Example problems: See your first-year assignments, tests and textbook.

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1 CHM212 Quantitative Chemical Analysis. The example problems suggested do not cover everything presented in the course and are not meant to limit the material that you study. You should, for example, understand terms, methods and procedures and be able to define and explain them. Lec. Date Topic 1 Sept. 9 Introduction. Syllabus, expectations. Prior knowledge: first-year chemistry or equivalent, eg. SI units, chemical nomenclature, stoichiometry, mathematical manipulations. Acceptable reference sources. Rules for success. Example problems: See your first-year assignments, tests and textbook. Wednesday: Lab safety orientation 2 Sept. 14 Overview of analytical chemistry, applications in clinical diagnostics, paperbased diagnostics, case study: FDA & heparin. Analytical methods specifications ( 5-1). General steps in a chemical analysis ( 0-3). Method validation ( 5-2). Concentration units ( 1-2) Example problems: 1-A, 1-B, 1-C, 1-4, 1-12, 1-13, 1-14, 1-17, 1-22, 1-28, 1-33, Tuesday: Lab safety orientation Wednesday: Experiment 1, Week 1 of 2. See recommended reading in lab write-up you are responsible for it. 3 Sept. 16 Concentration units ( 1-2) Introduction to activity and ionic strength ( 7-1, 7-2, 7-3). We will eventually develop the tools to solved for ph as shown in the example in 7-3. Example problems: 7-3, 7-4, 7-5, 7-6. Quiz #1 Assignment #1 4 Sept. 21 Ionic strength and activity, continued. Errors in chemical analysis (partly covered in 3-3; see notes for full coverage), quantification of errors. Quiz #2 Tuesday: Experiment 1, Week 1 of 2 Wednesday: Experiment 1, Week 2 of 2 5 Sept. 23 Interpolation of data (example from Assignment #1) Errors in chemical analysis (partly covered in 3-3; see notes for full coverage), quantification of errors.

2 Case study: ELISA ( 18-5). Rounding, page 53. Example problems: 3-10, 3-12, Sept. 28 Repeat of requirements for submitted work, 3 molarity/molality conversion approaches Constant vs. proportional errors Detection of errors (notes, also 5-2) Reporting: Be familiar with 3-2. Propagation of error 3-4, Table 3-1 (or physical chemistry rules) Chapter 4: Gaussian distribution and relation to standard deviation, variance, coefficient of variation. Understand page 71 Area under a Gaussian curve 4-2: Confidence intervals Example problems: see examples in text for propagation of error, also 3-15, 3-16, 3-17, 3-18, 3-19, 3-20, 3-21, 3-22; 4-2, 4-3, 4-4 Tuesday: Week 2 of 2 Wednesday: Experiment 2 7 Sept : Confidence intervals 4-3: t-test 4-4: F-test see also ed notes 4-6: Grubbs test Example problems: 4-8, 4-9, 4-11, 4-13, 4-14, Oct Calibration curves, sensitivity, selectivity, detection limits Example problems: 4-24, 4-25, 4-27, 4-28, 4-33 Tuesday: Experiment 2 Wednesday: Experiment 3 9 Oct : The equilibrium constant 6-5: Protic acids and bases, conjugate acid-base pairs 6-6: ph, autoprotolysis of water 6-7: Strengths of acids and bases, K a, polyprotic acids and bases 7-3: K w and activities Example problems: 6-Aa (you should be able to do this based only on the rules for reactions and equilibria constants), 6-H, 6-I, 6-J, 6-4, 6-5, 6-6, 6-30, 6-36, 6-41, 6-45, 6-47, 6-49, 6-50, Oct. 12 Assignment #3

3 Tuesday: no Tuesday classes Wednesday: Experiment 4 10 Oct & 7-3: Iterative solution to water autoprotolysis using activities. 11 Oct. 19 TEST #1: Bring calculators and pens Tuesday: Expt #3 Wednesday: Expt #5, Week 1 of 2 12 Oct : Iterative solution to water autoprotolysis using activities 7-4, 7-5: Systematic treatment of equilibrium (we have not yet covered K sp in CHM212). 13 Oct , , Oct , 8-4, Nov Example problems (activity questions are review): 7-B, 7-F, 7-G (add K w equilibrium), 7-11, 7-12, 7-18, 7-19, 7-20, 7-21, 7-23, 7-24, 7-24, 7-28 (perhaps delay 7-28). Tuesday: Expt #4 Wednesday: Expt #5, Week 2 of 2 Example problems: 8-A, 8-B, 8-D, 8-E, 8-F, 8-1, 8-2, 8-3, 8-4, 8-5, 8-6, 8-10, 8-11, 8-14, 8-19, Nov Chapter 9 Example problems: 8-H, 8-I, 8-J, 8-K, 8-26, 8-27, 8-31, 8-32, 8-37, 8-39, 8-40, 8-45 (constants over equilibria arrows are the equilibria constants for the listed equilibria). Tuesday: Expt #5, Week 1 of 2 Wednesday: Expt #6 17 Nov. 9 Example problems: Complete exercise given in class. 9-3, 9-24, 9-25, 9-26, 9-27

4 Tuesday: Expt #5, Week 2 of 2 Wednesday: no lab this week, Thursday class instead. 18 Nov. 10 Chapter 9: 9-1(save The Intermediate Form ), 9-4, 9-5 Example problems: 9-Aa, 9-Ac; 9-F, 9-4a, 9-4c, 9-5a, 9-5c, 9-28, 9-29, 9-30, 9-31, 9-32, 9-33, **9-36**-Sketch this instead of using Excel plot the correct significant points on the curve. WEDNESDAY (A Thursday class). NO CLASSES NOV Nov. 16 TEST #2 DATE Tuesday: Expt #6 Wednesday: Expt #7 20 Nov. 18 Finished 9-1, 9-3, 9-2 (do p. 193 example yourself). Example problems: 9-Ab, 9-B, 9-C, 9-1, 9-2, 9-3, 9-4b, 9-5b, 9-10, 9-13, 9-14, 9-15, 9-16, 9-17, 9-18, 9-19, 9-20, Note: When doing problems, it is recommended that you follow the examples in the class notes (eg. checking approximations) because it is the most general way of approaching problems. 21 Nov Box Tuesday: Expt #7 Example problems: 9-H, 9-38, 9-39, 9-40, Nov. 25 NO CLASSES, THANKSGIVING BREAK. 22 Nov : Beer s law as covered in class. Example problems: 17-B, (17-4 for those interested in physical chemistry), 17-7, 17-11, See next day for Chapter 10 example problems. Tuesday: Lab exam: Standardization of NaOH marked on results Wednesday: Lab Exam: Standardization of NaOH marked on results 23 Dec Example problems: 10-A, 10-B, 10-C, **10-G**, **10-J**, **10-1**, 10-2, **10-4**, 10-6, **10-7**, **10-8**, **10-12**, **10-13**, 10-14, **10-15**, **10-18**, **10-19**

5 24 Dec. 7 Finish diprotic titrations. Move to Sections 6-3 and 6-4. Tuesday: no lab Wednesday: no lab 25 Dec. 9 (Thursday) LAST CLASS

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