EKC 336 Chemical Reaction Engineering [Kejuruteraan Tindakbalas Kimia]

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1 UIVERSITI SAIS MALAYSIA First Semester Eamination 9/1 Academic Session ovember 9 EKC 6 Cemical Reaction Engineering [Kejuruteraan Tindakbalas Kimia] Duration : ours [Masa : jam] Please ceck tat tis eamination paper consists o IE pages o printed material and THREE pages o Appendi beore you begin te eamination. [Sila pastikan baawa kertas peperiksaan ini mengandungi SEMBILA muka surat yang bercetak dan TIGA muka surat Lampiran sebelum anda memulakan peperiksaan ini.] Instruction: Answer FOUR questions. Answer any TWO questions rom Section A. Answer any TWO questions rom Section B. All questions carry te same marks. [Araan: Jawab EMPAT soalan. Jawab DUA soalan dari Baagian A. Jawab DUA soalan dari Baagian B. Semua soalan membawa jumla marka yang sama.] In te event o any discrepancies, te Englis version sall be used. [Sekiranya terdapat sebarang percanggaan pada soalan peperiksaan, versi Baasa Inggeris endakla diguna pakai]. /-

2 - - [EKC6] Section A: Answer any TWO questions. Baagian A: Jawab mana-mana DUA soalan. 1. [a] Wat are te advantages o plug low reactor? Apaka kelebian reaktor aliran palam? [ marks/marka] [b] [c] Te gas pase decomposition A C k.1 s -1 is carried out in a plug low reactor at C and 1 atm. Reactor eed rate is at 1 mol/s, and contains 75 mol% inert. Determine te lengt o 1 inc diameter pipe needed to reac 99% conversion. Comment on te practicality o your design. Penguraian asa gas A C k.1 s -1 dilalukan dalam reaktor aliran palam pada suu C dan tekanan 1 atm. Kadar suapan reaktor adala 1 mol/s, dan mengandungi baan lengai 75% mol. Tentukan panjang yang diperlukan bagi paip yang berdiameter 1 inci bagi mencapai penukaran 99%. Berikan komen sama ada rekabentuk anda praktikal atau tidak. [8 marks/marka] Te gas-pase reaction A B C is being carried out batcwise in a vessel at 55 C and.5 atm. Te reactor is initially carged wit a gas miture o % A in inert. Tindakbalas asa gas A B C dijalankan dalam bekas secara kelompok pada suu 55 C dan tekanan.5 atm. Reaktor pada mulanya disuap dengan campuran gas yang terdiri daripada % A dan selebinya baan lengai. [i] [ii] Build a stoiciometric table sowing concentrations at any conversion, X. Bina jadual stoikiometri yang menunjukkan kepekatan pada mana-mana penukaran, X. Determine te amount o time required to acieve 85% conversion, i te reaction is elementary, te reactor is isotermal, and te rate constant is.5 r -1. Tentukan jumla masa yang diperlukan untuk mencapai penukaran 85%, sekiranya tindakbalas tersebut adala asas, reaktor pada keadaan sesuu dan pemalar kadar adala.5 jam -1. [1 marks/marka] [d] Starting wit te general mole balance, develop te design equation or a continuous stirred tank reactor. Clearly state eac assumption you make, simpliy te equation in term o space time by assuming a liquid-pase elementary isomerization reaction o reactant A. Bermula dengan imbangan mol umum, bina persamaan rekabentuk bagi reaktor tangki pengaduk berterusan. yatakan dengan jelas setiap anggapan yang dibuat, permudakan persamaan dalam bentuk masa ruang dengan beranggapan tindakbalas pengisomeran asas asa-cecair bagi baan tindak balas A. [5 marks/marka].../-

