J. Am. Chem. Soc., 1997, 119(41), , DOI: /ja964223u
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1 J. Am. Chem. Soc., 1997, 119(41), , DOI:1.121/ja964223u Terms & Conditions Electronic Supporting Information files are available without a subscription to ACS Web Editions. The American Chemical Society holds a copyright ownership interest in any copyrightable Supporting Information. Files available from the ACS website may be downloaded for personal use only. Users are not otherwise permitted to reproduce, republish, redistribute, or sell any Supporting Information from the ACS website, either in whole or in part, in either machinereadable form or any other form without permission from the American Chemical Society. For permission to reproduce, republish and redistribute this material, requesters must process their own requests via the RightsLink permission system. Information about how to use the RightsLink permission system can be found at Copyright 1997 American Chemical Society
2 PWRKIN ELMER / ~;:z" 61 u I to ) to CD N 1 O. CID Cl) 1 CD '.4.~J. Co ~-1 '.4 Cu Cu C cm'1 96/5/15 21: 59 X: 4 scans, 2.cm-1, flat, smooth
3 GZ-III-3-7 BR K4F. 3 AU PROG: XOO.AU DATE TIME 14: 21 N ":~ ( SOLVENT CDC13 SF SY SI TD SW HZ/PT.184 AG 2.72 RG 1 TE 297 FM OP 63L DO LB.9 GB.5 CX 35. CY 2. Fi 9.2P F2 -.8OOP HZ/CM PPM/CM.286 SR Di 1. PO 5. RGA RD. PM. DE 13.8 DS 5.1 NE PPM
4 z T r a n B 8 t a n C B Wavenumbers (cm-)
5 GZ-III-281 B R ML15F. 125 AU PROG: X.AU DATE 15-B-96 TIME 19: 16 SOLVENT CDC13 SF SY SI TO SW HZ/PT.184 AG 2.72 RG 8 TE 297 FM DP 63L PO LB.18 GB. CX 35. CY 2. Fi F2 9.2P -.BOOP HZ/CM PPM/CM.286 SR Di i. PO 7.2 RGA RD. PW. DE 13.8 DS D5.1 NE I 9. B PPM 1.
6 PERKIN ELMER % T 16/ p 1.35 I /4/15 18: 14 X: 8 scans, 4.cm-1, cm' flat, smooth
7 Z-III-217N 4.4,19 Z i MI15OF.138 AU PROG: XOO.AU DATE d TIME 22: 12 SOLVENT CDC13 SF i SI TD SW HZ/PT.368 BRR AG 2.72 RG 32 TE 297 FW OP 63L PO LB.18 GB. CX 35. CY 2. Fl 9.21P F P HZ/CM PPM/CM.286 SR PA RD RGA. 7.2 PW. DE 13.8 DS DS.1 NE 1 I. ITI I T I T -- T- T-1T - 9. B. L.... ( 1. (.
8 PERK IN ELJ ER AlJ Tif4 jrvltl 4. (3 Cu C CD CO N to1 to *3 C~u, ID 1 ID ~1 u '.1 CD /6/7 21: 22 X: 4 scans, 4.cm-i. Cu r 3 25 flat, smooth I ~1 cm'
9 ft q / BSR KTi7F.112 AU PROG: XOO.AU DATE TIME 13: 1 FA / C OC4,2 SOLVENT [EfW SF SY SI TD SW HZ/PT.368 AG 2.72 RG 2 NS TE FW OP 63L LB.9 GB.5 CX 35. CY 3. Fl 12.P F P HZ/CM PPM/CM.366 SR D1 1. PO 5. RGA RD. PW. DE 13.8 DS D5.1 NE I I-. 6. PPM
10 ERK IN ELMER CiIA CO C' t~om to-. VI) to 1 * a, M: t) (11 C,, to 1 CD F /6/8 9: 54 X: 4 scans, 4.cm-i. flat, smooth 2 i~oo Cur'
11 UZ-IV-6i B R KT17F.12 AU PROG: XOO.AU DATE TIME 14: 22 -j-fa/icrc SOLVENT AuSM SF SY oo SI TD SW HZ/PT.368 AG 2.72 RG 2 TE 297 FW DP 63L LB.9 GB.5 CX 35. CY 2. Fi 14.21P F P HZ/CM PPM/CM.429 SR Di 1. PO 5. RGA RD. PW. DE 13.8 DS DS.1 NE i i /. b PPM
12 P.E3KIN ELE J %T 'I _ d14 j2 r) L*fl1 In Mv M' M'- "'C In r-.m 1OO t- IV C') 1 ) N Mv wt1 (f~ cm- 1 96/5/2 14: 26 X: 4 scans. 4.cm-i, flat, smooth
13 GZ-IV-63 B R L I,' KT17F.Hi AU PROG: XOO.AU DATE TIME 12: 51 SOLVENT dew SF SY SI TD SW HZ/PT.368 AG 2.72 RG 2 TE 297 FW DP 63L DO LB.9 GB.5 CX 35. CY. Fi 12.OOOP F P HZ/CM PPM/CM.366 SR D1 1. PO 5. RGA RD. PW. DE 13.8 DS 5.1 NE PPM
