If you have any questions concerning this report, please feel free to contact me. REPORT OF LABORATORY ANALYSIS
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1 #=CL# LI USE: FR - JILL LAVOIE LI OBJECT ID: August 22, 2014 Jill Lavoie Merrimack Village District - UCMR3 2 Greens Pond Road Merrimack, NH RE: Dear Jill Lavoie: Enclosed are the analytical results for sample(s) received by the laboratory on July 23, The results relate only to the samples included in this report. s reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Veronica Brown veronica.brown@pacelabs.com Project Manager Enclosures Page 1 of 16
2 #=CP# CERTIFICATIONS Ormond Beach Certification IDs, Alabama Certification #: Arizona Certification #: AZ0735 Colorado Certification: FL NELAC Reciprocity Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E Kentucky Certification #: Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: Maryland Certification: #346 Massachusetts Certification #: M-FL1264 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS Nevada Certification: FL NELAC Reciprocity New Hampshire Certification #: 2958 New Jersey Certification #: FL765 New York Certification #: North Carolina Environmental Certificate #: 667 North Carolina Certification #: Pennsylvania Certification #: Puerto Rico Certification #: FL01264 South Carolina Certification: # Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: Washington Certification #: C955 West Virginia Certification #: 9962C Wisconsin Certification #: Wyoming (EPA Region 8): FL NELAC Reciprocity Page 2 of 16
3 #=SS# SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received 001 EP 502 Drinking Water 07/21/14 10:45 07/23/14 10: EP BLANK Drinking Water 07/21/14 10:45 07/23/14 10: MR002 Drinking Water 07/14/14 10:10 07/23/14 10:50 Page 3 of 16
4 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory 001 EP 502 EPA DRS 5 PASI-O EPA JLR 10 PASI-O EPA CLS 1 PASI-O 002 EP BLANK EPA HEA 5 PASI-O 003 MR002 EPA CLS 1 PASI-O Page 4 of 16
5 #=AR# ANALYTICAL RESULTS Sample: EP 502 Lab ID: 001 Collected: 07/21/14 10:45 Received: 07/23/14 10:50 Matrix: Drinking Water s s Units PQL MDL DF Prepared Analyzed CAS No. Qual MET ICP UCMR Analytical Method: EPA Preparation Method: EPA Chromium 0.37 ug/l /12/14 04:00 08/20/14 08: Cobalt 0.57 I ug/l /12/14 04:00 08/20/14 08: Molybdenum <0.33 ug/l /12/14 04:00 08/20/14 08: N2 Strontium 126 ug/l /12/14 04:00 08/20/14 09: D4 Vanadium 2.3 ug/l /12/14 04:00 08/20/14 08: N V Analytical Method: EPA Bromochloromethane <0.020 ug/l /04/14 18: Bromomethane <0.067 ug/l /04/14 18: ,3-Butadiene <0.033 ug/l /04/14 18: Chlorodifluoromethane <0.027 ug/l /04/14 18: Chloromethane <0.067 ug/l /04/14 18: ,1-Dichloroethane <0.010 ug/l /04/14 18: ,2,3-Trichloropropane <0.010 ug/l /04/14 18: Surrogates 4-Bromofluorobenzene (S) 101 % /04/14 18: ,2-Dichlorobenzene-d4 (S) 100 % /04/14 18: Methyl-tert-butyl ether-d3 (S) 92 % /04/14 18: Hexavalent Chromium by IC Analytical Method: EPA Chromium, Hexavalent 0.14 ug/l /24/14 18: Page 5 of 16
6 #=AR# ANALYTICAL RESULTS Sample: EP BLANK Lab ID: 002 Collected: 07/21/14 10:45 Received: 07/23/14 10:50 Matrix: Drinking Water s s Units PQL MDL DF Prepared Analyzed CAS No. Qual MET ICP UCMR Analytical Method: EPA Preparation Method: EPA Chromium <0.067 ug/l /01/14 11:23 08/07/14 14: Cobalt <0.33 ug/l /01/14 11:23 08/07/14 14: Molybdenum <0.33 ug/l /01/14 11:23 08/07/14 14: N2 Strontium <0.10 ug/l /01/14 11:23 08/07/14 14: Vanadium <0.067 ug/l /01/14 11:23 08/07/14 14: N2 Page 6 of 16
7 #=AR# ANALYTICAL RESULTS Sample: MR002 Lab ID: 003 Collected: 07/14/14 10:10 Received: 07/23/14 10:50 Matrix: Drinking Water s s Units PQL MDL DF Prepared Analyzed CAS No. Qual Hexavalent Chromium by IC Analytical Method: EPA Chromium, Hexavalent 0.14 ug/l /24/14 18: Page 7 of 16
8 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MPRP/19889 EPA Associated Lab Samples: 002 Analysis Method: Analysis Description: EPA MET UCMR Drinking Water METHOD BLANK: Associated Lab Samples: 002 Units Blank Matrix: Water Reporting Limit Analyzed Chromium ug/l < /07/14 14:39 Cobalt ug/l < /07/14 14:39 Molybdenum ug/l < /07/14 14:39 N2 Strontium ug/l < /07/14 14:39 Vanadium ug/l < /07/14 14:39 N2 Qualifiers LABORATORY CONTROL SAMPLE: Units LCS LCS Limits Chromium ug/l I Cobalt ug/l Molybdenum ug/l N2 Strontium ug/l Vanadium ug/l N2 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Units D D D Max Limits RPD RPD Chromium ug/l Cobalt ug/l Molybdenum ug/l N2 Strontium ug/l D4 Vanadium ug/l N2 Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 8 of 16