3 - - [EKC6]. [a] Te omogeneous gas decomposition o pospine, PH g P g 6H g, occurs at 69 C wit a rate constant o 1 r -1. Wat is te size o plug low reactor operating at 69 C and 6 kpa to acieve 8% conversion o a eed consisting o mol/r o pure pospine? Penguraian omogen gas osin, PH g P g 6 H g, berlaku pada suu 69 C dengan pemalar kadar sebanyak 1 jam -1. Apaka saiz reaktor aliran palam yang beroperasi pada suu 69 C dan tekanan 6 kpa yang diperlukan untuk mencapai penukaran 8% suapan yang terdiri daripada mol/jam osin tulen? [8 marks/marka] [b] Prepare a stoiciometric table as a unction o conversion A sowing te eluent concentrations o all species o a gas-pase plug low reactor or te reaction A B C. Te reactor eed contains 5 mole % inert. Sediakan jadual stoikiometri dalam ungsi penukaran A yang menunjukkan kepekatan keluar bagi semua spesis untuk reaktor aliran palam asa-gas bagi tindakbalas A B C. Suapan reaktor terdiri daripada 5 mol % baan lengai. [9 marks/marka] [c] How long sould a 5 L batc reactor be operated at 55 K to acieve 95% conversion o A or te elementary gas pase reaction A B C k.15 dm /mol s i te reactor is carged wit only te reactants y A.? Wat is te inal pressure o te vessel at 95% conversion? Assume an initial pressure o 8. atm. Berapa lamaka masa yang diperlukan bagi reaktor kelompok 5 L yang beroperasi pada suu 55 K bagi mencapai penukaran A sebanyak 95 % bagi tindakbalas asas asa gas A B C k.15 dm /mol s sekiranya reaktor disuap dengan baan tindakbalas y A.? Apaka tekanan akir reaktor pada taap penukaran 95%? Anggapkan tekanan awal adala 8. atm. [8 marks/marka]. [a] Te potocemical decay o aqueous bromine was studied, wit te ollowing results: Kesusutan otokimia bagi bromin akues tela dikaji, dan keputusannya adala seperti berikut: Time min Masa min C Br, ppm Kepekatan Br, ppm /-

4 - - [EKC6] [i] [ii] Determine te reaction order and speciic reaction rate. Tentukan tertib tindakbalas dan kadar tindakbalas tentu. At te steady state condition, calculate te required rate o bromine injected in pounds into a 5, gallon body o water illuminated by te sunligt to maintain a sterilizing level o 1 ppm bromine. Pada keadaan mantap, kirakan bromin yang perlu disuntik dalam paun ke dalam 5, gelen air yang dicaayakan ole mataari bagi mengekalkan paras pensterilan dengan kepekatan bromin sebanyak 1 ppm. 1 gallon.75 litre 1 pound 5 g 1 gelen.75 liter 1 paun 5 g [11 marks/marka] [b] Te eed to a reactor producing dipenyl is pure benzene in te gas pase at a total pressure o 5 atm and 76 C. Te speciic reaction rate is 18 t /lbmol s and te equilibrium constant is estimated to be.. Te reactor volume is 15 dm. At an equilibrium reaction one mole o dipenyl and ydrogen gas are produced. Wat is te equilibrium conversion? Suapan reaktor yang mengasilkan diernil adala merupakan benzena tulen dalam asa gas dengan jumla tekanan 5 atm dan suu 76 C. Kadar tindakbalas tentu adala 18 kaki /lbmol s dan pemalar keseimbangan dianggarkan sebanyak.. Isipadu reaktor adala 15 dm. Tindakbalas adala tindakbalas keseimbangan yang mengasilkan 1 mol diernil dan 1 mol gas idrogen. Apaka penukar keseimbangan? r A k A C A C AC K eq B 1 t.8 m 1 dm.1 m 1 lb.5 kg 1 kaki.8 m 1 dm.1 m 1 lb.5 kg [7 marks/marka] [c] Te catalytic liquid pase decomposition A C k.1 L/mol s is carried out under atmosperic pressure in a batc reactor. Reactant A is carged at.1 mol/l. Determine te duration in days needed to reac 99% conversion in a 1 L vessel. How does your answer cange or a 1 L vessel?...5/-

