M T A R E A I L H D D S [3 [ - 3 ] 8 ] M i o le ph e a : t u n : n : , C e P ep r a t a i o st d a d s l o t u i : L e a l l l c i a :

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1 Iri Jr hr srh & viw D 22; 8 : - s rh A ri Ayi M h Dvp Vii r Sis Esii isr ipri i hri Dsg Frs by p-h p *S kr A S K Si S h gsr V i swh V vihir V D pr hri Aysis Sh O hri Sis VISAS Vs Uivrsiy V Vihiyig vr Chi- 67 i Ii A BSAC A br rpi rvrs phs h r sii isr ipri sig UV i ws vp vi sig kri- C8 ODS bi phs psii ws phsph br iri (: w r 7 /i h irig wvgh s ws 2 UV i r i ws s b 8i bs pks r isr ripri wr bsrv r 8 i 37i h h ws vi s pr I CH giis r vris prrs ik Ary Liriy risi bsss ggss LOD LOQ sis h risi Sys Mh wr hk ws b i iis his iis h h is pris Crri ii ws b 999 h r vry v pr rgs wr b bw 98 2 whih iis h h is r s rvs h y s xipis iivs prs i phri ris wr irrig i prps hs h prps yi h pss bh bsss ggss ss O bh ss riv sr vii ws w sisry h prps h b s r ri ysis isr ipri bi ri b sg r i ss i Kywrs: ICH giis rvrs phs r ipri isr iv 6 Sp 22 iv i rvis r O 22 Ap 3 O 22 * Ahr r Crrsp S kr A S K A ssi rssr D pr hri Aysis Sh hri Sis Vs Uivrsiy Chi- 67 i Ii E- i: skskr@gi I NODUCION [ 2] isr: I is hiy 2-( -{ [ - Srk Dh r Crivsr hy-6-( -hy-h- 3-bziz-2- C ss i pp vr g y -2-prpy-H- 3-bziz-- h isry rry h r iss srk y ]hy}phybzi i s r p riphr vsr iss r ibs h yprsi whih h ps prv h bii i- p srks hr ks kiy prbs sg r s r prps h rg wrks by bkig hr h ws b sg r gisi rby rxig b vsss isr ipri i bii w hih y s b s r gsiv Fr irr srvy i ws h r ir h p h kiys pr h r r s yi hs r g ibs rpr r sii isr ipri : I is hiy ( 2S3S6S -- ipri by rvrs phs [(2S-2-{[(2S--hxy--x--phy - h s wrks rpr r b 2y] i} p rpy] - i LC/MS h prps wrk h yry p [ b] pyrr- 2 rbxyi ws i vp br rpi i s r h yprsi rvrs phs h r s isk Myri I ri sii isr ipri S kr A S K IJ 22; 8

2 I ri Jr hr srh & viw D 2 2; ( 8 : - isr ripri M AEIALS AND MEHODS [ 3-8 ] M bi phs: Mix ixr bv I srs : H LC A GILEN - M b r ( NO2 sris Cp Sys Csisig iri ( gs i Kri - C 8 O DS Eri rsi wr bh r is Fir b (SAOIOUS D igi H r hrgh μ ir r v ( OLOMAN S ir (FAS CLEAN iri C his : W r ( H LC Gr ipri rpri sr si: isr ( w rkig sr s Ary wigh rsr g M h ( H LC Gr Orh phsphri i ipri isr wrki g sr i ry vri sk L b i: isr g ipri b 7 i si g issv i py k v p rk s sv (sk M h vp : s i Frr pip ripri B r rpri: W igh 7 gs isr r bv s k K H 2 O i bkr issv s i i vri sk i wr i p rk i A js H 3 rh phsphri i D i prpri: s bi phs s is C hrgrphi iis: F w r : 7 pr i C : k ri -C 8 ODS D r wvg h : 2 C prr : A bi I ji v : 2 μ i : 8 i i i : ipri: 37 isr: 822 A ssy prps h B r prpri: Wigh 7gs K H 2 O i bkr issv i wr Ajs H 3 rh phsphri i M bi phs: Mix ixr bv br ( iri ( gs i rsi wr bh r is Fir hrgh μ ir r v iri rpri sk si: Ar y w igh rsr g ipri isr wrkig sr i ry vri sk b 7 i si issv i py k v p rk s sv (sk s i Frr pip ripri isr bv sk si i vri sk i p h rk i S kr A S K IJ 22; 8 2