9 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MPRP/20029 EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA MET UCMR Drinking Water METHOD BLANK: Associated Lab Samples: 001 Units Blank Matrix: Water Reporting Limit Analyzed Chromium ug/l < /20/14 07:48 Cobalt ug/l < /20/14 07:48 Molybdenum ug/l < /20/14 07:48 N2 Strontium ug/l < /20/14 07:48 Vanadium ug/l < /20/14 07:48 N2 Qualifiers LABORATORY CONTROL SAMPLE: Units LCS LCS Limits Chromium ug/l I Cobalt ug/l Molybdenum ug/l N2 Strontium ug/l Vanadium ug/l N2 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Units D D D Max Limits RPD RPD Chromium ug/l 0.18 I J(M1) Cobalt ug/l Molybdenum ug/l < N2 Strontium ug/l D4 Vanadium ug/l 0.16 I N2 Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 9 of 16
10 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: V/12347 EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA V UCMR METHOD BLANK: Associated Lab Samples: 001 Units Blank Matrix: Water Reporting Limit Analyzed 1,1-Dichloroethane ug/l < /04/14 17:08 1,2,3-Trichloropropane ug/l < /04/14 17:08 1,3-Butadiene ug/l < /04/14 17:08 Bromochloromethane ug/l < /04/14 17:08 Bromomethane ug/l < /04/14 17:08 Chlorodifluoromethane ug/l < /04/14 17:08 Chloromethane ug/l < /04/14 17:08 1,2-Dichlorobenzene-d4 (S) % /04/14 17:08 4-Bromofluorobenzene (S) % /04/14 17:08 Methyl-tert-butyl ether-d3 (S) % /04/14 17:08 Qualifiers LABORATORY CONTROL SAMPLE: Units LCS LCS Limits 1,1-Dichloroethane ug/l ,2,3-Trichloropropane ug/l ,3-Butadiene ug/l Bromochloromethane ug/l Bromomethane ug/l Chlorodifluoromethane ug/l Chloromethane ug/l ,2-Dichlorobenzene-d4 (S) % Bromofluorobenzene (S) % Methyl-tert-butyl ether-d3 (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Units D D D Max Limits RPD RPD 1,1-Dichloroethane ug/l < ,2,3-Trichloropropane ug/l < ,3-Butadiene ug/l < Bromochloromethane ug/l < Bromomethane ug/l < Chlorodifluoromethane ug/l < Chloromethane ug/l < ,2-Dichlorobenzene-d4 (S) % Bromofluorobenzene (S) % Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 10 of 16
11 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Units D D D Max Limits RPD RPD Methyl-tert-butyl ether-d3 (S) % Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 11 of 16
12 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: WETA/37982 EPA Associated Lab Samples: 001, 003 Analysis Method: Analysis Description: EPA Chromium, Hexavalent UCMR IC METHOD BLANK: Associated Lab Samples: 001, 003 Units Blank Matrix: Water Reporting Limit Analyzed Chromium, Hexavalent ug/l < /24/14 12:42 Qualifiers LABORATORY CONTROL SAMPLE: Units LCS LCS Limits Chromium, Hexavalent ug/l Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Units D D D Max Limits RPD RPD Chromium, Hexavalent ug/l Q Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Units D D D Max Limits RPD RPD Chromium, Hexavalent ug/l < Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 12 of 16
13 #=QL# QUALIFIERS DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) (D) - Matrix (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-O Pace Analytical Services - Ormond Beach ANALYTE QUALIFIERS I D4 J(M1) N2 Q The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Sample was diluted due to the presence of high levels of target analytes. Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. The lab does not hold TNI accreditation for this parameter. Sample held beyond the accepted holding time. Page 13 of 16
14 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 001 EP 502 EPA MPRP/20029 EPA ICPM/ EP BLANK EPA MPRP/19889 EPA ICPM/ EP 502 EPA V/ EP 502 EPA WETA/ MR002 EPA WETA/37982 Page 14 of 16
15 Page 15 of 16
16 Page 16 of 16
If you have any questions concerning this report, please feel free to contact me. REPORT OF LABORATORY ANALYSIS
#=CL# LIMS USE: FR - JILL LAVOIE LIMS OBJECT ID: July 16, 2015 Jill Lavoie Merrimack Village District - UCMR3 2 Greens Pond Road Merrimack, NH 03054 RE: Dear Jill Lavoie: Enclosed are the analytical results
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