N o.:ce/2014/c5460 Date:2015/01/05 Page:2of19 Test Resu lt(s) PART N AM E N o.1 : SIL V ER COL ORED M ETAL W IRE (IN CL UDIN G TH E PL ATIN G L AYER)

Transcription

1 N o.:c E/2014/C 5460 D ate:2015/01/05 P age:1of19 Thefollowingsam ple(s)was/weresu bm ittedandidentifiedby/on behalfoftheapplicant as : Sam pledescription Style/Item N o. Sam plereceivingdate TestingPeriod : : : : Cu B ON DIN G W IRE COPPER W IRE (EX1) 2014/12/ /12/26 T O 2015/01/05 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = Test Resu lt(s) : Pleaserefertonextpage(s).

2 N o.:ce/2014/c5460 Date:2015/01/05 Page:2of19 Test Resu lt(s) PART N AM E N o.1 : SIL V ER COL ORED M ETAL W IRE (IN CL UDIN G TH E PL ATIN G L AYER) Cadm ium (Cd) L ead(pb) M ercury(h g) H exavalentchrom ium Cr(V I) Antim ony(sb) B eryllium (B e) PV C Test Item (s) PolychlorinatedB iphenyls (PCB s) (CAS N o.: ) P olychlorinated N aphthalene (PCN s) P olychlorinated T erphenyls (PCTs) A lkanes,c 10-13,chloro(S hort Chain ChlorinatedParafins)(CAS N o.: ) Unit Method m g/kg W ithreferencetoiec :2013 andperform edbyicp-aes. m g/kg W ithreferencetoiec :2013 andperform edbyicp-aes. m g/kg W ithreferencetoiec :2013 andperform edbyicp-aes. ** W ithreferencetoiec 62321:2008and perform ed by B oiling w aterextraction M ethod.# m g/kg W ithreferencetoiec 62321:2008and perform edbyuv -V IS. m g/kg W ithreferencetous EPA M ethod 3052.Analysis was perform edbyicp- AES. m g/kg W ithreferencetous EPA M ethod 3050B.Analysis was perform edby ICP-AES. ** Analysis was perform edbyftir and FL AM E Test. m g/kg W ithreferencetous EPA 3540C m ethod.analysis was perform edby GC/M S. m g/kg W ithreferencetous EPA 3540C m ethod.analysis was perform edby GC/M S. m g/kg W ithreferencetous EPA 3540C m ethod.analysis was perform edby GC/M S. m g/kg W ithreferencetous EPA 3540C m ethod.analysis was perform edby GC/M S. Resu lt MDL N o.1 2 n.d. 2 n.d. 2 n.d. # N egative 2 n.d. 2 n.d. 2 n.d. - N egative 0.5 n.d. 5 n.d. 0.5 n.d. 100 n.d.

3 N o.:ce/2014/c5460 Date:2015/01/05 Page:3of19 Test Item (s) Unit Method MDL H exabrom ocyclododecane (H B CDD)andallm ajor dias tereois om ers identified (α- H B CDD, β- H B CDD, γ- H B CDD) (CAS N o.: and ( , , )) Perfluorooctanesulfonates (PFOS-Acid,M etalsalt,am ide) PFOA (CAS N o.: ) B B P (B utylb enzylphthalate) (CAS N o.: ) DEH P (Di-(2-ethylhexyl) phthalate)(cas N o.: ) DIDP (Di-isodecylphthalate)(CAS N o.: ; ) DIN P (Di-isononylphthalate)(CAS N o.: ; ) DN OP (Di-n-octylphthalate)(CAS N o.: ) DB P (Dibutylphthalate)(CAS N o.: ) DIB P (Di-isobutylphthalate)(CAS N o.: ) Organic-tin com pou nds TributylTin (TB T) TriphenylTin (TphT) DibutylTin (DB T) DioctylTin (DOT) TributylTin Oxide(TB TO)***(CAS N o.: ) m g/kg W ithreferencetoiec 62321:2008 m ethod.analysis was perform edby GC/M S. m g/kg W ithreferencetous EPA 3550C: 2007.Analysis was perform edby L C/M S. m g/kg W ithreferencetous EPA 3550C: 2007.Analysis was perform edby L C/M S. % W ithreferencetoen Analysis was perform edbygc/m S. % W ithreferencetoen Analysis was perform edbygc/m S. % W ithreferencetoen Analysis was perform edbygc/m S. % W ithreferencetoen Analysis was perform edbygc/m S. % W ithreferencetoen Analysis was perform edbygc/m S. % W ithreferencetoen Analysis was perform edbygc/m S. % W ithreferencetoen Analysis was perform edbygc/m S. Resu lt N o.1 5 n.d. 10 n.d. 10 n.d n.d n.d n.d n.d n.d n.d n.d. m g/kg 0.03 n.d. m g/kg 0.03 n.d. m g/kg W ithreferencetoiso17353.analysis 0.03 n.d. m g/kg was perform edbygc/fpd n.d. m g/kg - n.d.

