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1 Hier rcpe ppt header Large 01.emf platzieren Analytical Equipment Research Center Pharmaceutical Engineering GmbH (RCPE) K1 Competence Center - Initiated by the Federal Ministry of Transport, Innovation and Technology (BMVIT) and the Federal Ministry of Science, Research and Economy (BMWFW). Funded by the Austrian Research Promotion Agency (FFG), Land Steiermark and the Styrian Business Promotion Agency (SFG).
2 Overview Analytical Services I Particle Size Laser Diffraction HELOS KR (Sympatec) Particle Size Laser Diffraction Mastersizer 2000 (Malvern) Particle Size & Shape Dynamic Picture Analysis QICPIC (Sympatec) Particle Size Dynamic Light Scattering Nano ZS (Malvern)
3 Overview Analytical Services II Density Gas Pressure Differential AccuPyc 1340 Helium Pyknometer (Micromeritics) (Compacted) Bulk Density Volume Change of Bulk Powder PT-TD200 (Pharmatest) Flow Properties / Fluidisation Segregation / Cohesion / Friction Angle Normal Force, Shear Strength and Torque FT4 Powder Rheometer System (FreemanTechnology) Particle Size and Shape in Fluid Dispersion Flow-Through Microscopy MFI 5100 (Protein Simple)
4 Overview Analytical Services III Zeta Potential Laser Doppler Micro- Electrophoresis Nano ZS (Malvern) Dissolution Rate / in vitro Drug Release Information Dissolution Apparatus USP 1 (Basket) and USP 2 (Paddle) / UV Spectrophotometer DT820LH (Erweka) + UV/ViS Lambda 25 (Perkin Elmer) Friability Exposure of Tablets to Mechanical Shock and Attrition PTF10E (PharmaTest) Density / Velocity of Sound Oscillating U-tube Sensor DSA 5000 M (Anton Paar)
5 Overview Analytical Services IV Specific Surface / Porosity Specific Surface / Porosity Gas Adsorption Krypton / Nitrogen, BET (Brunauer Emmett Teller) theory Gas Adsorption Nitrogen, BET (Brunauer Emmett Teller) theory Tristar II 3020 (Micromeritics) ASAP 2000 (Micromeritics) Structure / Polymorphism / Inner Surface Small and Wide Angle X-Ray Scattering (SWAXS) S3-Micro SWAXS (Hecus/Bruker) Secondary Protein Structure / Extruder Residence Time Raman Scattering (Flexible Process Probe) RXN2 Hybrid (Kaiser Optics)
6 Overview Analytical Services V Concentration /Enzyme Kinetics UV/VIS Spectroscopy (Transmission, Absorption) Lambda 950 (Perkin Elmer) Concentration / Reaction Kinetics Fourier Transform IR/Near-IR Spectroscopy (Transmission, Absorption, Diffuse Reflection) Spectrum 400 (PerkinElmer) Concentration / Polymorphism / Surface Mapping Raman Scattering (Scan Stage, Flexible Probe) RamanStation 400 (PerkinElmer) Concentration / Reaction Kinetics In-line Near-IR Spectroscopy (Diffuse Reflection) SentroPAT FO (Sentronic), Probes: DR LS 300 (Dynisco)
7 Overview Analytical Services VI Concentration Seperation via Ultra-High Pressure Liquid Chromatography Acquity UPLC + MS ( Waters) Concentration Seperation via Liquid Chromatography / Photo Diode Array Detector Agilent 1260 HPLC + PDA (Agilent) Identification of Substances Triple- Quad Mass Spectroscopy Alliance HPLC + MS (Waters) Concentration Seperation via Gas Chromatography Clarus500 (PerkinElmer)
8 Overview Analytical Services VII Contact Angle / Surface Tension Sessile Drop and Captive Bubble Method (Static & Dynamic) Easydrop (Krüss) Contact Angle / Surface Tension Washburn Method for Powders / Sessile Drop and Captive Bubble KT100 (Krüss) Nanoparticle Inclusion Spray Drying (Piezoelectric Pulverizer) Nano Spray Dryer B-90 (Büchi) Residual Moisture Content Karl Fischer Titration TitroLine 7500 KF (SI Analytics )
9 Overview Analytical Services VIII Particle Shape / Imaging Microscopy DM4000 with DFC290 Camera (Leica) Weight (Precision 0.01 mg) High Precision Scale XP205DR /m (Mettler Toledo) Characterize Flow of Materials / Elasticity EC Motor Drive with Normal Force and Torque Sensor Physica MCR 300 (Anton Paar) Transformation Enthalpies / Specific Heat Differential Scanning Calorimetry DSC 204 F1 Phönix (Netzsch)
10 Overview Analytical Services IX Particle Separation due to differences in their size, shape, or density Sifting Segregation Jenike & Johanson Segregation Tester SS1 Testing of inhaled products, measuring the aerodynamic particle size distribution Inertial Impaction Copley Scientific Cascade Impactor Raman microscopy with Hot Stage Option observe vibrational, rotational, and other low-frequency modes Bruker Senterra Raman Microscope
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