Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 1 of 15 CTS Ref. CTSSA/13/3207/Tanaka
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1 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 1 o 15 TANAKA ELECTRONICS (M) SDN BHD PLOT 11, PHASE IV, BAYAN LEPAS FREE INDUSTRIAL ZONE PENANG, MALAYSIA The ollowing merchandise was (were) submitted and identiied by the client as: Sample Description : Au Bonding Wire Sample Receiving Date : 10/10/2013 Testing Period : 10/10/2013 to 17/10/2013 Date Completed : 17/10/2013 Reporting Date : 01/11/2013 Test Requested : Selected test(s) as requested by client Test Method : Please reer to next page(s). Test Results : Please reer to next page(s). Analysts : Ng Jing Wei, Cho Kar Yen, Tan Li Wei, Teh Pui Sean, Lim Meng Hoe Tay Siam Pine & Yee Sook Wai
2 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 2 o 15 Test results: Test Part Description : Sample Description : Au Bonding Wire RoHS Directive 2011/65/EU Annex II Test Item(s): Unit Test Method Results MDL Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium (CrVI) Hexavalent Chromium (CrVI) by Spot test / boiling water extraction (optional) # Sum o PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl perormed by ICP-OES perormed by ICP-OES perormed by ICP-OES With reerence to JIS H 8625, and perormed by UV-VIS Spectrophotometry N.D. 2 N.D. 2 N.D. 2 N.D With reerence to IEC 62321:2008 Negative - N.D. -
3 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 3 o 15 Sum o PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether N.D. - Note : (a) = ppm ; (0.1wt% = 1000ppm) (b) N.D. = Not Detected (c) MDL = Method Detection Limit (d) # = Spot-Test: a. Negative means the absence o Cr(VI) on the tested areas b. Positive means the presence o Cr(VI) on the tested areas (The tested sample should be urther veriied by boiling-water-extraction method i the spot test result is negative or cannot be conirmed) Boiling water extraction: a. Negative means the absence o Cr(VI) on the tested areas b. Positive means the presence o Cr(VI) on the tested areas; The detected concentration in 50 ml boiling water extraction solution is equal or greater than 0.02 with 50 cm 2 sample surace area. For corrosion protection coatings on metals: Inormation on storage conditions and production date o the tested sample is unavailable and thus results o Cr(VI) represent status o the sample at the time o testing. (e) - = Not regulated
4 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 4 o 15 Test results by chemical method: Test Item (s): Unit Method Result MDL Antimony (Sb) With reerence to EPA Method 3051A, and perormed by ICP-OES N.D. 2 Magnesium (Mg) With reerence to EPA Method 3051A, and perormed by ICP-OES N.D. 2 Beryllium (Be) With reerence to EPA Method 3051A, and perormed by ICP-OES 5 2 Polyvinylchloride (PVC) ** Analysis was perormed by FT-IR/ATR Negative - Halogen Halogen-Fluorine (F) With reerence to BS EN Analysis was perormed by IC method or Fluorine content. 0 Halogen-Chlorine (Cl) With reerence to BS EN Analysis was perormed by IC method or Chlorine content. 0 Halogen-Bromine (Br) With reerence to BS EN Analysis was perormed by IC method or Bromine content. 0 Halogen-Iodine (I) With reerence to BS EN Analysis was perormed by IC method or Iodine content. 0 Test Part Description: Sample Description : Au Bonding Wire Note : (a) = ppm (b) N.D. = Not Detected (d) --- = Not Conducted (e) - = Not regulated () ** = Qualitative analysis (no unit) (g) MDL= Method Detection Limit (h) Negative = Undetectable / Positive = Detectable
5 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 5 o 15 Test results by chemical method: Test Item (s): Unit Method Result MDL Hexabromocyclododecane (HBCDD) Based on EPA 3540C, and perormed by GC-MS N.D. 10 Phthalates DBP (Di-butyl phthalate) % DEHP (Di-(2-ethylhexyl phthalate) % BBP (Benzyl Butyl phthalate) % DINP (Di-isononyl phthalate) % DIDP (Di-isodecyl phthalate % DNOP (Di-n-octyl phthalate) % DNHP (Di-n-hexyl phthalate) % DMEP (Bis(2-methoxyethyl)phthalate) *Di-isobutyl phthalate (DIBP) % Test Part Description: Sample Description : Au Bonding Wire % With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. With reerence to Chromatographia Vol.47, No.784, Analysis was perormed by GC/MS. Note : (a) = ppm (b) N.D. = Not Detected (c) MDL = Method Detection Limit (d) --- = Not Conducted (e) * = The above result is extracted rom the Report No. CTSSA/22889/13 N.D N.D N.D N.D N.D N.D N.D N.D N.D
6 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 6 o 15 Test Part Description : Sample Description : Au Bonding Wire Test results: Test Item (s): Unit Method Result MDL Dimethyl Fumarate (CAS No ) Perluorooctane sulonates (PFOS) PFOS Acid, Metal Salt, Amide PFOA (CAS No.: ) *Phosphorus (P) *Polychlorinated Naphthalene (PCNs) *Polychlorinated Terphenyls (PCTs) With reerence to US EPA 3550C method. Analysis was perormed by GC/MS. With reerence to US EPA 3540C: 1996 method or PFOS content. Analysis was perormed by LC/MS. With reerence to US EPA 3540C: 1996 method or PFOA content. Analysis was perormed by LC/MS. With reerence to US EPA Method 3052 or Phosphorus Content. Analysis was perormed by ICP-AES With reerence to US EPA 3540C method. Analysis was perormed by GC/MS With reerence to US EPA 3540C method. Analysis was perormed by GC/MS N.D. 0.1 N.D. 10 N.D. 10 N.D. 2 N.D. 0.5 Note : (a) = ppm (b) N.D. = Not Detected (c) MDL = Method Detection Limit (d) --- = Not Conducted (e) * = The above tests were subcontracted to SGS Taiwan based on report no. KA/2013/A0723 PFOS Reerence Inormation : POPs (EU) 757/2010 Outlawing PFOS as substances or preparations in concentrations above 0.001% (10ppm), in semi-inished products or articles or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1µg/m 2.