4 N o.:ce/2014/c5460 Date:2015/01/05 Page:4of19 Resu lt N o.1 m g/kg - n.d. m g/kg W ithreferencetoiec 62321:2008and 5 n.d. m g/kg perform edbygc/m S. - n.d. Test Item (s) Unit Method MDL Su m ofpb B s M onobrom obiphenyl D ibrom obiphenyl T ribrom obiphenyl T etrabrom obiphenyl P entabrom obiphenyl H exabrom obiphenyl H eptabrom obiphenyl Octabrom obiphenyl N onabrom obiphenyl D ecabrom obiphenyl Su m ofpb DEs M onobrom odiphenylether D ibrom odiphenylether T ribrom odiphenylether T etrabrom odiphenylether P entabrom odiphenylether H exabrom odiphenylether H eptabrom odiphenylether Octabrom odiphenylether N onabrom odiphenylether D ecabrom odiphenylether H alogen H alogen-fluorine(f)(cas N o.: ) H alogen-chlorine(cl)(cas N o.: ) H alogen-b rom ine(b r)(cas N o.: ) H alogen-iodine(i)(cas N o.: ) m g/kg 50 n.d. m g/kg 50 n.d. W ithreferencetob S EN 14582:2007. m g/kg Analysis was perform edbyic. 50 n.d. m g/kg 50 n.d.

5 N o.:ce/2014/c5460 Date:2015/01/05 Page:5of19 N ote: 1. m g/kg= ppm ;0.1wt% = 1000ppm 2. n.d.= N ot D etected 3. M DL = M ethoddetection L im it 4. "-"= N otregulated 5. **= Qualitativeanalysis (N ounit) 6. N egative= Undetectable/Positive= Detectable 7. #= a.positivem eans thepresenceofcrv Ion thetestedareas b.n egativem eans theabsenceofcrv Ion thetestedareas Thedetectedconcentration in boiling-water-extraction solution is equalorgreaterthan 0.02m g/kgwith50cm ² testedareas. 8. ***:Thesubstancewas calculatedbythetestresultoftributyltin.them DL was evaluatedfortributyltin. 9. Param eterconversion Table:Pleaserefertohttp:/twap.sgs.com /sgsrsts/chn/download-reach _tw.asp 10. Thesam ple(s)was/wereanalyzedon behalfoftheapplicant as m ixingsam plein onetesting.theaboveresult(s)was/were onlygiven as theinform alityvalue. PFOS R eference Inform ation :POPs -(E U)757/2010 OutlawingPFOS as substances orpreparations in concentrations above0.001% (10ppm ),in sem i-finished products orarticles orparts atalevelabove0.1%(1000ppm ),in textiles orothercoatedm aterials above1µ g/m ².

6 N o.:ce/2014/c5460 Date:2015/01/05 Page:6of19 1) T hesesamples weredissolvedtotalybypre-conditioningmethodaccordingtobelow flow chart. (Cr 6+ testmethodexcluded) 2) N ameoftheperson whom adem easurem ent:clim bgreatyang 3) N ameoftheperson in chargeofmeasurem ent:troychang C u tting/preparation SampleM easurem ent Pb Cd Aciddigestion bysuitableacid dependedon diferentsample m aterial(as below table) H g M icrowavedigestion with H N O 3 /H Cl/H F Cr 6+ (N ote**) Addappropriateamount ofdiges tion reagent Filtration Solu tion ICP-AES Sam plem aterial Residu e 1) AlkaliFusion 2) H Cltodissolve D iges tion Acid H eat to appropriate tem peratu reto extract C ool,filterdiges tate throu gh filter A dd diphenyl-carbazide forcolordev elopm ent Steel,copper,alum inum,solder Aqu aregia,h N O 3,H Cl,H F,H 2 O 2 Glass H N O 3 /H F Gold,platinum,paladium,ceram ic Aqu aregia Silver H N O 3 Plastic Others H 2 SO 4,H 2 O 2,H N O 3,H Cl Added appropriatereagent to total diges tion m easuretheabsorbance at540nm byuv -V IS N ote**(foriec 62321) (1)Fornon-m eta licm aterial,add alkaline diges tion reagent and heat to 90~95. (2)Form eta licm aterial,add pu re w aterand heat to boiling.