5 - 5 - [EKC6] Penguraian asa cecair bermangkin A C k.1 L/mol s dijalankan pada tekanan atmosera dalam reaktor kelompok. Baan tindakbalas A disuap pada.1 mol/l. Tentukan tempo dalam ari yang diperlukan untuk mencapai 99% penukaran dalam reaktor 1 L. Bagaimana jawapan anda beruba bagi reaktor 1 L? [7 marks/marka] Section B : Answer any TWO questions. Baagian B : Jawab mana-mana DUA soalan.. [a] Te rate law or ormation o posgene, rom clorine, and carbon monoide, is given as : Hukum kadar bagi pembentukan osgen daripada klorin dan karbon monoksida diberikan seperti berikut: r kc COCl CO C 1.5 Cl Suggest a mecanism or tis reaction tat is consistent wit tis rate law and draw te reaction pat way. [Hint: Cl ormed rom te dissociation o Cl is one o te two active intermediates.] Cadangkan satu mekanisma bagi tindakbalas ini yang konsisten dengan ukum kadar dan lakarkan laluan tindakbalas tersebut. [Panduan: Cl yang terbentuk daripada penceraian Cl merupakan satu daripada dua perantaraan akti.] [1 marks/marka] [b] Te ollowing reversible, elementary, liquid pase reaction occurs in a CSTR: Tindakbalas asas, berbalik, asa cecair yang berikut berlaku dalam sebua CSTR: k A B Te entering low rate is 1 dm /s wit a concentration o M o A and te eed temperature is K. Wat is te reactor volume required in order to acieve 9% o te equilibrium conversion in a CSTR operated adiabatically? Kadar aliran suapan iala 1 dm /s dengan kepekatan M baan A dan suu suapan adala K. Apaka isipadu reaktor yang diperlukan untuk mencapai 9% penukaran keseimbangan dalam sebua CSTR yang beroperasi secara adiabatik? Additional inormation: Speciic eat capacities: C pa C pb 6 cal/mol/k o Heat o reaction: H rn -1, cal/mol A...6/-

6 - 6 - [EKC6] Maklumat tambaan: Haba muatan tentu: C pa C pb 6 cal/mol/k o Haba tindakbalas: H rn -1, cal/mol A Speciic rate constant k and equilibrium rate constant K e is given in Figure Q..[a] and Figure Q..[b]. Pemalar kadar tentu k dan pemalar kadar kesimbangan K e diberikan dalam Raja S..[a]dan Raja S..[b]. Adiabatic energy balance: Imbangan tenaga adiabatik: X [ H Θ C o R i T R P i T T C P i T T R ] [15 marks/marka] k, s -1 Temperature, K Suu, K Figure Q..[a] Raja S..[a]...7/-

7 - 7 - [EKC6] K e Temperature, K Suu, K Figure Q..[b] Raja S..[b] 5. [a] Select te reactor scemes tat will maimize te selectivity S o te desired product, D or te ollowing parallel reactions: Pili skema reaktor yang dapat memaksimakan kememilian S produk yang dikeendaki D bagi tindakbalas selari yang berikut: A B D: r k C C.. D 1 A B 1.5. r U1 kc A CB ru kc A 5 A B U 1 : A U : Wat is te eect i te overall reaction is igly eotermic? Apaka kesannya jika tindakbalas keseluruannya adala sangat eksotermik? [7 marks/marka] [b] Consider te ollowing gas-pase reaction were A is cracked into B and C: Pertimbangkan tindakbalas asa gas yang berikut di mana A dipecakan kepada B dan C: A B C Te reaction is irst order wit respect to A and tat te speciic reaction rate can be epressed by Tindakbalas tersebut adala tertib pertama bagi A dan kadar tindakbalas tentu bole ditentukan dengan ln k,. T...8/-