3 Iri Jr hr srh & viw D 22; 8 : - D i prpri: s bi phs s i rpri sp rg si r p hri ris: Ary w igh rsr qiv g ipri isr sp i ry vri sk b 7 i si issv i py k v p rk s sv (sk s i F rr pip ripri isr bv sk si i vri sk i p rk i rr r ibri rv: h s bi phs wr ir br s hrgh ir br pp r rspiv sv rsrvirs spii w r rir iji rg sis ws qiibr s 3 i bi phs wig hrgh sys h hrgrphi spri ws hiv sig bi phs sisig b r: iri : ESULS AND DISCUSSION v/v ws ir sig UV r wv gh 2 h ws ii bi prr iji v 2 μ h sr sp sis wr ij i sys g hrgrs h ri i pk r rg ws rr grph ws p by kig ri rg x-xis pk r y- xis A ypi hrgr isr ipri ( wrkig srs ws shw i F i g: w hrs F i g: 2 ws rsig hrgr isr ipri ( i b sg r C i: h rg prs i h phri ri ws by sig sr ibri rv s A yi h vii h yi vii prrs ik ry prisi iriy rg ii i ii qiii rggss wr rig ICH giis rss wr b ( b - b 6 F ig: i i ipri i s 37 isr is 822 b : Ary rss r ipri ri ( spii A r A (g A (g vry M r vry v S kr A S K IJ 22; 8 3

4 Iri Jr hr srh & viw D 22; 8 : - F ig 2: C hrgr isr ipri (i ri b 2: A ry rss r isr ri A A A r ( spii (g (g vry v M r vry 3 b 3 : L iriy S NO C I μg/ sps r ripri sps r isr C rri ii b : S ys s ibiiy rss S NO Chg i rgi psii i h bi phs ss 8 2 A 7 3 r b : L ii i Sys sibiiy rss r r ipri US U S iig US Sys sibiiy rss r isr US iig S NO N i i A r (μv*s H igh (μv ( i ipri isr S kr A S K IJ 22; 8

5 Iri Jr hr srh & viw D 22; 8 : - b 6 : L ii qiii S NO N i i A r (μv*s H igh (μv ( i ipri isr A rss bi wr b i iis rig ICH giis C ONCLUSION - h ws vp vi s pr ICH giis r sii isr ipri h yi h ws vp by s yig ir prrs Firs h xi bsrb ws b 2 pk priy ws x Iji v ws s b 2μ whih gv g pk r h s r sy ws kri C 8 whih gv g pk shp Abi prr ws b sib r r rg si h w r ws ix 7/i bs g pk r sisry ri i Dir ph r is bi phs wr si bi phs ri : ( p hsph b r: iri ws ix g syri pk S his bi phs ws s r prps sy Airi ws s bs xi xri rg pris wr py sb s hw g rvry i ws s b 8 i bs pks r isr ripri wr b r 8 i 3 7 i Ar vp h i ws vi r Ary Liriy risi bsss ggss LOD LOQ s is h risi sys h wr hk r b w ihi h iis his iis h h is pris C rri ii w s b 999 Fr rss s hw i Ary b i ws h rvry vs pr rgs wr bw 98 2 whih iis h h is r s rvs h y s xipis iivs prs i phri ris wr i rrig i prp s h h yi h pss bh bsss ggss ss O bh ss riv sr vii ws w sisry Bs rss bsrv i ws h prps h b s r ri ysis ss isr ipri bi b sg r EFEENCES UL: w wwrgbkisr 2 UL: wwwrgbkripri 3 K r V i M G G - Esii ipri isr i bs I i J hr Si 29; 72 : 8- jkr B riyk M Sbrhy KV Sy MA kshy rsgr Sis Drii Vii isr ipri i hr i Dsg Fr by HLC Chis-Jr-- hri-a ysis 2;2(2:2-22 ra DC Shikr KL S hikr B S rvkr M hirrhy A Nw - Mh D vp Vii r Sis sii isr igiz i hri D sg Fr J phr Ch s 2;3(: 8-6 S i Jw Jykshi K Krishrhy Kr Y Dvp Vii Sis h r E sii isr ipri i hri Fris IJ hrh s 2;2(2 : K y Kr B Shsh Kr S hrv Kr A V kshwr Dvp Vii - M h r Sis Esii ipri isr Hyrhrhizi i hri D sg F rs Jr hry srh 2;( 8 K ir i V ip J iprksh N S gshi D v B S hi A Sbiiy- Iiig LC Mh r Sis Drii isr ipri i Dsg Fr CHOMAOGAHIA ( 67: 7-82 S kr A S K IJ 22; 8

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