14 lv2- - (FO ~ '-I It U, to rl. j L xj Cu (Ir to,ri (O Cu F, ; I Cr) :boo 1 cm~ 96/5,'28 12: X: 4 scans, 27 4.Ocm-1, flat, smooth
15 GZ-IV A4 3 B R K4F.129 AU PROG: XOO.AU DATE TIME 14: 14 C SOLVENT CDC13 SF SY SI TO SW O HZ/PT.184 AG 2.72 RG 1 TE 297 FM DP 63L DO LB.9 GB.5 CX 35. CY 2. Fi 9.2P F2 -. 8OP HZ/CM < PPM/CM.286 SR Di 1. PO 5. RGA RD. PW. DE 13.8 DS D5.± NE I PPM
16 PERKIN ELMER 3.77 %T 1% 'a Co Cu Cli avv rm I I CDn to aa Eo N ) Cu to ZZ3 to a) O) CD U ) 18.33± /6/8 17: 3 X: 4 scans, 4.cm-i, flat, smooth cm-1
17 Filename: M497JUn24_12:18 U8C Mercury 4 STANDARD 1 OBBERVE Qz-III-224 I expl stdh ganpha cc. date Jun dfrg solvent CDC13 da file exp dpwr ACQUISITION dof sfrq di tol E1 dam at daf up 384 P sw tfil tb 36 proc be 16 fn tpwr 55 pw 7.7 werr di 1. Vexp tof wbm nt 16 Mt at 16 alock n gain 22 FLAGS 11 ni in n y DISPLAT sp -8. VP Vs 586 so wa 25 him in 5. rfl 78.5 rfy th 17 inn 1. al cdc ph & VT m1 4 ROCZSIG a 14 ft not used react glidevexp ~%' I; < m
18 P'ERKIN ELER %T *-b # OD * Wctil N* Cu Co WI CD In vi1 CI ED N (f~ cm~ 97/4/9 14: 11 X: 4 scans, 4.cm-1, flat, smooth
19 -s GZ (/D B8R KTOBOF.125 AU PROG: XOO.AU DATE TIME 19: 55 SOLVENT CDC13 SF SY SI TO SW HZ/PT.184 AG 2.72 RG 8 TE 297 FM 76 2 DP L LB.9 GB.5 CX 35. CY 2. F1 9.2P F2 -.8P HZ/CM PPM/CM.286 SR D1 1. PO 5. RGA RD PM.. DE 13.8 Ds 5.1 NE I 7. I I I I I I I I I I I II~I PPM 1 IiII I j I I I I 1..
20 PEMCIN ELMER cm 97/3/6 2* 58 X 4 scans, 4.cm-i. flat, smooth
21 GZ- BS R SHOF.118 AU PROG: XOO.AU DATE TIME 21: 29 SOLVENT COC13 SF SY SI TD SW HZ/PT.184 AG 2.72 RG 1 / B TE 297 FM 76 2 DP L DO LB.9 GB.5 CX 35. CY 2. Fi 9.2P F2 -.8OOP HZ/CM PPM/CM.286 SR PO 5. RGA RD. PM DE OS D NE I PPM
22 /3/13 14: 55 Y: 4 scans, 4.Cm-1, 3 25 flat, smooth cm-1
23 V B8R N7> KSIOOF 118 AU PROG: XOO.AU DATE TIME 21: 13 SOLVENT CDC13 SF SY SI TD SW HZ/PT.184 AG 2.72 RG 2 TE 297 FW DP 63L DO LB.9 GB.5 CX 35. CY 2. Fi 9.2P F2 -.8P HZ/CM PPM/CM.286 SR Di 1. PO 5. RGA RD. PW. DE 13.8 DS 5.1 NE I PPM 1..
24 psitin amiv 22 4 aeo 97/2/27 19: 17 X* 4 scans, 4.cm-1i. flat. smooth soo I 1 co-'
25 Gz-Iv- B R kr2if.11 AU PROG: XOO.AU DATE TIME ±1: 7 SOLVENT Other SF SY SI TD SW HZ/PT.184 AG 2.72 RG 4 TE 297 FM 76 2 DP L DO TEA LB GB.9.5 CX 35. CY 2. F1 12.OOOP F P HZ/CM PPM/CM.366 SR Di 1. PO 5. AGA RD. PM. DE 13.8 DS 5.1 NE PPM.
26 -1FawN JER U'- ~ I J- pi",la A a,,/ %T /1-, / N N ~1 ti~ C ~1 eu aie Nu cc PI vi i CD~ eo 97/3/3 It 31 X: 4 scans. 4.cm-1. s1oo flat, smooth aooo 15 1 cm-
27 GZ-IV-125,- KR2iOF. 16 AU PROG: XOO.AU DATE TIME 19:4 SOLVENT COC13 SF SY ioo.o SI TD SW HZ/PT.184 AG 2.72 RG 4 TE 297 FW 76 <, 2 OP L LB.9 GB.5 CX 35. CY 2. Fi 9.2P F2 -.8P HZ/CM PPM/CM.286 SR Di PO i. 5. RGA RD PW.. DE 13.8 DS D5.1 NE A PPM / , IIZ
28 TJR"IN ET lvf AP -7, C) U) to at) -Cu w tf) cn Cu Cx I- -,-- 4C 35 31,1 rico 1 crln- 9.16/1-18 O:? KL. ~.3t, smcoth smcot"
29 GZ-IV-198 B R C)- D KViOOF. 2 AU PRO: XOO.AU DATE TIME 19: 44 SOLVENT CDC13 SF SY 1oo SI TO SW HZ/PT.184 AG 2.72 RG 32 TE 297,r FW OP 63L DO LB.9 GB.5 CX 35. CY 2. Fi 9.2P F2 -.BOOP HZ/CM PPM/CM.286 SR /I Di i. PO 5. RGA RD. PW. DE 13.8 Os 5.1 NE I cc (D z PPM 1..
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