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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2016/ 2017 ACADEMIC SESSION 2016/ 2017 : SEMESTER I : SEMESTER I SCES 3314 : KIMIA BAHAN MATERIAL CHEMISTRY Dis 2016/Jan 2017 Dec 2016/ Jan 2017 Masa: 2 jam Time: 2 hours ARAHAN KEPADA CALON: INSTRUCTION TO CANDIDATES: Jawab SEMUA soalan. Answer ALL questions. (Kertas soalan ini mengandungi 4 soalan dalam 7 halaman yang dicetak) (This question paper consists of 4 questions on 7 printed pages)

2 BAHAGIAN A (50 MARKAH) SECTION A (50 MARKS) Jawab SEMUA soalan. Answer ALL questions. 1. (a) Mikroskop imbasan elektron (SEM) adalah sejenis mikroskop elektron yang menghasilkan imej sampel dengan cara pengkhususan imbasan elektron. Dengan bantuan gambar rajah di bawah, huraikan dengan lengkap prosedur mikroskop imbasan elektron tersebut. A scanning electron microscope (SEM) is a type of electron microscope that produces images of a sample by scanning it with a focused beam of electrons. With aid of the diagram below, describe in detail the scanning electron microscope procedure. (10 markah/marks) (b) Analisis terma berbeza (DTA) adalah teknik untuk mengenal pasti dan menganalisis kuantitatif komposisi kimia bahan dengan memerhati tingkah laku haba sampel apabila ia dipanaskan. DTA melibatkan pemanasan atau penyejukan sampel ujian dan rujukan lengai di bawah keadaan yang sama, sambil merakam sebarang perbezaan suhu antara sampel dan rujukan. Diberi takat lebur 2/7

3 aluminium tulen adalah 660 C. Lakarkan lengkung penyejukan aluminium tulen apabila ia disejukkan dari 750 C. Bagaimana ia akan kelihatan? Differential thermal analysis (DTA) is a technique for identifying and quantitatively analyzing the chemical composition of substances by observing the thermal behaviour of a sample as it is heated. DTA involves heating or cooling a test sample and an inert reference under identical conditions, while recording any temperature difference between the sample and reference. Sketch the cooling curve of pure aluminium as it is cooled from 750 C. Given the melting point of pure aluminium is 660 C. How would the DTA plot look like? (5 markah/marks) (c) Kompleks Cu(II) dengan formula [Cu(C 16 H 10 N 5 O) 2 ] mempamerkan dua langkah penguraian berbeza dalam julat suhu C. Langkah pertama dengan julat suhu C dan kehilangan jisim adalah 10.33% yang mana dikaitkan dengan pembebasan molekul C 7 H 5 N 2. Dalam langkah kedua pula, keluk Pengimbasan Pembezaan Kalorimeter (DSC) mendedahkan puncak endotermik pada suhu 120 C diikuti oleh satu puncak eksotermik berturut-turut pada suhu 380 C. Ini mungkin disebabkan daripada penguraian rancak molekul yang dikaji meninggalkan CuO sebagai sisa logam. Lakarkan keluk analisis terma gravimetrik (TG) dan pengimbasan pembezaan kalorimeter (DSC) berdasarkan huraian ini. Cu(II) complex with the formula of [Cu(C 16 H 10 N 5 O) 2 ] exhibits two distinct decomposition steps in the temperature range of C. The first step with temperature range of C and calculated mass loss is 10.33% may be attributed to the liberation of C 7 H 5 N 2 molecule. In the second step, Differential Scanning Calorimetry (DSC) curve reveals an endothermic peak at 120 C followed by one successive exothermic peak at 380 C. This may be accounted to the vigorous decomposition of the studied molecule leaving CuO as a metallic residue. Sketch the thermal gravimetric analysis (TG) and differential scanning calorimetry (DSC) curves based on these description. (5 markah/marks) (d) Berikan sebab mengapa corak serakan sinar-x adalah dalam bentuk spektrum dan bukan berupa imej sebenar seperti yang terhasil dari mikroskop elektron. Give reasons why x-ray scattering pattern is in the form of spectrum and not an actual image produced by electron microscope as for example. (3 markah/marks) 3/7

4 (e) Dalam ketiga-tiga jenis serakan Raman, satu foton tenaga terserak menaikkan molekul daripada keadaan getaran kepada keadaan maya yang terletak di antara dasar dan aras elektronik pertama. Jenis serakan terlihat adalah bergantung kepada bagaimana molekul direhatkan selepas pengujaan. Jelaskan semua jenis serakan yang dimaksudkan dengan menggunakan gambarajah dan penerangan. In all three types of Raman scattering, an incident photon of energy raises the molecule from a vibrational state to one of the infinite number of virtual states located between the ground and first electronic states. The type of scattering observed is dependent on how the molecule relaxes after excitation. Describe all type of scattering using diagrams and detailed descriptions. (13 markah/marks) (f) Tetrametilsilan (TMS) adalah piawaian dalaman yang diterima untuk menentukur anjakan kimia untuk 1 H, 13 C dan 29 Si spektroskopi resonan magnetik nuklear (NMR) dalam pelarut organik (di mana TMS terlarut). Rasionalkan penggunaan TMS dalam NMR. Tetramethylsilane is the accepted internal standard for calibrating chemical shift for 1 H, 13 C and 29 Si nuclear magnetic resonance spectroscopy (NMR) spectroscopy in organic solvents (where TMS is soluble). Rationalize the usage of TMS in NMR. (6 markah/marks) (g) Analisis spektroskopi sinar-x fotoelektron (XPS) adalah teknik analisis permukaan yang paling banyak digunakan. Terangkan dengan memberikan satu contoh bagaimana XPS boleh digunakan dalam analisis sampel. X-ray Photoelectron Spectroscopy (XPS) analysis is the most widely used surface analysis technique. Explain by giving one example how XPS can be applied in sample analysis. (8 markah/marks) BAHAGIAN B (50 MARKAH) 4/7

