying the VITON. DT080 Printed by Radiometer Analytical SAS France B

15 Keep your system in tiptop condition! Storage recommendations Form no. 7 Daily Rinse electrodes and delivery tip throughly with distilled water after use. Store the electrode(s) following the instructions given in the respective operating instructions. Overnight and up to week In case of spillages, clean the exterior surface of the instrument with a soft cloth and tepid water. Avoid the accumulation of excess water around the keyboard area. Long-term week or more Run the Rinse procedure from the Burette menu to remove reagent from burette and tubings. If the system is to be left in the same location, store electrode(s) following the long-term storage instructions given in the respective operating instructions. If the system is to be transported, dismount the burette stand, metal rod, and cell accessories before packing. For transportation, always use the packaging supplied by the manufacturer. DT080 Printed by Radiometer Analytical SAS France B

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17 Ordering information at a glance Spare parts & accessories Form no. 8 Part no. Type Description X5T05 X5T06 X5T07 X5T07 X5T08 Burette stands B50 Burette Stand, ml, UV protected with connection tubing B505 Burette Stand, 5 ml, UV protected with connection tubing B50 Burette Stand, 0 ml, UV protected with connection tubing B55 Burette Stand, 5 ml, UV protected with connection tubing B550 Burette Stand, 50 ml, UV protected with connection tubing Burette maintenance parts Anti-diffusion tip PTFE X3T5 Maintenance Kit of 3 tubes for B5xx & B6xx (excl, ml burette) X3T6 Maintenance Kit of 3 tubes for B50 & B60only X5T00 Delivery tip, glass, burette >5 ml X5T0 Delivery tip, glass, burette <5 ml X3T070 Titrant bottle stopper GL45 assembly with desiccant & suction tubing X3T0 Titrant bottle stopper GL45 assembly with desiccant & suction tubing for B50 Polypropylene titration vessels Titration Vessel, PP, ml (pack of 50 pcs) Titration Vessel, PP, -45 ml (pack of 50 pcs) Titration Vessel, PP, 8-5 ml (pack of 50 pcs) Titration Vessel, PP, -9 ml (pack of 50 pcs)

18 Part no. Type Description Notebook keyboard X3T08 X6T005 X6T006 Notebook Keyboard Mask Notebook Keyboard 83-keys, PS/ port, US version Notebook Keyboard 83-keys, PS/ port, French Balance connecting cables A95Z0 C0Z 9pf/m/5pm (Mettler PE+option 06; Mettler AE+option 0 or 0) A95Z05 C05Z 9pf/m/5pm (Mettler PE+option 06; Mettler AE+option 0 or 0) A95Z06 C06Z m serial cable for Mettler AM, PM, SM, AT, MT, UMT, PJ, AJ A95Z0 C0Z 9bf/m/5bm (Sartorius MasterPro, QC, MP8-4) A95Z04 C04Z 9bf/m/5bm (Sartorius MasterPro, QC, MP8-4) A95Z07 C07Z 9pf/.0m/5pm (Precisa, old models) A95Z08 C08Z 9pf/m/RJ45 (Precisa, XB series) For other balances, please consult. KF consumables X3T048 KF Pump Tubing assembly, cell - bottle solvent X3T06 KF Pump Tubing assembly, cell - bottle waste X3T Desiccant Tube with tubing, Bottle - KF pump for bottle stopper GL45 & S40 X3T05 Syringe, plastic, 5 ml (0 pcs) X4T006 Needle, 0 mm, KF cell (0 pcs) X3T038 Silicone Septa for X3T036, set of 0 X3T65 Sample Container with funnel, 5pcs S7T004 Molecular Sieve, 50 g DT080 Printed by Radiometer Analytical SAS France B

19 Ordering information at a glance Electrodes and solutions Form no. 9 Part no. Type Description Pt-Pt Metal electrodes Karl Fischer titrations E3M00 M3Pt Double platinum wire, banana plugs *** E3M00 M4Pt-8 Double platinum staples, short cable *** For use with adapter, type BNC-f/ Banana, part no. A94P80 Single Metal electrodes E34M003 M95Ag Silver Rod, ø = 7.5 mm, PTFE body, banana plug ** E3M00 M4Pt Platinum Plate, ø = 7.5 mm, glass body, banana plug ** ** For use with adapter, type BNC-m/Banana-f, part no. A94P807 Temperature Sensor E5M00 T0 Temperature Sensor, glass Electrode Maintenance Solutions S6M00 RENOVO N Normal Cleaning Solution, 50 ml S6M00 RENOVO X Xtra Strong Cleaning Solution, 50 ml DT080 Printed by Radiometer Analytical SAS France B