8 - 8 - [EKC6] Were k is in reciprocal seconds and T is in kelvin. It is required to eed 785 kg o A per r to a tubular reactor. Te reactor consists o 1 o 1-inc tubes. Te reactor is surrounded by a eat ecanger were te eat transer coeicient is 11 J/m.s.K, and te temperature o te eating medium, T a, is constant at 115 K. Te inlet temperature and pressure are at 15 K and 16 kpa, respectively. Given: Molecular weigt o A 58 g/mol Di mana, k dalam unit per saat dan T dalam unit Kelvin. Sebanyak 785 kg A per jam perlu disuapkan ke dalam sebua reaktor tiub. Reaktor tersebut mengandungi 1 tiub berdiameter 1 inci. Reaktor tersebut dikelilingi sebua penukar aba dengan pekali pemindaan aba sebanyak 11 J/m.s.K, dan suu pemanas, T a adala malar pada 115 K. Suu dan tekanan suapan adala masing-masing 15 K dan 16 kpa. Diberi berat molekul A 58 g/mol. [i] [ii] Derive te equations to determine te conversion o A and te temperature as a unction o te lengt o te reactor. Terbitkan persamaan bagi menentukan penukaran A dan suu dalam ungsi panjang reaktor. [1 marks/marka] Te proile o temperature and conversion are plotted as in Figure Q.5. Discuss te proiles. Proil suu dan penukaran A diplotkan dalam Raja S.5. Bincangkan proil tersebut. X T Figure Q.5. Raja S [a] Consider te reactions as below: Pertimbangkan tindakbalas yang berikut: k 1 k A B C V [5 marks/marka]...9/-

9 - 9 - [EKC6] wit k 1.15 s -1 and k. s -1 wit C AO.5 mol/dm. Determine te space velocity, τ tat te reaction need to be carried out in a CSTR in order to obtain te optimal concentration o C. Wat is te optimal concentration o C? dengan k 1.15 s -1 dan k. s -1 dengan C AO.5 mol/dm. Tentukan alaju ruang τ bagi tindakbalas tersebut yang perlu dijalankan dalam sebua CSTR untuk mendapat kepekatan C yang optimal. Apaka kepekatan optimal C? [7 marks/marka] [b] Te low troug a reactor is 1 dm /min. A pulse test gave te ollowing measurements at te outlet: Aliran melalui sebua reaktor adala 1 dm /min. Satu ujian denyutan memberi ukuran yang berikut pada alur keluar: tmin C 1 g/dm tmin C 1 g/dm [i] [ii] Plot te eternal age distribution Et curve as a unction o time. Plotkan lengkuk taburan usia keluar Et dalam ungsi masa. Wat is te mean residence time? Apaka purata untuk masa mastautin? [iii] Wat is te raction o te material wic spent longer tan 15 min in te reactor? Apaka pecaan bagi baan yang tinggal dalam reaktor melebii 15 min? [18 marks/marka] - ooo O ooo

10 - 1 - [EKC6] Appendi Useul dierential equations: d du v d dv u uv d d / v d dv u d du v v u d d umerical Evaluation o Integrals: 1. Trapezoidal rule ] [ 1 1 d wen 1. Simpson s tree-eigts rule ] [ 8 1 d Were ; 1 ; ;. Simpson s quadrature ormula ] [ 1 d Were. For 1 points, were / is an integer, ] [ d Were 5. For 1 points, were is even, ] [ 1 1 d Were.../-

11 [EKC6] Ideal gas constant R 8.1 kpa.dm mol.k R Btu o Ib mol R R.7 t.atm o Ib mol R R 8.1 J mol.k R.8 dm.atm mol.k.8 m.atm kmol.k R 1.987cal mol K.../-

12 - 1 - [EKC6]

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