5 SECTION B (50 MARKS) Jawab SEMUA soalan. Answer ALL questions. 2. Sel unit merujuk kepada unit pengulangan atom dalam kekisi kristal dan ia biasanya digunakan untuk mengkaji struktur bahan kristal. Unit cell refers to repetition unit of atoms in crystal lattice and it is commonly used to study the structure of crystalline material. (a) Faktor Kepadatan Atom (APF) sel unit mencerminkan sebahagian daripada jumlah isipadu dalam struktur kristal yang diduduki oleh zarah juzuk. Lukiskan gambarajah berkaitan dan buktikan bahawa APF badan berpusat sel padu (BCC) adalah Atomic packing factor (APF) of a unit cell reflects the fraction of volume in a crystal structure that is occupied by constituent particles. Draw relevant diagram and prove that the APF of body centered cubic cell (BCC) is (10 markah/marks) (b) Ketumpatan Ketumpatan bahan kristal boleh dikira dengan menggunakan model sel unitnya. Terbitkan persamaan yang mengaitkan ketumpatan, ρ kepada bilangan atom, n dan isipadu unit sel, Vc. Anda mungkin perlu memasukkan kuantiti lain dalam persamaan tersebut. Density of a crystalline material can be calculated using its unit cell model. Derive an expression that relates the density, ρ to the number of atoms, n and volume of unit cell, Vc. You may need to include other quantities in the expression. (4 markah/marks) (c) Guna persamaan yang telah diperolehi dalam 2(b) untuk mengira ketumpatan logam Cu. Diberi logam Cu mempunyai struktur kristal FCC, jejari atom nm, dan jisim atom 63.5 g /mol. Using the expression that you have derived in 2(b), calculate density of Cu metal. Given Cu has FCC crystal structure, atomic radius of nm, and atomic mass of 63.5 g/mol. [Pemalar Avogadro, N A = x mol -1 ; Avogadro constant, N A = x mol -1 ] (6 markah/marks) 5/7

6 3. (a) Selain daripada struktur, ikatan antara atom adalah salah satu faktor yang mempengaruhi sifat bahan. Terangkan yang berikut: Besides structure, interatomic bonding is known to be another factor that affects the properties of a material. Explain the followings: (i) (ii) Logam adalah berkilat tetapi kebanyakan seramik tidak Metal is lustrous but most ceramics not Logam boleh ditempa dan mulur, tetapi kebanyakan seramik rapuh Metal is malleable and ductile, but most ceramics are brittle (8 markah/marks) (b) Terangkan perbezaan di antara pembajaan haba dan pembajaan kimia bagi kaca. Huraian anda hendaklah termasuk proses pembajaan dan jenis kaca yang sesuai untuk setiap kaedah. Explain the difference between thermal tempering and chemical tempering of glass. Your explanation should include the tempering process, and types of glass suitable for each method. [12 markah/marks) 4. (a) Pencampuran dua unsur bersama dengan syarat unsur utama adalah logam akan menghasilkan produk akhir yang dikenali sebagai aloi binari. Terangkan faktor yang membawa kepada pembentukan aloi isomorfus binari dan aloi eutektik binari. Mixing two elements together in a way that the major element is a metal will produce an end product known as binary alloy. Explain the factors that lead to the formation of binary isomorphous alloy and binary eutectic alloys. (4 markah/marks) (b) Gambarajah fasa boleh digunakan untuk meramalkan bahagian fasa (L dan α) di dalam aloi pada suhu dan komposisi yang tertentu. Lakar gambarajah fasa bagi aloi isomorfus binari yang berikut sekali lagi pada kertas jawapan anda, dan tunjukkan bagaimana pecahan jisim fasa α dan fasa L pada titik B boleh diperolehi. [Nota: Anda tidak perlu melakar mengikut skala, dan anda boleh menggunakan simbol yang direka-bentuk sendiri] Phase diagram can be used to predict the proportion of phases (L and α) present in an alloy at given temperature and composition. Sketch the following phase diagram of a binary isomorphous alloy again in your answer sheet and show how the mass fraction of phase α and phase L at point B can be obtained. 6/7

7 [Note: You don t have to draw according to scale, and you may use your own designed symbol] (6 markah/marks) TAMAT END 7/7

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