7 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 7 o 15 Test Part Description : Sample Description : Au Bonding Wire TANAKA ELECTRONICS (M) SDN BHD CTSSA/22191/13+KA/2013/A0723 SGS authenticate the photo on original report only
8 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 8 o DETERMINATION OF CADMIUM CONTENT BY IEC Sample Receiving and Registration 2. DETERMINATION OF LEAD CONTENT BY IEC Sample Receiving and Registration Cut sample in small pieces Weight sample ( g) into digestion vessel Acid digestion (Microwave) Totally Dissolved Filtration Analyses by ICP 3. DETERMINATION OF MERCURY CONTENT BY IEC Sample Receiving and Registration Cut sample in small pieces Weight sample ( g) into digestion vessel Acid digestion (Microwave) Totally Dissolved Filtration Analyses by ICP 5. DETERMINATION OF PBB/PBDE WITH GC-MS BY IEC Cut sample in small pieces Weight sample ( g) into extraction thimble Soxhlet Extraction with Toluene Filter through 0.45 um membrane ilter Analyses by GC-MS (with appropriate dilution) Cut sample in small pieces Weight sample ( g) into digestion vessel Acid digestion (Microwave) Totally Dissolved Filtration Analyses by ICP 4. DETERMINATION OF HEXAVALENT CHROMIUM BY IEC Sample Receiving and Registration Sample Preparation Spot-test (Qualitative) Boiling-water-extraction Analyses by UV- Spectrophotometer Test Report 6. DETERMINATION OF HEXAVALENT CHROMIUM BY JIS H 8625 Sample Preparation Hot water extraction Add colour-developing reagent Let stand or 5-10 min Analyses by UV- Spectrophotometer (540 nm)
9 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 9 o 15 DETERMINATION OF HALOGEN CONTENT Sample pretreatment Weighting and putting sample in cell Combustion / Absorption Dilution to ixed volume Analyses by IC MICROWAVE ASSISTED ACID DIGESTION OF ORGANICALLY BASED METRICES (US EPA 3051A) Cut sample in small pieces Weight sample ( g) into digestion vessel Acid digestion (HNO 3) Microwave Totally Dissolved Filtration Analyses by ICP FLOW CHART FOR PVC DETECTION WITH FTIR Sample preparation (apply ATR or analysis) FT-IR Scanning Report
10 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 10 o 15 DETERMINATION OF HBCDD CONTENT BY IEC Cut sample in small pieces Weight sample ( g) into extraction thimble Soxhlet Extraction with Toluene Filter through 0.45 um membrane ilter Analyses by GC-MS (with appropriate dilution)
11 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 11 o 15 Analytical low chart o Phthalates Content Sample pre-treatment/separation Sample extraction by soxhlet method Concentrate/Dilute Extracted solution Analysis was perormed by GC/MS Data
12 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 12 o 15 Analytical Flow Chart or Dimethyl Fumarate Sample pre-treatment/separation Sample extraction by organic solvent Concentrate/Dilute Extracted solution Analysis was perormed by GC/MS Data
13 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 13 o 15 Analytical Flow Chart o PFOS & PFOA Content Sample pre-treatment/separation Sample extraction by soxhlet method Concentrate/Dilute Extracted solution Analysis was perormed by LC/MS Data
14 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 14 o 15 1) These samples were dissolved totally by pre-conditioning method according to below low chart. 2) Name o the person who made measurement: Alex Chang 3) Name o the person in charge o measurement: Ray Chang Flow Chart o digestion or the elements analysis perormed by ICP-AES Cutting / Preparation Sample Measurement Acid digestion by suitable acid depended on dierent sample material (as below table) Filtration Solution Residue 1) Alkali Fusion 2) HCI to dissolve ICP-AES Steel, copper, aluminium, solder Aqua regia, HNO 3, HCI, HF, H 2 O 2 Glass HNO 3 /HF Gold, platinum, palladium, ceramic Aqua regia Silver HNO 3 Plastic H 2 SO 4, H 2 O 2, HNO 3, HCI Others Any acid to total digestion
15 Test Report No. CTSSA/22191/13+KA/2013/A0723 Date : 01/11/2013 Page: 15 o 15 Chlorinated Flame retardant analytical Flow Chart 1) Name o the person who made measurement: Anson Tsao 2) Name o the person in charge o measurement: Ray Chang Reerence method: US EPA 8270D, US EPA 3540 Test Item: PCNs, PCTs, Mirex Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the Extracted solution Analysis was perormed by GC/MS Data **** End o Report ****
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