7 N o.:ce/2014/c5460 Date:2015/01/05 Page:7of19 1) T hesesamples weredissolvedtotalybypre-conditioningm ethodaccordingtobelow flow chart. 2) N ameoftheperson whom adem easurement:clim bgreatyang 3) N ameoftheperson in chargeofmeasurement:troychang Flow Chart ofdigestion fortheelem ents analysis perform edbyicp-aes C u tting/preparation SampleM easurem ent Aciddigestion bysuitableaciddependedon diferent s am plem aterial(as below table) Filtration Solu tion Residue 1) AlkaliFusion 2) H Cltodissolve ICP-AES Steel,copper,aluminum,solder Aquaregia,H N O 3,H Cl,H F,H 2 O 2 Glass Gold,platinum,paladium,ceramic H N O 3 /H F Aquaregia Silver H N O 3 Plastic Others H 2 SO 4,H 2 O 2,H N O 3,H Cl A dded appropriate reagent to totaldiges tion

8 N o.:ce/2014/c5460 Date:2015/01/05 Page:8of19 Analysis flow chart fordeterm ination ofpv C in m aterial N am eoftheperson whomademeasurem ent:royl in N am eoftheperson in chargeofm easurem ent:t roychang S am plepre-treatm ent Flametest SampleanalyzedbyFT IR Checkwave-num berofc-clbonding Data

9 N o.:ce/2014/c5460 Date:2015/01/05 Page:9of19 PC B s analyticalflow chart N ameoftheperson whom adem easurement:b arrytseng N ameoftheperson in chargeofmeasurement:troychang S am plepretreatm ent Sampleextraction byorganicsolvent Concentrate/Dilutetheextractedsolution Analysis was perform edbygc/m S Data

10 N o.:ce/2014/c5460 Date:2015/01/05 Page:10of19 PC N s analyticalflow chart N ameoftheperson whom adem easurement:b arrytseng N ameoftheperson in chargeofmeasurement:troychang S am plepretreatm ent Sampleextraction byorganicsolvent Concentrate/Dilutetheextractedsolution Analysis was perform edbygc/m S Data

11 N o.:ce/2014/c5460 Date:2015/01/05 Page:11of19 PC T s analyticalflow chart N ameoftheperson whom adem easurement:b arrytseng N ameoftheperson in chargeofmeasurement:troychang S am plepretreatm ent Sampleextraction byorganicsolvent Concentrate/Dilutetheextractedsolution Analysis was perform edbygc/m S Data

12 N o.:ce/2014/c5460 Date:2015/01/05 Page:12of19 C hlorinated Paraffins analyticalflow chart N am eoftheperson whomademeasurem ent:b arrytseng N am eoftheperson in chargeofm easurem ent:troychang Sam plepretreatm ent Sam pleextraction by organics olv ent Concentrate/Dilutetheextractedsolution Analysis was performedbygc/m S Data

13 N o.:ce/2014/c5460 Date:2015/01/05 Page:13of19 H B CDD analyticalflow chart N am eoftheperson whomademeasurement:roman W ong N am eoftheperson in chargeofm easurement:troychang Samplepretreatm ent Sampleextraction /Ultrasonicm ethod Concentrate/DiluteExtractedsolu tion Filter Analysis was performedbygc/m S Data

14 N o.:ce/2014/c5460 Date:2015/01/05 Page:14of19 PFOA/PFOS analyticalflow chart ofu ltras onic extraction (L C/M S)procedu re N am eoftheperson whomademeasurem ent:rom an W ong N am eoftheperson in chargeofm easurem ent:troychang Sam plepretreatm ent S am ple extraction by U ltras onicextraction (Referencemethod:US EPA 3550C) Concentrate/DiluteExtractedsolution Analysis was perform edbyl C/M S Data

15 N o.:ce/2014/c5460 Date:2015/01/05 Page:15of19 A nalyticalflow chart ofphthalate content N am eoftheperson whomademeasurem ent:rom an W ong N am eoftheperson in chargeofm easurem ent:troychang S am plepretreatm ent/s eparation Sampleextraction bysoxhletmethod Concentrate/DiluteExtractedsolu tion Analysis was perform edbygc/m S Data

16 N o.:ce/2014/c5460 Date:2015/01/05 Page:16of19 A nalyticalflow chart oforganic-t in content N am eoftheperson whomademeasurem ent:royl in N am eoftheperson in chargeofm easurem ent:troychang S am plepretreatm ent Sampleextraction byorganicsolvent D eriv ed by S odiu m tetraethylborate Concentrate/DiluteExtractedsolu tion Analysis was performedbygc/fpd Data

17 N o.:ce/2014/c5460 Date:2015/01/05 Page:17of19 PB B /PB DE analyticalfl OW CH ART N ameoftheperson whom adem easurement:rom an W ong N ameoftheperson in chargeofmeasurement:t roychang Firsttestingprocess Optionals creen proces s Confirmation process Sam ple S am plepretreatm ent Screen analysis S am pleextraction/ Soxhlet m ethod C oncentrate/d ilu te Extractedsolution Filter Analysis bygc/m S IssueReport

18 N o.:ce/2014/c5460 Date:2015/01/05 Page:18of19 A nalyticalflow chart ofhalogen content N ameoftheperson whom adem easurement:ritachen N ameoftheperson in chargeofmeasurement:t roychang Sam plepretreatm ent/s eparation W eightingandputtingsam plein cel Oxygen B ombcombustion /Absorption Dilution tofixedvolume Analysis was perform edbyic

19 N o.:ce/2014/c5460 Date:2015/01/05 Page:19of19 *Thetestedsam ple/part is m arkedbyan arrow ifit's shown on thephoto.* **EndofReport **